• Journal of the Korean Chemical Society
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• v.20 no.5
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• pp.417-423
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• 1976

Corona treatment of PE, PP and PVC showed a dramatic increase of bond strength when lap joints were made between the polymers and aluminum plates. Heating the corona-treated PE and PP, and PVC in a drying oven at 80 and $50^{\circ}C$, respectively, for 15 min reduced the bond strength to about a half of that of corona-treated but unheated polymers, which indicated that the increase of bond strength was not due to oxidation of the polymer surface. The Weibull distribution function was employed to check reliability of the scattered data obtained from testing the lap joints. It is speculated that electron was deposited on the corona-treated polymer surface to enhance bond strength with aluminum.

• Journal of the Korean Society for Nondestructive Testing
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• v.14 no.2
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• pp.112-121
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• 1994

This paper discusses the feasibility of ultrasonic C-scan technique for nondestructive evaluation of spot weld quality. Ultrasonic evaluation for spot weld quality was performed by immersion method with the mechanical and the electronic scanning of point-focussed ultrasonic beam(25 MHz). For the sake of the approach to the quantitative measurement of nugget diameter and the discrimination of the corona bond from nugget, preliminary infinitesimal gap experiment by newton ring is tried in order to set up the optimum ultrasonic test condition. Ultrasonic image data obtained were confirmed and compared by optical microscope and SAM(Scanning Acoustic Microscope) observation of the spot-weld cross section. The results show that the nugget diameter can be measured with the accuracy of 1.0mm, and voids included in nugget can be detected to $10{\mu}m$ extent with simplicity and accuracy. Finally, it was found that it is necessary to make a profound study of definite discrimination of corona bond from nugget and the approach of quantitative evaluation of nugget diameter by utilizing the various image processing techniques.

• Journal of the Korean Chemical Society
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• v.55 no.5
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• pp.741-745
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• 2011

Well-resolved vibronic emission spectra were recorded in the visible region from the corona discharge of precursor alkylbenzenes in a technique of corona excited supersonic expansion using a pinhole-type glass nozzle. From the observed spectra, we found the evidence of the presence of benzyl-type radicals generated by dissociation of C-C or C-H bonds of alkyl group. After identification of benzyl-type radicals formed in the corona discharge, we suggest that energy densities in alkyl chain play a crucial role in determining the bond dissociation during corona excitation.

• Journal of Welding and Joining
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• v.12 no.3
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• pp.109-117
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• 1994

Spot welding has wide used with a high work efficiency in the automotive and aerospace industries. Up to the present, the technique mainly used to test spot welds on production lines has been entirely depended upon destructive chisel or peel testing. Therefore, it's being very important assignment to secure the NDE technique which can be evaluate spot weld quality with more efficiency and high reliability. This paper discusses the feasibility of UNDE techniques to evaluate spot weld quality. For the sake of the approach to the quantitative measurement of nugget diameter and the discrimination of a the corona bond from nugget, ultrasonic c-scan image and distribution of reflective echo amplitude was measured by immersion method with the mechanical and the electronic scanning of point-focussed ultrasonic beam(25 MHz). As the results of this study, corona bond which is the most dangerous types of interface defects can be successfully detected, as well as expulsion and voids. Ultrasonic testing results were confirmed and compared by optical microscope and SAM(Scanning Acoustic Microscope) observation of the spot-weld cross section. The results show that the nugget diameter can be successfully measured with the accuracy of 0.8 mm.

• Proceedings of the Korean Society of Machine Tool Engineers Conference
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• 2003.10a
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• pp.301-306
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• 2003

Spot welding is frequently used for industrial purpose, such as automobile and aerospace industries and household appliances due to its high performance. In these day, robotization and systemization of welding process made it possible to produce more precise or smaller electric parts. And when it comes to welding of steel sheet, the size of nugget must be getting smaller. Therefore, welding conditions are limited to avoid defects, such as deformation, damage, weakening of joining area. In this research, the measurement of the nugget size by the nondestructive inspection has been conducted. As a result, the right estimation of the nugget size and void defects, the detection of corona bond near joining area, the selection of the optimum ultrasonic mode, and set up for ultrasonic inspection are studied. From the trustworthy solutions of nugget size estimated by results of measurement, the optimum inspection conditions depending upon the width of welding parts are determined as well.

• Proceedings of the Korean Society of Machine Tool Engineers Conference
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• 2004.10a
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• pp.49-53
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• 2004

Thin spot welding is frequently used for industrial purpose, such as automobile and aerospace industries and household appliances due to its high performance. In these days, the systemization of welding process made it possible to produce more precise or smaller electric parts. And when it comes to welding of steel sheets, the size of nugget must be getting smaller. Therefore, welding conditions are limited to avoid defects, such as deformation, damage and weakening of joining area. In this research, thin spot welding establishes the welding conditions, and then the measurement of the nugget size by the nondestructive inspection has been conducted. As a result, the right estimation of the nugget size, the detection of corona bond near joining area, the selection of the optimum ultrasonic mode, and setup for ultrasonic inspection are studied. From the trustworthy solutions of the nugget size estimated by results of measurement, the optimum inspection conditions depending upon the width of welding parts are determined as well.

