• Title/Summary/Keyword: controlled synthesis

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Planar Error Sensitivity Analysis in a CNC Turning Cen (2차원 CNC 선반에서 평면오차 민감도 분석)

  • 여규환;이진현;양승한
    • Proceedings of the Korean Society of Precision Engineering Conference
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    • 1995.10a
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    • pp.1017-1021
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    • 1995
  • Geometric and thermal errors are responsible for major components of the errors of a computer numerically controlled turning center. The planar error of a CNC turning center are comprised of 11 geometric and thermal error components. The error synthesis model is formulated by homogeneous coordinate transformation method and expresses the effect of such error components on the planar error of a CNC turning center. In this paper, the sensitivity analysis of the model on the noises through sensing and the change of temperature is addressed. The sensitivity analysis show that the error systhesis model is robust on the noses and z planar error is much affected by the change of temperatures.

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Thermal Chemical Vapor Deposition of Graphene Layers

  • Kwon, Kyoeng-Woo;Do, Woo-Ri;Hwang, Jinha
    • Proceedings of the Korean Vacuum Society Conference
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    • 2013.02a
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    • pp.644-644
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    • 2013
  • Graphene is a two-dimensional sp2 layer material. Despite the short history in the empirical synthesis of the graphene layers, the academic/industrial unique features have brought highly significant interest in research and development related to graphene-related materials. In particular, the electrical and optical performances have been targeted towards pre-existing microelectronicand emerging nanoelectronic applications. The graphene synthesis relies on a variety of processing factors, such as temperature, pressure, and gas ratios involving H2, CH4, and Ar, in addition to the inherent selection of copper substrates. The current work places its emphasis on the role of experimental factors in growing graphene thin films. The thermally-grown graphene layers are characterized using physical/chemical analyses, i.e., four point resistance measurements, Raman spectroscopy, and UV-Visible spectrophotometry. Ultimately, an optimization strategy is proposed in growing high-quality graphene layers well-controlled through empirical factors.

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Glutamine Synthetase of some Fermentation Bacteria: Function and Application

  • Tachiki, Takashi
    • Proceedings of the Korean Society for Applied Microbiology Conference
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    • 1986.12a
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    • pp.506-508
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    • 1986
  • Metabolic activity of inorganic nitrogenous compounds affects not only microbial growth but also metabolite production in fermentation technology. We have worked on the enzymes participating in ammonia assimulation of some fermentation bacteria. This paper summarizes the results on glutamine synthetase and its application in practical field. Glutamine synthetase (L-glutamate:ammonia ligase, EC. 6.3.1.2) catalyzes the formation of glutamine from glutamate and ammonia at the expense of cleavage of ATP and inorganic phosphate. The enzyme plays a dual role in nitrogen metabolism in bacteria; it is a key enzyme not only in the biosynthesis of various compounds through glutamine but also in the regulation of synthesis of some enzymes involved in the metabolism of nitrogenous compounds. The detailed works with the Eschericia coli and other enterobacterial enzymes revealed that glutamine synthetase is controlled by the following complex of mechanisms: (a) feedback inhibition by end products, (b) repression and derepression of enzyme synthesis, (c) modulation of enzyme activity in response to divalent cation and (d) covalent modification of enzyme protein by adenylylation and its cascade control. Comparative studies have also been made on the enzymes from other organisms.

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Synthesis of Nanostructured Fe-Co Alloy Powders from Metal Salts

  • Lee, Young-Jung;Lee, Jea-Sung;Seo, Young-Ik;Kim, Young-Do
    • Journal of Powder Materials
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    • v.13 no.5 s.58
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    • pp.336-339
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    • 2006
  • Magnetic properties of nanostructured materials are affected in complicated manner by their microstructure such as pain size (or particle size), internal strain and crystal structure. Thus, studies on the synthesis of nanostructured materials with controlled microstructure are necessary fur a significant improvement in magnetic properties. In the present work, nanostructured Fe-Co alloy powders with a grain size of 50 nm were successfully fabricated from the powder mixtures of (99.9% purity) $FeCl_2$ and $CoCl_2$ by chemical solution mixing and hydrogen reduction.

A Study On Holistic Synthesis Human Face Images (얼굴 영상의 합성에 관한 연구)

  • 박호식;배철수
    • Journal of the Korea Institute of Information and Communication Engineering
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    • v.6 no.4
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    • pp.645-651
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    • 2002
  • This paper presents a method to automatically synthesized human fare images from holistic descriptions. We compactly represent the face set by a small set of prototypes, which can be used in simple ways generated controlled morphings. This becomes possible because separation of 2D-shape and texture provides a faithful, closed and convex representation of images, and smooths the mapping between images and their properties. With this approach, the user watches an images being continuously morphed according to his indications, and the synthesized images always obey the natural physiognomic constraints.

