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Mixed Lanthanide Shift Reagents (혼합 란탄족 Shift Reagents)

  • Man-Ho Lee;Charles N. Reilley
    • Journal of the Korean Chemical Society
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    • v.26 no.1
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    • pp.24-30
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    • 1982
  • Contact-only (COM) and dipolar-only (DOM) mixtures of the lanthanide shift reagents were prepared based on the Fi and Gi values deduced using individual Ln$(fod)_3$ (Ln = Pr, Nd, Eu, and Yb) and 4-picoline. The $F_i$ and $G_i$ values obtained directly by COM 1 and by DOM 1, which were appropriate mixture of Pr$(fod)_3$ and Eu$(fod)_3$, agreed well with those values obtained by experiments using individual Ln$(fod)_3$ shift reagents. Ei and Gi values obtained directly by COM 2 and by DOM 2, which were mixtures of Nd$(fod)_3$ and Yb$(fod)_3$, deviated from the expected values. The error was traced to the behavior of the ytterbium complexes.

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Effect of Organic Fertilizer as Bio-com Application on the Changes of Soil Microorganisms, Gas Evolution, and Mineral-N Transformation in Submerged Condition (유기질비료(有機質肥料) Bio-com 시용(施用)이 토양(土壤)의 미생물상(微生物相) 및 화학성(化學性)에 미치는 영향(影響))

  • Kim, Jeong-Je;Lee, Sang-Kyu
    • Korean Journal of Soil Science and Fertilizer
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    • v.20 no.4
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    • pp.351-357
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    • 1987
  • A laboratory experiment was conducted to find out the effect of organic fertilizer as Bio-com$^{(R)}$ on the changes of pH and Eh values, gas evolution, ammonification and nitrification, and microbial population with farmer's compost and refused mushroom compost in submerged paddy condition. The results obtained are summarized as follows: 1. Application of compost and refused mushroom compost was increased the pH values than that of NPK alone. Organic fertilizer of Bio-com$^{(R)}$ showed the same results of the farmer's compost or refused mushroom compost. 2. Population of soil microbes as bacteria, actinomycetes and fungi was increased by application of compost, refused mushroom compost and Bio-com$^{(R)}$. Moreover, the results were pronounced more with the addition of NPK. 3. The application of Bio-com$^{(R)}$ was effected to the increase of the amount of $NO_3-N$ and the rate of nitrification than NPK, farmer's compost or refused mushroom compost. 4. The amounts of evolved gases as $CH_4$, $CO_2$, and $N_2O$ were not much differed with application of kinds of compost and NPK, but little increasing tendency was observed in application of NPK than that of NPK+kinds of compost.

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Validation of Analytical Methods for Unriped Rubus crataegifolius, Gardenia jasminoides and Ulmus macrocarpa Marker Compounds for Standardization of Natural Complex LS-RUG-com Preparation as Functional Ingredient (천연복합소재 LS-RUG-com의 기능성원료 표준화를 위한 산딸기 미숙과, 치자 및 유백피 지표성분의 분석법 검증)

  • Young Ik Lee;Su Jin Pyo;Hee Jin Lee;Hye Jung Yoon;Ho Yong Sohn;Jin Sook Cho
    • Journal of Life Science
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    • v.34 no.1
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    • pp.59-67
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    • 2024
  • LS-RUG-com preparation in a complex extract from mixture of three natural plants. Rubus crataegifolius/unriped, Gardenia jasminoides and Ulmus marcrocarpa that have been widely used in traditional functional health food. This study was conducted to establish the HPLC analysis methods that can be used to establish quantitative analysis of R. crataegifolius, G. jasminoides and U. macrocarpa for standardization of LS-RUG-com preparations. HPLC analysis methods for simultaneous determination of ellagic acid and geniposide and single determination of catechin-7-O-β-D-apiofuranoside were established for the quality control of natural plants complex (LS-RUG-com). Validation of HPLC analysis were performed by checking specificity, accuracy, precision, limit of detection and quantitation, and linearity following ICH (International Council for Harmonisation) guideline. As the result of quantitative analysis, the contents of ellagic acid, geniposide and catechin-7-O-β-D-apiofuranoside in each plant extracts were 11.2 mg/g (ellagic acid) and 72 mg/g (geniposide) and 10.2 mg/g (catechin-7-O-β-D-apiofuranoside). The contents of ellagic acid, geniposide and catechin-7-O-β-D-apiofuranoside in LS-RUG-com were 4.62~6.82 mg/g (ellagic acid), 19.2~28.8 mg/g (geniposide) and 1.36~2.04 mg/g (catechin-7-O-β-D-apiofuranoside) respectively.