• Restorative Dentistry and Endodontics
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• v.47 no.3
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• pp.28.1-28.12
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• 2022

Objectives: Metalloproteinase-inhibiting agents, such as chitosan, can prevent collagen degradation in demineralized dental substrates, thereby improving the adhesive interface. This study evaluated the bond strength (BS) and chemical and morphological characterization of the adhesive interface after applying chitosan solution to demineralized dentin. Materials and Methods: The 80 third molars were selected. Forty teeth underwent caries induction using the pH cycling method. The teeth were divided according to the treatment: distilled water (control) and 2.5% chitosan solution. The surfaces were restored using adhesive and composite resins. Half of the specimens in each group were aged, and the other half underwent immediate analyses. The teeth were sectioned and underwent the microtensile bond strength test (µTBS), and chemical and morphological analyses using energy-dispersive spectroscopy and scanning electron microscopy, respectively. Data analysis was performed using 3-way analysis of variance. Results: For µTBS, sound dentin was superior to demineralized dentin (p < 0.001), chitosan-treated specimens had higher bond strength than the untreated ones (p < 0.001), and those that underwent immediate analysis had higher values than the aged specimens (p = 0.019). No significant differences were observed in the chemical or morphological compositions. Conclusions: Chitosan treatment improved bond strength both immediately and after aging, even in demineralized dentin.

• Journal of Welding and Joining
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• v.35 no.1
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• pp.34-42
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• 2017

This paper presents a comparative study of the AC and MFDC resistance spot welding process with consideration of sheet thickness. The previous studies have confirmed that there is difference in the optimum welding current and expulsion current with AC and MFDC. The aim of this study was revealing the effect of sheet thickness on weldable current range and expulsion behavior for AC and MFDC welding processes. The optimum welding current of AC was lower (1.6 kA) than MFDC welding process in 0.8 mm sheet thickness. Early nugget growth being caused by the peak current of AC developed weld interface deformation, which resulted in suppressing the growth of corona bond and occurrence of low current expulsion. The resistance spot welding for thicker sheet (1.4 mm) required lower current of 0.6 kA for the expulsion on the MFDC welding process. The growth of contact diameter (size of corona bond) and button diameter was linear up to the expulsion current with MFDC welding process. Therefore, more attention is required when the AC and MFDC resistance spot welding process is applied for different thickness of steel sheet combination for automotive application.

• Journal of the Korean Society of Manufacturing Process Engineers
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• v.21 no.3
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• pp.1-11
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• 2022

In this study, an electric resistance dual-spot welding process using a copper electrode inserted in a heating electrode is suggested for the spot welding of AZ31 magnesium sheets. This spot-welding process involves two heating methods for welding at the interfacial zone between the magnesium sheets, one of which is the heating method by thermal conduction from the heating electrode heated by the welding current induced to the steel electrode, and the other heating method uses the electric resistance between the contacted surfaces of the two sheets by the welding current induced to the copper electrode. This welding process includes the welding variables, such as the current induced in the heating electrode and the copper electrode, and the outer diameters of the heating electrode. This is because the heat conducted from the heating electrode can be maintained at a higher temperature in the welding zone, which has a slow cooling effect on the nugget of the melted metal after the welding step. The pressure exerted during the pressing of the magnesium sheets by the heating electrode can be increased around the nugget zone at the spot-welding zone. Thus, it not only reduces the warping effect of the elastoplastic deformation of sheets, but also the corona bond can make it less prone to cracking at the welded zone, thereby reducing the number of nuggets expelled out of the corona bond. In conclusion, it was known that an electric resistance dual spot welding process using the copper electrode inserted in the heating electrode can improve the welding properties in the electric resistance spot welding process of AZ31 magnesium sheets.

• Journal of the Korea institute for structural maintenance and inspection
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• v.18 no.3
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• pp.153-159
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• 2014

This research reviewed the joint and duration characteristics depending on the surface treatment condition and lap spliced length in the PET film jointing method using the high hardness liquid material. As a result, the corona discharge treatment was improved to the contact angle, joint tensile strength, and joint peel resistance compared to non-treatment. Particularly, a surface treatment E (Corona discharge + Primer + PU bond + Polyester fabric) turned out to the best, and especially when the lap spliced length is longer than 15mm, stable joint performance was secured under the long term deterioration treatment of 16 weeks. Thus, the joint is considered to be applicable as the water-proof material.