Synthesis of Star like Random Copolymers from Resorcinarene-based Alkoxyamine Initiator via Nitroxide Mediated Free Radical Polymerization

  • Abraham, Sinoj;Choi, Jae-Ho;Ha, Chang-Sik;Kim, Il
    • Proceedings of the Polymer Society of Korea Conference
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    • 2006.10a
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    • pp.337-337
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    • 2006
  • The synthesis of an octafunctional resorcinarene based initiator for nitroxide mediated polymerization and its ability to yield random star copolymers of styrene and methyl methacrylate is studied. The effect of the initiator conformations towards its activity and the conditions that permit the formation of well-defined star block copolymers is also investigated in detail. The characterization of the initiator and the polymers were carried out by various spectro-analytical techniques. Well-defined random copolymers were obtained with controlled molecular weight and low PDI depending on the monomer feed.

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Synthesis of iron oxide powders by hydrothermal process

  • Bae, Dong-Sik;Park, Chul-Won;Gam, Jig-Sang;Han, Kyong-Sop
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.11 no.4
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    • pp.176-179
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    • 2001
  • Iron oxide powders were prepared under high temperature (up to $175^{\circ}C$) and pressure conditions( up to 129 pasi) by precipitation from metal nitrates with aqueous potassium hydroxide. Various types of iron oxide powders were obtained at different conditions. The size and the shape of the particles can be controlled as afunction of starting solution pH. The average particles size of the synthesized iron oxide powders increased, the particle shapes of the powders became fibrous, and the crystalline phase of the powder changes from iron oxide to iron hydroxide with increasing solution pH. The effects of synthesis parameters are discussed.

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Process Control for the Synthesis of Ultrafine Si3N4-SiC Powders by the Hybrid Plasma Processing (Hybrid Plasma Processing에 의한 Si3N4-SiC계 미립자의 합성과정 제어)

  • ;吉田禮
    • Journal of the Korean Ceramic Society
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    • v.29 no.9
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    • pp.681-688
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    • 1992
  • Ultrafine Si3N4 and Si3N4+SiC mixed powders were synthesized through thermal plasma chemical vapor deposition(CVD) using a hybrid plasma, which was characterized by the supersposition of a radio-frequency plasma and arc jet. The reactant SiCl4 was injected into an arc jet and completely decomposed in a hybrid plasma, and the second reactant CH4 and/or NH3 mixed with H2 were injected into the tail flame through double stage ring slits. In the case of ultrafine Si3N4 powder synthesis, reaction efficiency increased significantly by double stage injection compared to single stage one, although crystallizing behaviors depended upon injection speed of reactive quenching gas (NH3+N2) and injection method. For the preparation of Si2N4+SiC mixed powders, N/C composition ratio could be controlled by regulating the injection speed of NH3 and/or CH4 reactant and H2 quenching gas mixtures as well as by adjusting the reaction space.

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Hardware design and control method for controlling an input clock frequency in the application

  • Lee, Kwanho;Lee, Jooyoung
    • International Journal of Advanced Culture Technology
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    • v.4 no.4
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    • pp.30-37
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    • 2016
  • In this paper, the method of controlling the clock that is inputted on the hardware from the application, and the hardware design method are to be proposed. When the hardware is synthesized to the Field Programmable Gate Array(FPGA), the input clock is fixed, and when the input clock is changed, the synthesis process must be passed again to require more time. To solve this problem, the Mixed-Mode Clock Manager(MMCM) module is mounted to control the MMCM module from the application. The controlled MMCM module controls the input clock of the module. The experiment was process the Neural Network algorithm in the x86 CPU and SIMT based processor mounted the FPGA. The results of the experiment, SIMT-based processors, the time that is processed at a frequency of 50MHz was 77ms, 100MHz was 34ms. There was no additional synthesis time due to a change of the clock frequency.

Synthesis and Optically Characterization of CdSe Nanocrystal (CdSe 나노입자의 합성과 광학 특징)

  • Kim, Chanyoung;Kim, Sunghyun;Jung, Daehyuk
    • Journal of Integrative Natural Science
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    • v.1 no.3
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    • pp.250-253
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    • 2008
  • New issues arise as to surface characterization, quantification and interface formation. Surface and interface control of CdSe nanocrystal systems, one of the most studied and useful nanostructures. Semiconductor quantum dots (QDs) have been the subject of much interest for both fundamental reseach and technical applications in recent years, due mainly to their strong size dependent properties and excellent chemical processibility. In this dissertation, the synthesis of CdSe quantum dots were synthesized by pyrolysis of high-temperature organometallic reagents. In order to modify the size and quality of quantum dots, we controlled the growth temperature and the relative amount of precursors to be injected into the coordinating solvent. Moreover, an effective surface passivation of monodisperse nanocrystals was achieved by overcoating them with a higher-band-gap material. Synthesized CdSe quantum dots were studied to evaluate the optical, electronic and structural properties using UV-absorption, and photoluminescence measurement.

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