• Title/Summary/Keyword: conductivity measurement

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Comparison of Nitrogen and Oxygen Annealing Effects on the Structural, Optical and Electrical Properties of ALD-ZnO Thin Films (ALD법으로 증착한 ZnO 박막의 열처리 분위기에 따른 구조적, 전기적 특성 비교)

  • Park Y. K.;Park A. N.;Lee C. M.
    • Korean Journal of Materials Research
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    • v.15 no.8
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    • pp.514-517
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    • 2005
  • Effects of nitrogen and oxygen annealing on the carrier concentration, carrier mobility, electrical resistivity and PL characteristics as well as the crystallinity of ZnO films deposited on sapphire substrates by atomic layer deposition (ALD). X-ray diffraction (XRD), Scanning electron microscope (SEM), photoluminescence (PL) analyses, and Hall measurement were performed to investigate the crystallinity, optical properties and electrical properties of the ZnO thin films, respectively. According to the XRD analysis results the crystallinity of the ZnO film annealed in an oxygen atmosphere is better than that of the ZnO film annealed in a nitrogen atmosphere. Annealing undoped ZnO films grown by ALD at a high temperature above $600^{\circ}C$ improves the crystallinity and enhances W emission but deteriorates the electrical conductivity of the flms. The resistivity of the ZnO film annealed particularly at $800^[\circ}C$ in a nitrogen atmosphere is much higher than that annealed at the same temperature in an oxygen atmosphere.

Temperature Analysis of Nozzle in a FDM Type 3D Printer Through Computer Simulation and Experiment

  • Park, Jung Hyun;Lyu, Min-Young;Kwon, Soon Yong;Roh, Hyung Jin;Koo, Myung Sool;Cho, Sung Hwan
    • Elastomers and Composites
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    • v.51 no.4
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    • pp.301-307
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    • 2016
  • Additive manufacturing (AM), so called 3D Printing is a new manufacturing process and is getting attraction from many industries. There are several methods of 3D printing. Among them fused deposition modeling (FDM) type is most widely used by reason of cheap maintenance, easy operation and variety of polymeric materials. Articles manufactured by 3D printing have weak deposition strength compared with conventionally manufactured products. Deposition strength of FDM type 3D printed article is highly dependent of deposition temperature. Subsequently the nozzle temperature in the FDM type 3D printing is very important and it is controlled by heat source in the 3D printer. Nozzle is connected with heat block and barrel, and heat block contains heat source. Nozzle becomes hot through heat conduction from heat source. Nozzle temperature has been predicted for various thermal boundary conditions by computer simulation and compared with experimental measurement. Nozzle temperature highly depends upon thermal conductivities of heat block and nozzle. Simulation results are good agreement with experiment.

Synthesis and Characterization of Delafossite $CuLaO_2$ for Thermoelectric Application

  • Takahashi, Yuhsuke;Matsushita, Hiroaki;Katsui, Akinori
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2006.09b
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    • pp.1114-1115
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    • 2006
  • The preparation of single-phase $CuLaO_2$ with delafossite-type structure by means of the solid-state reaction method was investigated using X-ray diffraction. The results showed that notwhistanding the fact that there was a trace of metallic copper, nearly single-phase $CuLaO_2$ was obtained by using $La(OH)_3$ as a lanthanum source and by firing the mixed powder with nonstoichiometric composition ratio of $La(OH)_3:Cu_2O=1:1.425$ in a vacuum at 1273 K for 10 h. The measurement of electrical conductivity and Seebeck coefficient showed that $CuLaO_2$ thus obtained was a p-type semiconductor and had a Seebeck coefficient of approximately $70{\mu}V/K$.

