• Title/Summary/Keyword: compaction temperature

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Densification Behavior of Fe-Ni Alloy Nanoparticles

  • Kim, Sang-Phil;Lee, Woo-Seok;Lee, Jae-Wook;Choi, Chul-Jin
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2006.09a
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    • pp.531-532
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    • 2006
  • The effects of compaction pressure and sintering temperature on the densification of Fe-40wt%Ni alloy nanoparticles were analyzed. The Fe-Ni nanoparticles were fabricated by an arc-discharge method and then, compacted at three different pressures and sintered at 550 to $900\;^{\circ}C$. Densification was completed at temperature as low as $600\;^{\circ}C$ and high-pressure compaction was found to enhance densification. Densification behaviors and microstructure developments have been investigated through density measurements, electron microscopies, and hardness measurements.

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Micro Fabrication Process of Powder Compact with Semi-solid Mold

  • Tsumori, Fujio
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2006.09a
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    • pp.258-259
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    • 2006
  • New powder compaction process, in which a Bingham semi-solid/fluid mold is utilized, is developed to fabricate micro parts. In the present process, a powder material is filled as slurry in a solid wax mold, dried and compressed. The wax is heated during compaction and becomes semi-solid state, which can acts as a pressurized medium for isostatic compaction. Since the compacted micro parts are very fragile, the mold's temperature is controlled to higher than its melting point during unloading, to avoid breakage of the compacts. To demonstrate effectiveness of this process, some micro compacts of alumina are shown as examples.

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Magnetic Pulsed Compaction of nanostructured Al-Fe-Cr-Ti Powder and wear properties (Al-Fe-Cr-Ti 나노결정 합금분말의 자기펄스 성형 및 마모 특성)

  • Kim, Jun-Ho;Hong, Soon-Jik
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 2008.05a
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    • pp.528-530
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    • 2008
  • The effect of consolidation temperature on the microstructure, density and mechanical properties (especially, wear property) of $Al_{92.5}-Fe_{2.5}-Cr_{2.5}-Ti_{2.5}$ alloy fabricated by gas atomization and magnetic pulsed compaction was investigated. All consolidated alloys consisted of homogeneously distributed fine-grained fcc-Al matrix and intermetallic compounds. Relative higher mechanical properties in the MPCed specimen were attributed to the retention of the nanostructure in consolidated bulk without cracks. The as consolidated bulk by magnetic pulsed compaction showed the enhanced wear properties than that of a general consolidation process. In addition, the wear mechanism and fracture mode of MPCed bulk was discussed.

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Theoretical Development of Compaction Density (다짐밀도의 이론적 전개)

  • Huh, Jung-Do;Kim, Han-Yong;Nam, Young-Kug
    • International Journal of Highway Engineering
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    • v.2 no.1
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    • pp.147-156
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    • 2000
  • Compaction is known to critically affect pavement performance. Due to its importance, a theoretical modelling of compacted density in the term of number of roller coverages is attempted by assuming compaction process essentially identical to pavement rutting. Excellent data fittings by the developed equation may prove the validation of assumptions made as well as justification of its use. According to the derived equation, a plot of density difference with respect to number of roller coverages in the logarithmic scale Produces a linear relationship. However, this linearity is turned out to be deviated by cooling effect, change of amplitude and frequency. Investigation of these three factors proposes a new generalized compaction density equation, which shows a promising future. By applying this general formula, the equations for the number of roller coverages required and the final compaction density obtained for a particular compaction project is derived first time in compaction research.

