• Textile Coloration and Finishing
• /
• v.25 no.4
• /
• pp.327-336
• /
• 2013

The purpose of this study was to evaluate the color image of the natural-dyed silk fabrics. The dye was extracted from pine needle by boiling pine needle with ethanol at $78^{\circ}C$ for 3hours and distilled water at $100^{\circ}C$ for 2hours. The 100% silk fabric was dyed of extract in pH 5 at $90-100^{\circ}C$ for 1 hr. As mordants used were compounds of Al, Sn, Fe, and Cr, color image of pine-needle dyed silk fabrics was classified into 5 factors (pure, gentle, sophisticate, comfortable, pastorale) and the factor pure is most important one of those. Most cheerful image in pure factor was from the fabrics dyed with ethanol extract and then, none and Cr mordanting. Dignified image was from the fabrics dyed with ethanol extract and then, Cu or Fe mordanting. In production, products dyed with ethanol extracts was preferred to those dyed with distilled water extracts. Color image and preference of the silk fabrics dyed with pine needles extracted was affected by extraction solvents and mordants.

• Journal of the Korean Society of Clothing and Textiles
• /
• v.28 no.7
• /
• pp.882-891
• /
• 2004

The purpose of this study was to improve dye effect and method in order to facilitate the use of persimmon juice dyeing. Silk fabrics were pad-dyed to 100% pick-up using padding machine after dipping in persimmon juice extracted from unripe persimmons indigenous to Jeju. The color of dyed silk fabrics by padding method was more even and repeatable than that by traditional hand method. Persimmon juice concentrations were 4 types 10, 25, 50 and 100%. The silk fabrics were pad-dyed to 100% pick-up and were repeatedly dyed two times and three times with 100% concentration. The higher the concentration, the more color deepened. UV Irradiation instead of sunlight was applied to color developing. Irradiation times were shortened to 1-8hrs. Color values which reguired 30-50 hrs. in sunlight irradiation. were obtained in 3-5 hrs. with UV irradiation. Tensile strengths of silk fabrics in UV irradiation decreased but not decreased in sunlight irradiation. Elongations of silk fabrics in sunlight irradiation increased but decreased in W irradiation. Drape stiffness increased up to three times.

• Fashion & Textile Research Journal
• /
• v.3 no.1
• /
• pp.35-41
• /
• 2001

Dyeing properties of silk fabric with onion shell were studied by investigating the effect of dyeing conditions, such as concentration of onion shell, dyeing temperature, dyeing time and pH, on dye uptakes. And also the effects of mordants and mordanting methods or color change and dye uptakes were investigated. For the practical use, the various color fastness of dyed and mordanted fabric were evaluated. The color fastness was improved when Fe mordant was added.

• The Research Journal of the Costume Culture
• /
• v.20 no.2
• /
• pp.238-250
• /
• 2012

This study examined the degradation behavior of SB(standard berberine) dye and SB dyed silk using HPLC-MS instrument after degradation in the hydrogen peroxide/ultraviolet ray radiation/oxygen system up to 9 days and 40 hours respectively. In the degraded samples, berberine was detected at 5.2 min in the SB dye and 5.3 min in the SB dyed silk with its molecular ion=336 and the UV spectra of quaternary alkaloid. Degradation product 3(m/z=102) newly appeared after 5 day degradation treatment with continued increase till the end of degradation treatment. The amount of berberine in the degraded dye decreased with degradation progression. In the silk dyeings, berberine was detected only up to 21 hour degradation sample. The amount of berberine decreased dramatically during the first 6 hours of degradation treatment. The CIELAB color measurement of the silk dyeings showed dramatic change in the b* value, near zero in the 40 hour degraded silk. CIELAB and Munsell color measurements were in agreement with the HPLC-MS results of the dyed silk in the change of berberine content that the degraded silk became white and lost yellow color.

• Journal of the Korean Society of Clothing and Textiles
• /
• v.41 no.5
• /
• pp.914-928
• /
• 2017

This research investigated the effect of pH of dyebath and dyeing temperature on the dyeability of indigotin and indirubin on silk as well as the relationship between the amount of indigotin and indirubin detected from the dyed silk through HPLC-DAD analysis and the color of samples measured using a spectro-colorimeter. Indigo standard dye and indirubin standard dye were deliberately mixed by ratios 100:0, 80:20, 60:40, 40:60, 20:80, and 0:100 to dye silk with a different pH of dyebath (7, 11) and different dyeing temperatures ($50^{\circ}C$, $70^{\circ}C$). The amount of indigotin and indirubin pigments in silk was calculated using regression equations obtained from standard calibration curves of indigotin and indirubin. A higher indigotin percent ratio resulted in the higher K/S values and the higher amount of indigotin detected from silk. However, higher indirubin percent ratio in the mixed dye did not relate to the higher indirubin pigment detected in silk. While indirubin showed low or negative contribution to the K/S values, it showed a higher effect on the color of dyed silk. Higher amounts of indirubin in dyed silk resulted in a darker PB color, which led to P color with increases in indirubin content.