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Mechanical and Antibacterial Properties of Copper-added Austenitic Stainless Steel (304L) by MIM

  • Nishiyabu, Kazuaki;Masai, Yoshikaze;Ishida, Masashi;Tanaka, Shigeo
    • Journal of Powder Materials
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    • v.9 no.4
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    • pp.227-234
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    • 2002
  • For the austenitic stainless steel (304L) manufactured by metal injection molding(MIM), the effects of copper content and sintering temperature on the mechanical properties, antibacterial activities, corrosion resistance, and electric resistances were investigated. The specimens were prepared by injection molding of the premixed powders of water-atomized 304 L and Cu with poly-acetyl binders. The green compacts were prepared with various copper contents from 0 to 10 wt.% Cu, which were debound thermally at 873 K for 7.2 ks in $N_2$gas atmosphere and subsequently sintered at various temperatures from 1323 K to 1623 K for 7.2 ks in Ar gas atmosphere. The relative density and tensile strength of the sintered compacts showed the minimum values at 5 and 8 wt.% Cu, respectively. Both the relative density and the tensile strength of the specimen with 10 wt.% Cu sintered at 1373 K showed the highest values, higher than those of copper-free specimen. Antibacterial activities investigated by the plastic film contact printing method for bacilli and the quantitative analysis of copper ion dissolved in water increased as the increase of the copper content to stainless steels. It was also verified by the measurement of pitting potential that the copper addition in 304 L could improve the corrosion resistance. Furthermore the electric conductivity increased with the increase of copper content.

Application of Bulk Talc to Molding Material (주형재료로서 덩어리 활석의 이용)

  • Ha, Man-Jin;Lee, Zin-Hyoung;Lee, Sang-Soo;Eun, Hee-Joon
    • Journal of Korea Foundry Society
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    • v.14 no.1
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    • pp.45-51
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    • 1994
  • The possibility of using bulk talc as molding material was reviewed and tested with the measurement of thermal properties and computer simulations. The measured thermal conductivity and heat diffusivity($k{\rho}c$) of talc were $2.4W/m^{\circ}C$ and $6.6{\times}10^6J^2/m^4^{\circ}C^2s$, respectively. Thermal properties of talc could be ranked between those of sand mold and iron mold. Talc transforms into cristobalite and enstatite at $910^{\circ}C$, During the transformation volume and structure change, cracks appear on the surface and distortion occurs. Therefore talc can be used for molding material below $910^{\circ}C$ if carefully treated. Computer simulation was carried out to test whether talc insert could promote directional solidification in sand mold and iron mold. In sand mold, it was possible to achieve directional solidification of thin plate casting with the length to thickness ratio of 15, if both iron insert and talc insert were used. In iron mold, it was possible to achieve directional solidification only with talc insert.

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Estimation of Microwave Path Loss and Cross-Polarization Coupling in a Simple Urban Area

  • Yisok Oh;No, Chan-Ho;Sung, Hyuk-Je;Lee, Byung-Hoon;Koo, Yeon-Geon
    • Journal of electromagnetic engineering and science
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    • v.1 no.1
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    • pp.30-36
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    • 2001
  • Whereas it is well known that microwave propagation around corners of urban area is estimated well by the uniform geometrical theory of diffraction (UTD), it is not clear how much depolarization occurs at a given receiver position and how much transmission through walls affects to total path loss. This paper presents the results of the ray tracing simulation to answer these questions. Simulations of microwave propagation around corners were performed for various line-of-sight (LOS) and out-of-sight(OOS) positions of a receiver, by summing the electrical fields of reflected, diffracted and transmitted rays coherently. Since height difference between transmitter and receiver, as well as ground plane, causes depolarization, the ray tracing simulation estimates the cross-polarization coupling. It was found that the cross-polarization coupling decreases as receiver moves away from transmitter. Another part of the study focused on the signal transmitted through building walls of the corner. It was found that the transmitted field is dominant at OOS region when the conductivity of the walls is low (for example, lower than 0.0l S/m). The simulation results of the ray tracing technique in this study agreed well with an experimental measurement around corners.

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Gas Response and Electrical Properties of Organic Ultra-thin Films (유기 박막의 전기적 특성 및 가스 반응 특성)

  • 박재철
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.11 no.10
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    • pp.820-825
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    • 1998
  • We deposited stearic acid LB films by using Langmuir-Blodgett (LB)method and investigated anisotropy electrical conduction characteristics by I-V measurement for horizontal direction and vertical direction. Also, we measured gad response between deposited LB films and organic gas for various temperature(0~8$0^{\circ}C$) by 9MHz At-cut quartz crystal microbalance. The LB films have electrical conduction characteristics such as semiconducting and insulating properties. The is, the conductivity of LB films for the horizontal and vertical direction is about 10\ulcornerS/cm and 10\ulcorners/cm, respectively. the frequency shift of stearic acid LB films for the organic gases depended on the mass change by the surface adsorption and the inner penetration to the sensing films. The resonant frequency shift of the quartz crystal microbalance for temperature properties of LB films is thought to the effect of the rearrangement or the damage pf LB films above the melting point and the mobility increasement of the organic gas by the temperature rising.