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Study of Hydrolysis of Al Powder and Compaction of Nano Alumina by Spark Plasma Sintering(SPS) (Al 분말의 수화 반응과 스파크 플라즈마 열처리법으로 제조된 알루미나 성형체 연구)

  • Uhm Y. R.;Lee M. K.;Rhee C. K.
    • Journal of Powder Materials
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    • v.12 no.6 s.53
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    • pp.422-427
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    • 2005
  • The $Al_2O_3$ with various phases were prepared by simple ex-situ hydrolysis and spark plasma sintering (SPS) process of Al powder. The nano bayerite $(\beta-Al(OH)_3)$ phase was derived by hydrolysis of commercial powder of Al with micrometer size, whereas the bohemite (AlO(OH)) phase was obtained by hydrolysis of nano Al powder synthesized by pulsed wire evaporation (PWE) method. Compaction as well as dehydration of both nano bayerite and bohemite was carried out simultaneously by SPS method, which is used to fabricate dense powder compacts with a rapid heating rate of $100^{\circ}C$ per min. under the pressure of 50MPa. After compaction treatment in the temperature ranges from $100^{\circ}C\;to\; 1100^{\circ}C$, the bayerite and bohemite phases change into various alumina phases depending on the compaction temperatures. The bayerite shows phase transition of $Al(OH)_3{\to}{\eta}-Al_2O_3{\to}{\theta}-Al_2O_3{\to}\alpha-Al_2O_3$ sequences. On the other hand, the bohemite experiences the phase transition from AlO(OH) to ${\gamma}-Al_2O_3\;at\;350^{\circ}C.$ It shows AlO(OH) ${\gamma}-Al_2O_3{\to}{\delta}-Al_2O_3{\to}{\alpha}-Al_2O_3$ sequences. The ${\gamma}-Al_2O_3$ compacted at $550^{\circ}C$ shows a high surface area $(138m^2/g)$.

Warm Compaction of Fe-Si/Fe Powder Mixture and its Magnetic Property (Fe-Si/Fe 혼합분말의 온간성형 및 자성특성)

  • Kim, Se-Hoon;Suk, Myung-Jin;Kim, Young-Do
    • Journal of Powder Materials
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    • v.16 no.4
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    • pp.249-253
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    • 2009
  • 3-D shape soft magnetic composite parts can be formed by general compaction method of powder metallurgy. In this study, the results on the high density nanostructured Fe-Si/Fe composite prepared by a warm compaction method were presented. Ball-milled Fe-25 wt.%Si powder, pure Fe powder and Si-polymer were mixed and then the powder mixture was compacted at various temperatures and pressures. Pore free density of samples up to 95% theoretical value has been obtained. The warm compacted sample prepared at 650 MPa and 240$^{\circ}C$ had highest compaction properties in comparison with other compacts prepared at 300, 400 MPa and room temperature and 120$^{\circ}C$. The magnetic properties such as core loss, magnetization saturation and coercivity were measured by B-H curve analyzer and vibration sample magnetometer.

Soil Characteristic of Plow and Compaction Layer in Fluvio-marine Deposit Paddy Soil (하해혼성 충적층 논토양 작토층과 경반층의 토양특성)

