• Title/Summary/Keyword: chemical image

Search Result 502, Processing Time 0.034 seconds

Production of Hydrogen and Carbon Black Using Natural Gas Thermal Decomposition Method (천연가스 열분해법에 의한 수소 및 탄소 제조)

  • Jang, Hun;Lee, Byung Gwon;Lim, Jong Sung
    • Clean Technology
    • /
    • v.10 no.4
    • /
    • pp.203-213
    • /
    • 2004
  • Natural gas thermal decomposition method is the technology of converting natural gas (methane) into hydrogen and carbon at high temperature. The most advantage of thermal decomposition method is that hydrogen and carbon can be produced without emitting carbon dioxide. In this study, the generation of hydrogen and carbon was investigated by this natural gas (methane) thermal decomposition method. We found that pyrocarbon was created on the surface of reactor, carbon black was deposited on the pyrocarbon and final plugging phenomenon took place. To solve this problem, we tried several attempts such as introduction of double pipe reactor instead of single pipe reactor or oxidization of carbon black using $O_2$ or $CO_2$ at regular intervals of reaction. Therefore, some plugging phenomenon was resolved by this methods. Also, carbon particle size was measured by SEM (Scanning Electron Microscope) image and the size was about 200 nm.

  • PDF

Thermal and Mechanical Properties with Hydrolysis of PLLA/MMT Nanocomposite (PLLA/MMT 나노복합재료의 가수분해에 따른 열적, 기계적 물성)

  • Lee Jong Hun;Lee Yun Hui;Lee Doo Sung;Lee Youn-Kwan;Nam Jae-Do
    • Polymer(Korea)
    • /
    • v.29 no.4
    • /
    • pp.375-379
    • /
    • 2005
  • The morphology and therma]/viscoelastic characteristics were investigated for PLLA/MMT nanocomposite manufactured by incorporating inorganic nanosized silicate nanoplatelets into biodeuadable poly(l-lactic acid) (PLLA). The XRD difiactogram and TEM image may be regarded as a formation of homogeneously dispersed nanocomposites. The melting energy(${\Delta}H_m$) was increased during hydrolysis process because of increase of crystallinity. As MMT played a role of reinforcing agent, the storage modulus was increase in case of PLLA/MMT nanocomposite, it was well coincided with our previous results. From SEM image, many tiny pinholes formed by spinodal decomposition were observed on the surface, and the shape of nanocomposite was maintained during hydrolysis process. In this study, it was shown that the control of biodegradation rate, thermal/mechnical property was possibile by incorporating MMT.

Whether Pinhole Scan or Single Photon Emission Computed Tomography (SPECT) in the Diagnosis of Bone and Joint Diseases (골격계진단에 있어서 핀홀스캔의 우월성)

  • Bahk, Yong-Whee
    • The Korean Journal of Nuclear Medicine
    • /
    • v.30 no.1
    • /
    • pp.1-14
    • /
    • 1996
  • Since the publication of the first bone scintiscans in 1962 three decades have elapsed. The bone scan has made great strides during this period, becoming one of the most commonly used nuclear imaging tests. In spite of the progress, however, the specificity of bone scan has remained relatively low. As the result it is a common practice to seek additional information from radiograph, CT scan and MR image, which is euphemistically termed as "image fusion or co-location." The basic reason is the inapplicability of the classical piecemeal analysis to interpreting planar and SPECT bone scans. Such analysis has its base on the observation of elemental features of morphology, which include the size, shape, contour, location, topography and internal architecture. The physiochemical profile may well also be included. Understandably, however, the miniatured images of the planar bone scan cannot provide these features in acceptable detail and the same holds true even with SPECT Images which are but sliced views of the reconstructed planar scans. Fortunately pinhole scanning has the capacity to portray both the morphological and chemical profiles of bone and joint diseases in greater detail through true magnification. The magnitude of pinhole scan resolution is practically comparable to that of radiography as far as gross anatomy is concerned. Thus, we feel strongly that pinhole scanning is a potential breakthrough of the long-lamented low specificity of bone scan. This presentation will discuss the fun-damentals, advantages and disadvantages and the most recent advances of pinhole scanning. It high-lights the actual clinical applications of pinhole scanning in relation to the diagnosis of infective and inflammatory diseases of bone and joint.