Website Homepage Design and Service Design of USATODAY.com Analysis (유에스에이투데이닷컴의 웹사이트 홈페이지디자인과 서비스디자인 분석)

  • Han, Qing-Bo;Kim, Eun-Ju;Lee, Ji-Hyun
    • Journal of Digital Convergence
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    • v.14 no.10
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    • pp.423-430
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    • 2016
  • The purpose of this paper is to explore and analyze design of USATODAY.COM aimed at being helpful for Chinese online news industry to search for the way forward. USATODAY.COM which converges print and online newsrooms is regarded as a pioneer in the online communication media. It engages interaction with users and their demand, and provides the best level of website and service design. This paper conducted through both theoretical works and design analyses by randomly visiting USATODAY.COM from May 23 to June 5, 2016. USATODAY.COM maintains consistent and high quality of a visual identity system on its homepage, and it is strongly linked to that of USA TODAY. Also, USATODAY.COM provides unique content provision methods, interactive features, advertisement and payment functions through service design considering the user experiences and needs. Based on its results, it is expected to contribute to Chinese online newspaper market which has an astonishing chance to grow.

Linear Expansion and Durability of a Composite Boards (MDF Laminated Using Three Selected Wood Veneers) against Drywood Termites

  • CAHYONO, Tekat Dwi;YANTI, Hikma;ANISAH, Laela Nur;MASSIJAYA, Muh Yusram;ISWANTO, Apri Heri
    • Journal of the Korean Wood Science and Technology
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    • v.48 no.6
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    • pp.907-916
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    • 2020
  • This research was conducted to investigate the linear expansion and resistance properties of a composite board (com-ply). This board was made of medium-density fiberboard (MDF) laminated using avocado (Persea americana), mahogany (Swietenia mahogani), and pine (Pinus merkusii) veneers. These three types of veneers were laminated on both surfaces of the MDF using adhesives, namely, epoxy and isocyanate. Glue (250 g·m-2) was spread on the surface, followed by cold press for 3 h with an applied pressure of 15 kg·cm-2. The research result revealed that com-ply exhibited an increased dimensional stability compared with MDF, indicated by reduction in water absorption, thickness swelling, and linear expansion. The com-ply made of the pine veneer and isocyanate adhesive exhibited high density, water absorption, thickness swelling, and screw withdrawal load. The com-ply that exhibited the strongest resistance to drywood termite attacks was the one made of the mahogany veneer and isocyanate adhesive. Moreover, the com-ply that exhibited the biggest weight loss (3.6 %) was made of the pine veneer and epoxy adhesive. The results of this research may facilitate in manufacturing com-ply using the selected veneer and adhesive without the application of hot press.

Design Techniques and Development of Mypage when Join the 6005+ Web-site (회원가입과 동시에 경험하게 되는 6005+사이트 Mypage 설계기법 및 개발)

  • Zhao, Mei-Hua;Ko, Hee-Ae;Kim, Jong-Keun;Sim, Kun-Ho;Lim, Young-Hwan
    • Journal of Digital Contents Society
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    • v.11 no.3
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    • pp.407-416
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    • 2010
  • As the mobile internet rapidly progress and mobile terminals are activated, business entities which want to operate mobile web contents and individuals who want to use it increase. 6005plus.com as "I wish the mobile world" which is mobile UCC(User Created Contents) ponpy/invitation service web site(www.6005plus.com) was constructed. In 6005plus.com web site, which users could easily produce mobile contents and establish mobile web service servers as well, in order for mobile service users to create mobile invitation or ponpy and use it. But the service 6005plus.com advocates is that users can attach ponpy and invitations to the MMS/SMS Call back URL, which needs resolution since it has several inactivated problems. In this paper, we allow users who registered 6005plus.com can create mobile card, invitation, and personal ponpy with registration, so that apply automatic generation technique for users to experience ponpy/invitation service into MMS/SMS Call back URL which 6005plus.com advocates through registration. We also designed my page to which users can send their contents easily, conveniently and by one-stop.