  • Yang, Chang-Hyu;Kim, Taek-Kyum;Ryu, Jin-Hee;Kim, Jae-Duk;Jung, Kwang-Yong
    • Korean Journal of Soil Science and Fertilizer
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    • v.42 no.5
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    • pp.364-370
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    • 2009
  • This study was conducted to survey, analyze on the compaction layer and the plow layer at Jeonbug and Jisan series paddy soil, which is the representative soil in fluvio-marine and local alluvium, respectively. The depths of surface soil were 12.6 and 12.7 cm in Jeonbug and Jisan series, respectively. A plowing depth was 10.5 cm. The properties of compaction layer in two soil series were as follows. The hardness were $14.7kg\;cm^{-2}(25.3mm)$ and $8.7kg\;cm^{-2}(22.1mm)$ in Jeonbug and Jisan series, respectively. The thickness were 22.3 cm and 17.8 cm in Jeonbug and Jisan series, respectively. The depth of soil compaction, which means depth from surface, were 15 and 20 cm in Jeonbug and Jisan series, respectively. The relationship between the hardness of compaction layer and the depth of surface soil showed negative correlation, however relationship between the hardness and the thickness of compaction layer showed positive correlation. Soil temperature was lower in compaction layer than in plow layer. This temperature differences between compaction layer and plow layer were from 1.0 to $2.5^{\circ}C$ in Jeonbug series and from 0.7 to 2.1 in Jisan series. The soil physical properties of compaction layer were higher in bulk density and solid phase and lower in porosity and gaseous phase than those of plow layer in all soil series. The soil chemical properties of compaction layer were higher in pH, content of available silicate, exchangeable calcium and magnesium but lower in total nitrogen, content of organic matter and available phosphate than those of plow layer in all soil series. Cation exchangeable capacity and content of exchangeable potassium were similar between compaction layer and plow layer in Jeonbug series, however, in Jisan series these were lower in compaction layer than in plow layer. Elution amount of inorganic nitrogen were lower in compaction layer than in plow layer in all soil series. The content of soluble Fe and Mn were plenty in compaction layer compared with plow layer and these tendency was apparent in Jeonbug series. The water depth decrease were fast until the latter part of June, and were slow as $1{\sim}3mm\;day^{-1}$ for July and August, and were fast again from september. Rice roots distributions as each soil series and tillage method were 25 cm at rotary plowing in Jeonbug series, 30 cm at deep plowing in Jeonbug series, and 20 cm at tillage in Jisan series. Dry weight per m2 at heading stage were much in order of deep plowing in Jeonbug series, rotary plowing in Jeonbug series, and tillage in Jisan series.

Effect of Carbon Addition and Sintering Temperature on Densification and Microstructural Evolution of Sinter-Hardening Alloys Steels

  • Verma, N.;Anand, S.;Upadhyaya, A.
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2006.09a
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    • pp.557-558
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    • 2006
  • In all conventional sintered PM products, the pores present are of two types, primary and secondary. Primary pores forming during compaction and latter during sintering, due to penetration of formed liquid through the matrix grain boundary. Effect of carbon addition on diffusion of Cu in SH737-2Cu system was investigated. After compaction and transient liquid phase sintering at $1120^{\circ}C$ and $1180^{\circ}C$, samples were characterized for densification, showing rise in sintering density and reduction in swelling on carbon addition. Quantitative microstructural characterization (shape factor and pore size) revealed bimodal distribution for 0% carbon, more rounded pores for 0.9% carbon and higher sintering temperature, and pore coarsening at higher sintering temperature.

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Temperature Effects on the Compaction and Compressive Strength of Soils (온도변화가 흙의 다짐과 압축강도에 미치는 영향)

  • 김재영
    • Magazine of the Korean Society of Agricultural Engineers
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    • v.15 no.4
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    • pp.3137-3146
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    • 1973
  • This study was to investigate the effects of compaction, compressive strength and Atterberg limits in accordance with the temperatures changes. It was conducted on four soils-KJ, JJ, MH, SS-at temperatures of -1, 1, 3, 5, 7, 10, 15, 19, $22^{\circ}C$. These tests were obtained the maximum dry density and the optimum moisture content of four soils in accordance with temperature changes by using distilled water and $CaCl_2$ 10% solution, and were put to the compressive strength tests on remolded specimens of soils compacted at the optimum moisture content. The result of the study can be summarized as follows; The maximum dry density increased with an increase in temperature, and the use of $CaCl_2$ 10% solution had higher maximum dry density than distilled water. The optimum moisture content decreased with an increase in temperature, and the use of $CaCl_2$ 10% solution had lower optimum moisture content than distilled water. The maximum compressive strength was shown high peak from $7^{\circ}C\;to\;15^{\circ}C$, and the use of $CaCl_2$ 10% solution had higher maximum compressive strength than distilled water. The liquid limit and plasticity index decreased with an increased in temperature. It is estimated that the use of $CaCl_2$ 10% solution can lower the minimum compacted temperature from $2^{\circ}C\;to\;4^{\circ}C$ in low temperature.

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