• Title/Summary/Keyword: cultural temperature

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Study on the Resistance for Atmospheric Corrosion of Conventional Epoxy Resins applied to the Restoration of Iron Relics (철기 유물 복원에 사용되는 에폭시 수지 내후성 연구)

  • Lee, Sang-Jin;Kwon, Jeong-Soon;Nam, Byeong-Jik;Ahn, Byung-Chan
    • Journal of Conservation Science
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    • v.21
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    • pp.41-48
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    • 2007
  • The resistance for atmospheric corrosion of the conventional 5 epoxy resins (Araldite rapid, Araldite AW 106, Araldite SV 427, Devcon, and CDK), those were used to restoration of the iron relics, were investigated in this study. Temperature, UV light, and water were chosen for the factors of the atmospheric corrosion. The drastic voluminous changes of the epoxy resins were found at the temperature range between $40^{\circ}C$ and $70^{\circ}C$ After UV exposure, the colors of the epoxy resins were severely changed. In case of the indoor exposure the chroma value(${\Delta}E$) of the resins were less than 2, which showed a little changes of the colors. The result of the water contact angle test was Araldite rapid>AW 106>Devcon>SV 427>CDK. Although the contact angles of the resins were reduced by UV exposure, SV 427 was stable comparatively.

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Cultural Conditions for Mass Production of Antagonistic Bacillus subtills CAP134 (길항균 Bacillus subtillis CAP134의 대량생산을 위한 배양조건)

  • 박흥섭;조정일
    • Korean Journal of Organic Agriculture
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    • v.5 no.1
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    • pp.87-99
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    • 1996
  • Cultural conditions for mass production of the antagonistic bacteria, Bacillus subtills CAP134 against pathogens causing major airborne diseases to apple tree, effect of temperature, pH, carbon and nitrogen source in the culture broth were investigated. The bacterial growth was most vigorous when the temperature and pH of the culture broth was 30~$35^{\circ}$C, and 7, respectively. As for carbon source, dextrose was best followed in order by dextrose(monosaccharides)>sucrose(disaccharides)$\geq$saccharose(di-saccharides)>starch (polysaccharides). Among different sugars, bacterial growth was favored by in the order of brown, black and white sugars, indicating that the bacterial growth might be promoted by the minor elements presented as impurities in the less purified sugars. As for nitrogen source, organic forms were better to bacterial growth than inorganic forms, that is polypeptone was best followed in order by soy sauce, soybeen milk and inoganic nitrogens. Differences in bacterial growth among different forms of inorganic nitrogen were negligible.

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Cultural Conditions for Mass Production of Bacillus subtilis CAP141 (Bacillus subtilis CAP141의 고농도 배양조건)

  • 조정일;박흥섭
    • Korean Journal of Organic Agriculture
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    • v.6 no.1
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    • pp.85-98
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    • 1997
  • Cultural conditions for mass production of the antagonistic bacteria, Bacillus subtills CAP141 against pathogens causing major airborne diseases to apple trees, effects of temperature, pH, carbon and nitrogen source in the culture broth were investigated. The bacterial growth was most vigorous when the temperature and pH of the culture broth was 30~35$^{\circ}$C and 7, respectively. As for carbon source, dextrose was best followed in order by dextrose(monosaccharide) > sucrose(disaccharide) $\geq$ saccharose (market disaccharides) > starch (polysaccharieds). Among different sugars, bacterial growth was favored by in the order of brown, black and white supars, indicating that the bacterial growth might be promoted by the minor elements presented as impurities in the less purified sugars. As for nitrogen source, organic forms were better to bacterial growth than inorganic forms, that is polypeptone was best followed in order by soy sauce, soybeen milk and inorganic nitrogens. Differences in bacterial growth among different forms of inorganic nitrogen were negligible.

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Characterization of a Smelting Furnace in Ungyo Site in Wanju, Jeollabuk-do, Through Slag Analysis

  • Lee, Su Jeong;Cho, Nam Chul;Kang, Byoung Sun
    • Journal of Conservation Science
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    • v.35 no.4
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    • pp.373-383
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    • 2019
  • We characterized the smelting process and smelting furnace through scanning electron microscopy-energy dispersive spectroscopy, wavelength dispersive X-ray fluorescence, X-ray diffraction, and raman micro-spectroscopy with 13 relics including slags and furnace walls excavated from square-shaped building sites and pits of the Three Kingdoms site at the Ungyo site section I. Our results revealed that the principal components were FeO and SiO2; and CuO, PbO, and ZnO were contained in small quantities. Furthermore, fayalite, magnetite, augite, copper, and cuprite were found. High contents of FeO or SiO2 components seem to have been added to form fayalite to remove gangue in the smelting process. The relatively low content of S detected in the copper prills suggests that roasting was performed well. Cristobalite and mullite, which are minerals that indicate high-temperature found in the furnace wall, show that the smelting temperature was higher than 1,250℃. The findings of this study show a high possibility that the Wanju Ungyo site is smelting remains of copper ores, which are nonferrous metals, rather than iron. Various smelting byproducts excavated in this area in the future will help us better understand the copper smelting process that may have been performed since ancient times.