PHOTOMETRIC OBSERVATIONS OF THE CONTACT BINARY SYSTEM CC COM (접촉쌍성 CC Com의 측광학적 관측과 분석)

  • Jeong, Jang-Hae;Kim, Chun-Hwey;Kim, Yong-Gi
    • Journal of Astronomy and Space Sciences
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    • v.24 no.2
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    • pp.99-110
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    • 2007
  • A total of 824 observations (206 in ${\Delta}B$, 206 in ${\Delta}V$, 206 in ${\Delta}R$, 206 in ${\Delta}I$ for CC Com were made on 3 nights from March 3 to April 3 in 2002 using the 61cm telescope with 2K CCD camera of the Sobaeksan Optical Astronomy Observatory of KASI. From our observations 9 times of minimum light were newly determined. Combined analysis of our new BVRI light curves with the double-lined radial velocity curves of Pribulla et al. (2007) were made with the 2004 Wilson-Devinney(WD) binary model code to yield new physical parameters of the CC Com system. Small asymmetries in light curves were explained with the adoption of two hot spots on the cool secondary.

The Efficacy of Simultaneous Bilateral Internal Carotid Angiography during Coil Embolization for Anterior Communicating Artery Aneurysms

  • Kwon, Soon-Chan;Park, Jun-Bum;Shin, Shang-Hun;Sim, Hong-Bo;Lyo, In-Uk;Kim, Young
    • Journal of Korean Neurosurgical Society
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    • v.49 no.5
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    • pp.257-261
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    • 2011
  • Objective : Successful coil embolization of anterior communicating (A-com) artery aneurysms requires good visualization and understanding of the entire H complex. Bilateral carotid angiography may optimize anatomical understanding and visualization of the H complex. We therefore assessed the efficacy of simultaneous bilateral internal carotid angiography during coil embolization for A-com artery aneurysms. Methods : Of the 153 patients with intracranial saccular aneurysms who underwent embolization between July 2008 and December 2009, 12 had A-com artery aneurysms and were embolized under bilateral carotid angiography. Patients were evaluated angiographically, immediately and 6 months (n=11) after embolization, using a 3-point scale (complete, residual neck, residual aneurysm). The safety, performance and efficacy of this approach were retrospectively evaluated. Results: In all patients, bilateral internal carotid artery angiography provided more detailed anatomical information and understanding around the A-com artery, and, in complex situations, it allowed for more effective coil embolization through bilateral routes to the A-com artery. Angiography immediately after embolization showed occlusion of 11 of the 12 (92%) aneurysms, with none of these 11 showing evidence of recanalization at 6 months. Conclusion : These findings indicate that simultaneous bilateral carotid angiography during coil embolization of selected complex A-com artery aneurysms provided improved anatomical understanding, and resulted in more effective and safer procedures than typical unilateral angiography.

Evaluation of Organic Sudangrass for Feed Value, Silage Quality and Palatability in Korea (유기 수단그라스의 사료가치, 사일리지 품질 및 기호성 평가)

  • Kim, Jong-Duk;Shim, Keum-Seob;Joo, Jong-Cheol;Lee, Hyun-Jiun;Jeon, Gyeong-Hyeop;Youn, Young-You;Oh, Eung-Yong;Lee, Hyo-Won
    • Korean Journal of Organic Agriculture
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    • v.19 no.spc
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    • pp.144-147
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    • 2011
  • The main nutritional problem of sorghum${\times}$sudangrass hybrid (Sorghum bicolor${\times}$Sorghum sudanese) silage is low quality and palatability. This experiment was conducted to evaluate whether organic com grain and crushed rice addition of sorghum${\times}$sudangrass hybrid silage increases forage quality of the silage. The sorghum${\times}$sudangrass hybrid silages with added com grain and crushed rice were similar to conventional com silage in moisture content. However organic sorghum${\times}$sudangrass hybrid silage had low pH values. Silage added with gain and byproduct had higher crude ash, acid detergent fiber (ADF) and neutral detergent fiber (NDF) contents than control com silages, while its non-fiber carbohydrate (NFC) and total digestible nutrients (TDN) showed the opposite results. Lactic acid, butyric acid and lactic percentage of total organic acid (L/T) of sorghum${\times}$sudangrass hybrid silages were higher than those of com silage, but acetic acid was higher than control. In vitro dry matter digestibility (IVDMD) of com silage was higher than other sorghum silages. Feed intake of sorghum${\times}$sudangrass hybrid silage added with crushed rice was highest among silages. Therefore, these data indicate that crushed rice and com grain added sorghum${\times}$sudangrass hybrid silage could be recommended as the most effective treatment for increasing silage quality and palatability.