• Journal of the Korean Society for Aeronautical & Space Sciences
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• v.34 no.9
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• pp.25-32
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• 2006

In this study, the characteristics of filament wound composite/aluminum ring specimens were investigated at cryogenic temperature. The ring specimens were manufactured using carbon fibre and Type B epoxy resin which had been developed for cryogenic use. As a result of measuring thermal strains at -150℃, it was found that compressive thermal stress was induced in composite part on the contrary, tensile thermal stress in aluminum part which was about 32% of yield stress and in turn, caused aluminum to be yielded at lower load level. In addition, Thermal strains which resulted from finite element analysis showed good agreement with those of the experiment. After 6 mechanical loading cycles had been applied to the ring specimen at -150℃, tensile tests were performed at -150℃ using a split disk fixture. As a result, it was shown that composite strength in a liner-composite tank structure which is for the use of cryogenic propellant tank would be decreased by auto-frettage pressure which is applied to it.

• Polymer(Korea)
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• v.26 no.1
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• pp.98-104
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• 2002

This study was investigated to fabricate the isotropic $Nd_2Fe_{14}B$/epoxy bonded magnets with high characteristics paroduced by compression molding. The magnetic characteristics of the bonded magnets were directly proportional to the density of the magnets and were enhanced by using raw $Nd_2Fe_{14}B$ magnetic powders, having the mean particle size of $200{\mu} m$.without additional milling process. The high characteristics of the bonded magnets were achieved at the following conditions: epoxy resin of 2.0 wt%, silane coupling agent of 0.8 wt%, curing agent of 0.7 wt% on the base of magnetic powders, and curing condition of $150^{\circ}C$/3 hrs. The bonded magnets at the optimum conditions indicated the high characteristics such as the density of 6.1 g/㎤, the remanent flux density of 7.1 kG, the maximum energy product of 9.7 MGOe, and the compressive strength of 17 kg/$mm^2$.

• Journal of Adhesion and Interface
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• v.10 no.4
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• pp.162-168
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• 2009

As a preliminary study of optimum composite properties under cryogenic temperature, the comparison of interfacial properties of carbon or glass fibers reinforced epoxy composites was evaluated at ambient and intermediate low temperature, i.e., 25 and $-10^{\circ}C$ by using micromechanical techniques. Under tensile and compressive loading conditions, their mechanical modulus at low temperature was higher than that atambient temperature. Interfacial shear strength (IFSS) at ambient and low temperatures was compared to each other, depending on epoxy matrix toughness and apparent modulus at the interface. The IFSS was much higher at low temperature than that at room temperature because of the increased epoxy matrix modulus. Statistical distributions of tensile strengths of glass and carbon fibers were evaluated for different temperature ranges, which is dependent upon fiber's inherent flaws and rigidity.

• Elastomers and Composites
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• v.50 no.2
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• pp.103-109
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• 2015

In this study, epoxy/anhydride mixing ratio for the highly silica filled compounds with chromium (III) octoate catalyst was investigated at a low curing temperature ($71^{\circ}C$ for 40 hr) by evaluating the compressive strength with the weight ratio ranges from 0.3/1.0 to 1.0/1.0 of epoxy part (Part A)/anhydride part (Part B). In case of epoxy/anhydride compounds used surface unmodified silica by coupling agent, these compounds need excess anhydride unlike the weight ratio in the conventional epoxy/anhydride compounds. In curing behavior, the epoxy/anhydride compounds containing chromium (III) octoate showed high conversions at $71^{\circ}C$ for 40 hr, even if a dipropylene glycol (DPG) was not used as a polymerization initiator. Also, DPG leads to a poor epoxy network structure. In conclusion, the appropriate weight ratio of Part A/Part B of highly silica filled epoxy/anhydride compounds with chromium (III) octoate catalyst is 0.5/1.0 and the maximum amounts of silica is 1470 phr of epoxy resin.

