• Transactions of the Korean Society of Mechanical Engineers
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• v.19 no.4
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• pp.929-940
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• 1995

The fatigue strength and fracture topography in the friction welded interface of high speed steel (HSS-Co) to SM55C carbon steel have been investigated through the fatigue test, SEM fractograph and EDS (energy dispersive spectrometer) analysis. Three kinds of specimens used in this research are the friction welded joints, HSS-Co and SM55C carbon steel with circumferential notch, saw notch and smooth, respectively. The notch sensitivity factor, .eta. of the friction welded joints is lower than that of the base materials, and that represents a superiority of the joint performance of FRW. Fracture topography of the FRW specimens with a notch showed a cleavage or brittle appearance, while that of the FRW smooth specimen appeared to be ductile. Furthermore, although fatigue crack likely initiated near the weld interface of the FRW smooth specimen, crack propagation continued into the HAZ of SM55C steel. Finally, fatigue fractures of the base materials were associated primarily with the inclusions located at the outer periphery of the specimen.

• Journal of Welding and Joining
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• v.15 no.6
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• pp.57-65
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• 1997

A study was undertaken to determine the influence of welding variables such as shielding and plasma gases, torch standoff, travel speed and heat input, etc. on the quality of plasma arc welds in Zircaloy-4 sheet, 2mm thick. Effect of shielding gases and their flow rates on the mechanical properties of Zircaloy-4 welds by plasma arc welding were determined in terms of tensile, bardness and bend tests. The microstructure and fracture surface of Zircaloy-4 welds were investigated by optical and scanning electron microscopies. In addition, the causes of porosity and undercut in plasma arc welds of Zircaloy-4 were also investigated. Zircaloy-4 weld bead width and depth by helium shielding gas showed a wider and deeper than those by argon. It was found that Zircaloy-4 welds with shielding gas of helium did dxhibit a little smoother and uniform weld beads than those with shielding gas of argon. It was also found that the optimum gas flow rates for Zircaloy-4 welding were 0.45l/min for plasma gas with Ar and 4.5 - 6 l/min for shielding gas with He. In addition, there was no big difference in the microstructure and fracture surface of the weld metals made by either Ar shielding gas or He shielding gas.

• Transactions of the Korean Society of Mechanical Engineers A
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• v.27 no.9
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• pp.1444-1450
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• 2003

The fatigue life and tensile strength of JLF-1 steel (Fe-9Cr-2W-V-Ta) and its TIG weldment were investigated at the room temperature and $400^{\circ}C$. Four kinds of test specimens, which associated with the rolling direction and the TIG welding direction were machined. The base metal of JLF-1 steel represented almost anisotropy in the tensile properties for the rolling direction. And the base metal of JLF-1 steel showed lower strength than that of TIG weldment. Also, the strength of all materials entirely decreased in accordance with elevating test temperature. Moreover, the fatigue limit of weld metal was largely increase than that of base metal at both temperatures. The fatigue limit of JLF-1 steel decreased in accordance with elevating test temperature. The fatigue limit of JLF-1 steel decreased in accordance with elevating test temperature. The SEM fractography of tensile test specimen showed conspicuous cleavage fracture of a radial shape. In case of fatigue life test specimen, there were so many striations at crack initiation region, and dimple was observed at final fracture region as a ductile fracture mode.

• Journal of Welding and Joining
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• v.7 no.2
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• pp.35-48
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• 1989

This study is concerned with a correlation of microstructure and local brittle zone (LBZ) in offshore structural steel welds. The influence of the LBZ on fracture toughness was investigated by means of simulated heat-affected zone (HAZ) tests as well as welded joint tests. Micromechanical processes involved in void and cleavage microcrack formation were also identified using notched round tensile tests and subsequent SEM observations. The LBZ in the HAZ of a multiphase welded joint is the interstitially reheated coarse grained HAZ, which is influenced by metallurgical factors such as effective grain size, the major matrix structure and the amount of high-carbon martensite-austenite (M-A) constituents. The experimental results indicate that Chirpy energy was found to scale monotonically with the amount of M-A constituents, confirming that the M-A constituent is the major microstructural factor controlling the HAZ toughness. In addition, voids and microcracks are observed to initiate at M-A constituents by the shear cracking process. Thus, the M-A constituent played an important role in initiating the voids and microcracks, and consequently caused brittle fracture.

• Journal of the Korean Society for Heat Treatment
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• v.36 no.1
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• pp.15-21
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• 2023

Recently, ultra-high strength bolts have been developed for weight lightening of a vehicle and fuel efficiency. However, some amount of diffusible H is absorbed into the bolt during its manufacturing process so that H embrittlement (HE) often occurs particularly in high strength bolts with a tempered martensitic microstructure. This brings attention to ultra-high strength pearlitic bolts with a high resistance to HE. Therefore, in this study the HE resistance of the 1.6 GPa grade pearlitic bolt was evaluated through tightening tests and slow strain rate tests (SSRTs), and fracture surfaces of failed bolts were comparatively observed. A critical H content for the tightening test turned out to be ~0.23-0.35 mass ppm. The bolt with a diffusible H content of ~0.35 mass ppm was fractured during the tightening test, showing a quasi-cleavage fracture surface, indicating the occurrence of HE. In addition, the bolt underwent premature elastic failure during the SSRT. This implies that the HE resistance of high strength bolts can be evaluated by both tightening test and SSRT.