A Scientific Study for Physical Properties of Celadon in Firing Experiment (소성실험을 통한 청자의 물리적 특성 변화 연구)

  • Han, Min-su;Hong, Jong-Uk;Park, Ji-hee
    • 보존과학연구
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    • s.27
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    • pp.145-163
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    • 2006
  • This study is to be investigated through firing experiment in studio in order to reveal a physical properties of celadon according to change firing temperature. The results can be briefly summarized as below; Firstly, in measurement of color chromaticity, samples of first firing in body were effective in differentiating of changed color in samples from each other but there of second firing were not. The color of the glaze was more effective change than that of the body. Secondly, bulk density of body was increased with temperature and it was attained highest point in $1200^{\circ}C$ Additionally, water absorption ratio was most rapidly changed between $1000^{\circ}C$ and $1200^{\circ}C$Thirdly, in the microstructural analysis, body of samples in first firing have not specific characteristics in the changed patterns of microstructure. body and glaze of samples in second firing have many that. Consequently, we knew that this experiment can be provided researcher with physical properties and firing mechanisms of celadon.

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Study on the Prediction of Surface Color Change of Cultural Properties Materials by Fog Occurrence (안개 발생에 따른 문화재 표면의 색 변화 예측 연구)

  • Han, Ye Bin;Park, Sang Hyeon;Yu, Ji A;Chung, Yong Jae
    • Journal of Conservation Science
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    • v.32 no.4
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    • pp.491-500
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    • 2016
  • Fog is atmospheric in which tiny drops of water vapor are suspended in the air near the ground. Its form, occurrence, etc., change according to the temperature, relative humidity, wind and geographical features of the space around it. In particular, fog tends to occur near a source of water because of temperature and relative humidity difference. These days, climate change is increasingly affecting the occurrence of fog. Therefore the purpose of this study was to investigate how fog affects materials that are part of our cultural properties through outdoor exposure tests and artificial degradation. The degradation evaluation of materials as a function of fog occurrence frequency, showed that the color of metals changed noticeably, whereas dyed silk and Dancheong showed degradation on the surface and color differences but no particular tendencies. Therefore, damage prediction by color differences as a function of fog occurrence frequency was based on metal samples, which showed constant color differences. Through a comparison of the predictive value and color difference by outdoor exposure, the accuracy and applicability of the damage prediction formula was confirmed. If a more complex damage prediction formula is created, it is expected that prediction of the degree of material damage in the field would be possible.

A Study on Ion Extraction Characteristics of Ceramics by Cleaning Agents (보존처리용 세척제에 대한 토기의 이온용출 특성연구)

  • Park, Dae-Woo;Kang, Hyun-Mi;Nam, Byeong-Jik;Jang, Sung-Yoon;Ham, Chul-Hee
    • 보존과학연구
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    • s.31
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    • pp.43-57
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    • 2010
  • This study intends to provide quantitative data about the extraction characteristics of major elements of earthenware by executing soaking test of cleaning agents. It aims at providing basic data for the stability assessment when applying the cleaning agents for conserving earthenware. The data will be extracted from the analysis of co-relationship between the physical characteristics and the ion extraction characteristics. XRD analysis displayed that AT-1, AT-2 and AT-3 which did not generate mullite were fired at lower than 1,000 whereas AT-3 and AT-5 that included mullite were higher than 1,000. The degree of absorption was AT-4 > AT-2 > AT-1 > AT-3 > AT-5 in order and the correlation between the degree of absorption and firing temperature of earthenware displayed a positive correlation. Extraction amount of oxalic acid which was used for the removing iron oxide was AT-1 > AT-2 AT-4 > AT-3 > AT-5 in order. and the ion extraction data displayed that there is a positive correlation with absorption level. However AT-1 and AT-2 which were fired at lower temperature showed that there was no correlation between the ion extraction characteristics and absorption level. Ion extraction of citric acid produced little amount compared with the one of oxalic acid, yet it caused less damage to earthenware than oxalic acid when it applied. The result of ion extraction level in the absorption test displayed that Fe had higher level than in Si, Al from the test for both oxalic acid and citric acid. Based on the regression analysis of the data from the previous studies, the physical characteristics of the earthenware and ion extraction level, further studies will be conducted on the predicting technique on the extraction characteristics of major elements of earthenware samples for the conservation in future.

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Material Stability Assessment of Low Oxygen and Heating Treatment (저산소 및 열처리법에 대한 문화재 재질 안정성 평가)

  • Jang, Han Gyeol;Baek, Na Yeon;Kang, Dai Ill
    • Journal of Conservation Science
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    • v.30 no.2
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    • pp.149-156
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    • 2014
  • Low oxygen treatment and heating treatment are used to prevent insects in the field of food science. These eco-friendly control methods can be applied to biological control technique in conservation treatment of organic cultural properties. To evaluate material stability, low-oxygen treatment and low oxygen treatment are applied to wood, pigment, paper and textile that are related to historical wooden buildings. As a result, wood moisture content declined after low oxygen treatment. But decline rate is a little, so it can be expected to turn back original state as time passes. And test result on pigment, paper, textile of chrominance and strength of test materials are stable. But after heating treatment, pigments are separated.

A Study of Extracting Appropriate Conditions for Efficient Desalination for the Underwater Archaeological Ceramics from Ma Island in Taean (태안 마도출토 도자기의 효율적 탈염처리를 위한 조건도출 연구)

  • Nam, Byeong-Jik;Park, Dae-Woo;Kang, Hyun-Mi;Jang, Sung-Yoon;Jung, Yong-Hwa
    • Journal of Conservation Science
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    • v.26 no.2
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    • pp.133-142
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    • 2010
  • This paper focused on desalination method for the underwater archaeological ceramics. The desalination method applied in this study takes additional conditions such as the amount of desalting water, temperature, and agitation conditions and compares the effects of desalt process. The result of efficiency rate appears that the twenty-times of the object weight of desalting water is more effective than that of ten-times one, but shows less economic compared to the cost. In addition, the research shows that the efficiency rate has been improved around 20 to 30 %, yet such improvement is not taken into account as an effective result considering the risk of damage from the physical and chemical impact and the consumption of energy in applying additional method.