• Restorative Dentistry and Endodontics
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• v.22 no.2
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• pp.739-750
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• 1997

Treatment of root perforation elicits special considerations due to its blood-contaminated circumstances. It is known that conventional dental restorative materials are all leaking. Calcium sulfate is the material which react with water to become chemically set. This study, therefore, was performed to develop a new compound containing calcium sulfate and to evaluate its physical and biological characteristics. Three materials were used, IRM, calcium sulfate, calcium sulfate-hydroxyapatite compound. The composition of the calcium sulfate-hydroxyapatite compound was basically 50 % of calcium sulfate and 50 % of hydroxyapatite mixed with guajacol. The materials were mixed in conventional way and underwent four physical test procedures, setting time, solubility test, compressive strength, and marginal leakage test. All materials were evaluated under the scanning electron microscope to examine the marginal sealing ability. Animal experiment was also performed to test the materials' tissue response. Twenty-four dog's premolars were tested with either furcation perforations or apical retro-fillings. From the results, we found that calcium sulfate possess the good marginal sealing ability. However, calcium sulfate creates many voids which is caused by crystal thrusting action when it reacts with water. It seemed that the voids caused disintegration of the material which eventually lead to tissue reaction. By compounding calcium sulfate and hydroxyapatite, we were able to obtain the better physical properties but it showed larger marginal gap between the material and the root surface. Within the six weeks observation period, both IRM and calcium sulfate-hydroxyapatite compound showed good tissue responses in animal experiment. It is concluded that calcium sulfate would be the material of choice in root perforation repair, but the physical property needs to be further improved.

• Korean Journal of Materials Research
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• v.24 no.2
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• pp.111-115
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• 2014

Titanium and its alloys are useful for implant materials. In this study, porous Ti-Nb-Zr biomaterials were successfully synthesized by powder metallurgy using a $NH_4HCO_3$ as space holder and $TiH_2$ as foaming agent. Consolidation of powder was accomplished by spark plasma sintering process(SPS) at $850^{\circ}C$ under 30 MPa condition. The effect of high energy milling time on pore size and distribution in Ti-Nb-Zr alloys with space holder($NH_4HCO_3$) was investigated by optical microscope(OM), scanning electron microscope(SEM) & energy dispersive spectroscopy(EDS) and X-ray diffraction(XRD). Microstructure observation revealed that, a lot of pores were uniformly distributed in the Ti-Nb-Zr alloys as size of about $30-100{\mu}m$ using mixed powder and milled powders. In addition, the pore ratio was found to be about 5-20% by image analysis, using an image analyzer(Image Pro Plus). Furthermore, the physical properties of specimens were improved with increasing milling time as results of hardness, relative density, compressive strength and Young's modulus. Particularly Young's modulus of the sintered alloy using 4h milled powder reached 52 GPa which is similar to bone elastic modulus.

• Magazine of the Korean Society of Agricultural Engineers
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• v.38 no.6
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• pp.83-95
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• 1996

The normal cement concrete is widely used material to build the construction recently, but it has a fault to increase the dead load on account of its unit weight is large compared with strength. So, main purpose of this study was to establish the physical and mechanical properties of lightweight concrete using expanded polystyrene bead on fine aggregate and natural gravel, expanded clay and pumice stone on coarse aggregate. The test rusults of this study are summarized as follows; 1. The water-cement ratio of concrete using pumice stone was larger than that of the concrete using natural gravel and expanded clay. 2. The unit weights of concrete using pumice stone and expanded caly were shown less than 1,000g/$m^3$. 3. The compressive strengths of all types were shown less than 60kg/$cm^2$, tensile and bending strengths were shown less than l3kg/$cm^2$ and 3lkg/$cm^2$$^2$, respectively. 4. The pulse velocity of concrete was shown similar with using natural gravel and pumice stone, and shown the lowest using pumice stone. 5. The dynamic modulus of elasticity of concrete was shown considerably smaller, and shown the lowest using pumice stone. 6. The static modulus of elasticity of concrete using expanded clay and pumice stone were shown considerably smaller, and shown 22% ~29% as compared with the dynamic modulus of elasticity. 7. The stress-strain curves of concrete were shown similar, generally. And the curves were repeated at short intervals increase and decreased irregularly.