• Tunnel and Underground Space
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• v.26 no.4
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• pp.327-337
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• 2016

In this study, laboratory hydraulic fracturing tests are carried out to evaluate the effects of the cleavage anisotropy of Pocheon granite. Breakdown pressure is smaller when cracks are generated to the direction of rift plane in constant pressurization rate condition because of higher microcracks density. Besides not only injection rate changes but also the amount of injection pressure for fracture initiation and crack expansion is detected while testing due to internal deformation. Pressurization rate is higher while hydraulic fracture testing with constant injection rate condition in case of the specimen which has rift plane perpendicular to borehole because there are much flow paths to penetrate compared to the specimen which has hardway plane perpendicular to borehole. Observation by X-ray CT scanning shows that almost all of cracks due to hydraulic fracturing are generated to the direction of plane which has higher microcrack density that is rift plane or grain plane.

• Korean Journal of Materials Research
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• v.30 no.5
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• pp.231-238
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• 2020

The composition of martensite transformation in NiAl alloy is determined using pure nickel and aluminum powder by vacuum hot press powder metallurgy, which is a composition of martensitic transformation, and the characteristics of martensitic transformation and microstructure of sintered NiAl alloys are investigated. The produced sintered alloys are presintered and hot pressed in vacuum; after homogenizing heat treatment at 1,273 K for 86.4 ks, they are water-cooled to produce NiAl sintered alloys having relative density of 99 % or more. As a result of observations of the microstructure of the sintered NiAl alloy specimens quenched in ice water after homogenization treatment at 1,273 K, it is found that specimens of all compositions consisted of two phases and voids. In addition, it is found that martensite transformation did not occur because surface fluctuation shapes did not appear inside the crystal grains with quenching at 1,273 K. As a result of examining the relationship between the density and composition after martensitic transformation of the sintered alloys, the density after transformation is found to have increased by about 1 % compared to before the transformation. As a result of examining the relationship between the hardness (Hv) at room temperature and the composition of the matrix phase and the martensite phase, the hardness of the martensite phase is found to be smaller than that of the matrix phase. As a result of examining the relationship between the temperature at which the shape recovery is completed by heating and the composition, the shape recovery temperature is found to decrease almost linearly as the Al concentration increases, and the gradient is about -160 K/at% Al. After quenching the sintered NiAl alloys of the 37 at%Al into martensite, specimens fractured by three-point bending at room temperature are observed by SEM and, as a result, some grain boundary fractures are observed on the fracture surface, and mainly intergranular cleavage fractures.

• Nuclear Engineering and Technology
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• v.17 no.3
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• pp.211-215
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• 1985

The effects of temperature and strain rate on the I-SCC behaviors of Zircaloy-4 were investigated by constant load test at 30$0^{\circ}C$ and constant elongation rate test at 300, 350 and 40$0^{\circ}C$ in 3.34mg $I_2$/㎤. The results showed that I-SCC susceptibility increased as the strain rate decreased or the temperature increased. The empirical relation between the stress and the time to failure at 30$0^{\circ}C$ was given by 1/ $t_{f}$∝exp (0.3$\sigma$/$\sigma$$_{UTS}$-31.5) When the I-SCC susceptibility was expressed by the ratio of fracture energy in iodine atmosphere to that in the inert atmosphere, severe I-SCC susceptibility was found near 7.6$\times$10$^{-6}$ sec at 30$0^{\circ}C$ and the maximum point of I-SCC susceptibility tended to shift to the higher strain rate with increasing the temperature. The quasi-cleavage fracture was observed in I-SCC fracture surface. From these results, it was certain that the film repture step was involved as an important process in the I-SCC mechanism of Zircaloy-4.4.

• Corrosion Science and Technology
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• v.4 no.5
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• pp.211-216
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• 2005

Failure analysis of the latch ram ball and the C-ram ball with the trade name AFBMA Gr. 50 Colmonoy No. 6, has been performed to identify the root cause of the failure. The study required the extraction of the both failed and normal balls from the nuclear fuel exchanger. Microstructures of both balls were examined after polishing and etching. Breaking tests of both the ball revealed similarity in cleavage surfaces. Fracture surfaces of both failed ball and normal ball after breaking test were examined with SEM and EDX. Microstructure of the ball revealed an austenite phase with coarse Cr rich precipitate. Indented marks observed on the surface of the failed ball are believed to be produced by overloading. In the light of the afore mentioned observations and studies, the failure mechanism of the ball in nuclear fuel exchanger seem to be caused by impact or mechanical overloading on ball.

• Journal of Korea Foundry Society
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• v.21 no.6
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• pp.336-342
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• 2001

This study was carried out to examine the effects of adding 0.3at.%Hf in Fe-30at.%Al-5at.%Cr alloy on the variation of microstructures and hot workability. The effect of hot rolling on mechanical properties was estimated by measuring the elongation and tensile strength after rolling at 800 and 1000 respectively. Microstructure of Fe-30at.%Al-5at.%Cr alloy was consisted of large equiaxed grains and it was changed to quasi-equiaxed or columnar structures by adding 0.3at.%Hf to Fe-30at.%Al-5at.%Cr alloy. Every specimens showed a decreased tensile strength after hot rolling compared to that of before rolling. The elongation was increased by hot rolling. Remarkable changes in elongation by hot rollong was observed such as from 1.4% to 4.5% elongation at the specimen of 0.3at.%Hf added to Fe-30at.%Al-5at.%Cr. Fe-30at.%Al-5at.%Cr alloy showed typical cleavage fracture on tensile failure and hot rolling has negligible effects on fracture mode in this alloy. However at the alloy containing Hf fracture mode was changed by hot rolling from intergranular to mixed intergranular and transgranular fracture mode.