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Development of Thermal Conductivity Measurement Device of Nanofluids Using Quasi-Steady State Method (준정상 상태법을 이용한 나노유체의 열전도도 측정장치 개발)

  • Park, Ji-Hun;Kim, Hyun-Jin;Jang, Seok-Pil
    • Proceedings of the Computational Structural Engineering Institute Conference
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    • 2010.04a
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    • pp.636-639
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    • 2010
  • 본 논문에서는 준정상 상태법을 이용한 열전도도 측정장치의 불확실도를 분석하고 측정된 열전도도의 불확실도에 가장 큰 영향을 미치는 요인이 온도 측정 센서의 정확도와 측정유체의 윗면과 아랫면의 온도 차임을 알아내었다. 특히 온도 측정센서의 정확도가 $0.1^{\circ}C$일 때 측정유체의 윗면과 아랫면의 온도차가 $18^{\circ}C$이상이면 준정상 상태법을 이용한 열전도도 측정장치의 불확실도가 ${\pm}1%$이내로 들어옴을 알 수 있었다. 따라서 온도 측정센서가 $0.1^{\circ}C$의 정확도를 가지며 측정유체의 윗면과 아랫면의 온도차가 $18^{\circ}C$이상이 되는 불확실도 ${\pm}1%$을 갖는 준정상 상태법을 이용한 나노유체의 열전도도 측정장치를 개발하였다. 개발된 실험장치의 검증을 위하여 DI-Water의 열전도도와 $Al_2O_3$ 나노유체의 열전도도를 각각 측정하여 기존 문헌 및 선행 연구자의 결과와 비교하여 보았고 개발된 장치가 ${\pm}1%$ 이내의 불확실도를 가지고 나노유체의 열전도도를 측정할 수 있음을 확인하였다.

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Determination of Springwater Characteristics by Measurement of Tritium in Water (삼중수소 측정에 의한 약수터 물의 수질특성 연구)

  • Kim, Jong Hun;Choi, Yong Wook;Chung, Taek Kyun
    • Journal of the Korean Chemical Society
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    • v.40 no.6
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    • pp.436-444
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    • 1996
  • The characteristics of water have been studied for 1 year by means of relationships between tritium and total dissolved solid(TDS), tritium and conductivity, tritium and chloride, and tritium and total hardness for 15 springs in the vicinity of Jeonju city of Korea. From the results of the study, the springs were divided into four characteristic groups, but the characteristics of most springwaters studied were similar to those of rainfall. Fifteen springwaters were evaluated to see if those are tasty and healthy using the Hashimoto's Mineral Balance Index. As a result, only one spring (J-4) was found as tasty and healthy.

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Preparation of bi-polar membranes and their application to hypochlorite production

  • Kim, Jung Sik;Cho, Eun Hye;Rhim, Ji Won;Park, Chan Jong;Park, Soo-Gil
    • Membrane and Water Treatment
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    • v.6 no.1
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    • pp.27-42
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    • 2015
  • In this study, poly (phenylene oxide) (PPO) and poysulfone (PSf) were sulfonated and aminated respectively. Both sulfonated poly (phenylene oxide) (SPPO) and aminated polysulfone (APSf) were characterized via the measurement of FT-IR, swelling degree, ion exchange capacity (IEC), and ion conductivity. Then the surfaces of these membranes were modified by surface fluorination using 2000 ppm $F_2$ gas against $N_2$ gas for 1 h at room temperature. The surface fluorinated SPPO and APSf membranes were characterized again to determine any differences between the pristine and fluorinated membranes. In total, 3 types of bi-polar membranes were prepared by varying the IEC of the APSf and having a fixed value for the IEC of the SPPO. The hypochlorite concentration generated by using the surface fluorinated membranes was dependent on the IEC of the APSf and ranged from 683 to 826 ppm, while there was a considerable improvement in the durability of the surface fluorinated membranes as they remained intact even after operating for 4 h.