• Journal of Biomedical Engineering Research
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• v.34 no.1
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• pp.14-23
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• 2013

In this study, biomechanical stability of the newly developed revision total knee arthroplasty (rTKA) was evaluated through strain and stress distribution analysis within the implanted proximal tibia using a three-dimensional finite element (FE) analysis. 2000N of compressive load (about 3 times body weight) was applied to the condyle surface on spacer, sharing by the medial (60%) and lateral (40%) condyles simulating a stance phase before toe-off. The results showed that PVMS within the revision total knee arthroplasty and the proximal tibia were less than yield strength considering safe factor 4.0 (rTKA: less than 10%, Cortical bone: less than 70%, Cancellous bone: less than 70%). The materials composed of them and the strain and stress distributions within the proximal tibia were generally well matched with those of a traditional revision total knee arthoplasty (Scorpio TS revision system, Stryker Corp., Michigan, USA) without the critical damage strain and stress, which may reduce the capacity for bone remodeling, leading to bone degeneration. This study may be useful to design parameter improvement of the revision total knee arthoplasty in biomechanical stability point of view beyond structural stability of revision total knee arthoplasty itself.

• Journal of Korean Society of Environmental Engineers
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• v.28 no.3
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• pp.265-269
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• 2006

This study was to investigate the effect of acidic leachate on the landfill liner system and healing of cracks by using industrial by-products; BFS(Blast Furnace Slag) and FA(Fly Ash). From the results of pH measurement, for OPC(Ordinary Portland Cement) and DM(Dredged Mud) mixtures immersed acidic leachate, the initial pH($4.5{\sim}5.5$) was heavily increased to approximately 10 after 60 days experiment due to the production of 2 mole $OH^-$ which was occurred by hydrolysis of CaO and MgO etc.. Meanwhile, the initial pH of acidic leachate immersed DM mixtures with BFS and FA respectively was lasted for longer period as compared to the comparison. The reason was that production of low Ca C-S-H hydrates which stabilized in acidic liquid. The physical properties(compressive strength, hydraulic conductivity) of DM mixtures added BFS and FA was improved. It was concluded that the dissolution of hydrates was disturbed by high alkalinity of BFS and FA.

• Environmental Engineering Research
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• v.21 no.1
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• pp.15-21
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• 2016

Magnesium potassium phosphate cement (MKPC) is an effective agent for solidification/stabilization (S/S) technology. To further explore the mechanism of the S/S by MKPC, two kinds of Cd including $Cd(NO_3)_2$ solution (L-Cd) and municipal solid waste incineration fly ash (MSWI FA) adsorbed Cd (S-Cd), were used to compare the effects of the form of heavy metal on S/S. The results showed that all the MKPC pastes had a high unconfined compressive strength (UCS) above 11 MPa. For L-Cd pastes, Cd leaching concentration increased with the increase of Cd content, and decreased with the increase of curing time. With the percentage of MSWI FA below 20%, S-Cd pastes exhibited similar Cd leaching concentrations as those of L-Cd pastes, while when the content of MSWI FA come up to 30%, the Cd leaching concentration increased significantly. To meet the standard GB5085.3-2007, the highest addition of S-Cd was 30% MSWI FA (6% Cd contained), with the Cd leaching concentration of 0.817 mg/L. The S/S of L-Cd is mainly due to chemical fixation, and the hydration compound of Cd was $NaCdPO_4$, while the S/S of S-Cd is due to physical encapsulation, which is dependent on the pore/crack size and porosity of the MKPC pastes.