• Textile Coloration and Finishing
• /
• v.22 no.4
• /
• pp.306-313
• /
• 2010

To achieve color diversification of natural dyeing, color mixture dyeing with Indigo and Japanese pagoda tree is applied to wool and silk fabrics. After dyeing with Japanese pagoda tree extract solution of 5~25%(o.w.f.), the indigo dyeing was carried out up to four times. Alternatively after repeat dyeing with indigo one to seven times, the dyeing with Japanese pagoda tree extract solution was applied in 5 steps(5~25%). In color mixture dyeing, the dye uptake of wool fabrics appears higher than that of silk. The sequence of Japanese pagoda tree extract dyeing after Indigo dyeing was generally higher dye uptake compared with that of Indigo dyeing after Japanese pagoda tree extract dyeing. For wool and silk fabric, the pre-dyeing with Japanese pagoda tree solution was more effective for color diversification but the pre-dyeing with Indigo was more effective for the exhibition of intermediate color shade.

• Korean Journal of Human Ecology
• /
• v.7 no.1
• /
• pp.43-50
• /
• 2004

The purpose of this study is to reach silk protein added in differing amounts to Jeolpyon, Korean traditional rice cake, using rice powder as its primary material, estimation of the micro organism quality, physicochemical property, sensory evaluation and the property of storage period (20${pm} 5 ^{\circ}C$). In the physicochemical property, the content of proximate composition of rice powder was measured as 38.11% of moisture, 56.62% of total sugar, 5.11% of crude protein, 0.52% of crude lipid, 0.25% of ash. And the raw material of silk protein was measured as 6.61% of moisture, 91.22% of crude protein, 6.41% of crude lipid and 0.75% of ash. The pH of raw material for rice powder and silk protein Jeolpyon showed mild acidity as 6.41 and 6.23, respectively. In rice powder and silk protein, total free sugar contents was 0.89% and 0.02%, and total amino acids contents was 4.28% and 52.21 %, respectively. For sensory evaluation. color, taste, softness and adhesiveness were significantly acceptable in control and adding 1 % silk protein. Control and samples added 1$\sim$3% silk protein had high sensory score color in overall acceptance. In conclusion. Jeolpyon can be manufactured with nutritious Jeolpyon by adding silk protein.

• Science of Emotion and Sensibility
• /
• v.13 no.2
• /
• pp.403-412
• /
• 2010

This study was aimed to consider the influence of hue-tone, dyes, and mordants of naturally dyed silk fabric on color sensibility image factors and to establish color sensibility image scales of naturally dyed silk fabric by color and image descriptors. By single or sequential dyeing with various natural dyes commercially available in domestic and foreign market on the same silk fabric, a total of 66 colored fabric stimuli were prepared and they were used to evaluate subjective color sensibility image by 40 participants. As results, four different color sensibility image factors for naturally dyed silk fabric, 'delight', 'natural', 'modern' and 'attractive' were extracted. All of factors were significantly influenced by hue-tone, dyes, and mordants. Furthermore, by using color sensibility image adjectives and colors, multidimensional image scales were established, which leads to the conclusions that the results of this study help to design color sensibility-oriented naturally dyed fabric and apparel products.

• Journal of Sericultural and Entomological Science
• /
• v.38 no.2
• /
• pp.168-174
• /
• 1996

Dyeing on silk with vat dyes which shows good color fastness at strong alkaline conditions were newly examined. The optimum conditions of dyeing bath to prevent the damage on the tensile strength and elongation were sodium hydroxide(NaOH) 10g/l, sodium hydrosulfite(Na2S2O4) 20~22 g/l, for 30 min at 5$0^{\circ}C$. The color yield of silk fabrics was increase according to the concentration of NaOH and Na2S2O4, but decreased at higher concentration than that of NaOH 10g/l and Na2S2O4 22g/l. The vat dyeings showed excellent color fastness against washing and light, compared with the conventional dyeings.

• The Korean Journal of Community Living Science
• /
• v.14 no.2
• /
• pp.125-130
• /
• 2003

To develop natural dyeing materials from the unused plant materials, we had several dyeing experiments to investigate the optimum conditions of dyeing fabrics with the dyebath extracted from wisteria. Dyeing experiments were done under different dyeing conditions of dyeing temperature, pH of dyebath, dyeing time, concentration of dyebath and mordant treatment which were treated after dyeing. Experimental fabrics were silk, wool, cotton, ramie and hemp. Color difference(ΔE) and Munsell's HV/C of the dyed fabrics and color fastness of silk and cotton fabrics to dry cleaning, washing, rubbing, perspiration and light were measured. In silk and wool fabrics(non mordant, dyeing time-20min), color differences increased in case of dyeing temperature of $100^{\circ}C$, but in cotton, ramie and hemp fabrics, color differences did not increase. Without mordant treatment, color differences of all experimental fabrics were about 10-20, so in wisteria dyeing mordant treatment was necessary. Color differences were increased by the mordant treatment; the color of dyed fabrics with Al mordant is dull yellow, Cu mordant is gold and Fe mordant is olive tone. Color difference was not affected by pH of dyebath in all experimental fabrics. On the whole, the color fastness of dyed silk and cotton fabrics were good, but color fastness to washing and perspiration in Fe mordant was weak and improved in Cu mordant.