  • PDF

Flow Visualization by Light Emission in the Post-chamber of Hybrid Rocket (광도측정에 의한 하이브리드 로켓 후연소실의 유동 가시화)

  • Park, Kyung-su;Choi, Go Eun;Lee, Changjin
    • Journal of the Korean Society for Aeronautical & Space Sciences
    • /
    • v.43 no.8
    • /
    • pp.677-683
    • /
    • 2015
  • Hybrid rocket combustion displays low frequency instability(LFI, 10~30Hz) at a certain condition. Vortex shedding in the post-chamber is suspected to cause the occurrence of LFI. This study focused on the visualization of flow image using light emissions from high temperature combustion gas. Results shows that combustion pressure oscillates at a frequency of about 18 Hz, which is in phase with oscillations of light emission. Since LFI is not a property of thermo-acoustic instability, this result suggested there exists a physical coupling of pressure fluctuations with light emissions proportional to chemical reaction. Also POD analysis shows that dominant symmetric spatial modes in the stable combustion shift suddenly into asymmetric spatial pattern with the appearance of LFI. Especially, the appearance of mode 3 is a typical change of flow dynamics in unstable combustion representing a rotational fluid motions associated with vortex shedding.

Assessment of Relapsing Urolithiasis from K43 with Erosive Gastritis (미란성 위염 환자 K43에서 재발성 요로 결석에 관한 연구)

  • 김재웅
    • The Korean Journal of Food And Nutrition
    • /
    • v.10 no.1
    • /
    • pp.44-52
    • /
    • 1997
  • Nephrolithiasis is the most common disorder of the urinary tract in hospitalized patients, more frequently increased in 30~50 years of age, more common in males than in females, prior right stone to left side, and than upper ureteral stone is found in cultural country, while lower ureteral stone is increased in uncultural country. Stone components are classified as calcium oxalate, calcium phosphate, magnesium ammonium phosphate, uric acid, cystine, and their mixed stone, respectively. According to the pathophysiology of urinary stones, supersaturation/crystalization of inorganic salt concentration in urine, organic matrix, inhibitor deficiency, and epitaxy theory could be based on the stone formation. Not only hypercalciuria, hyperparathyroidism, hyperoxaluria, hyperuricosuria, and cystinuria, but also renal tubular acidosis, hypervitaminosis D, and peptic ulcer, are significantly associated with nephrolithiasis. In this study upper ureteral stone component were analyzed with chemical analysis, infrared spectrum, and image analyzer from K43 patient wit erosive gastritis. As the results, mixed stone of calcium oxalate dihydrate and calcium phosphate apatite was identified, the values of clinical test in blood and urine maintained normal revels. The relapsing urinary stone from K43 have no correlation between factors for stone formation reported early, also have no evidence for risk from erosive gastritis.

  • PDF

A Research Study on Work-Man's Uniform(1) (직장 남성들의 근무복 실태조사 연구(1) -근무복 만족도와 선호도를 중심으로-)

  • 박선희;서미아
    • The Research Journal of the Costume Culture
    • /
    • v.4 no.1
    • /
    • pp.75-91
    • /
    • 1996
  • The work-man's uniform should be coincident wit the image of his firm and accounted of the function according as its purpose. We made questions to 404 workers at 8 firm in our country through the questionnaire papers to know about a work-man's uniform and researched whether the satisfactory in wearing his uniform had relation with his type of business, grade, carrier, age, marriage, and monthly income. The results of this study is as follows; 1. In the uniform status of the fir, thee were many jumper styles in he design of the uniform. The color of that was more dark than bright and the materials of one was used much more chemical fiber than natural fiber. Each of the field office supplied the uniform to his work-man more frequently than the main office. All of firm payed off the uniform expense and decision of the uniform design was almost made both the firm and the labour union. 2. In he satisfaction of the uniform, the satisfaction of uniform was shown high in the design, color, materials, size and function. The highest dissatisfaction reason is as follows; it was disagreeable to concrete design in the design and dark color and keeping warm or draft was bad in the materials, the bust and pant's length was long in the size. 3. In preference of the uniform, the older of preference in the design was what the working environment and the image of firm was suitable, the characteristic uniform. The order of preference in the color was beige, blue, grey. The preference of in the materials was good to keep warm and draft. The preference in the pattern was 'no pattern' every type of business. The experts, or administrators and office workers than others preferred 'no pattern' of the uniform in the pattern.

  • PDF

Proximate Content Monitoring of Black Soldier Fly Larval (Hermetia illucens) Dry Matter for Feed Material using Short-Wave Infrared Hyperspectral Imaging

  • Juntae Kim;Hary Kurniawan;Mohammad Akbar Faqeerzada;Geonwoo Kim;Hoonsoo Lee;Moon Sung Kim;Insuck Baek;Byoung-Kwan Cho
    • Food Science of Animal Resources
    • /
    • v.43 no.6
    • /
    • pp.1150-1169
    • /
    • 2023
  • Edible insects are gaining popularity as a potential future food source because of their high protein content and efficient use of space. Black soldier fly larvae (BSFL) are noteworthy because they can be used as feed for various animals including reptiles, dogs, fish, chickens, and pigs. However, if the edible insect industry is to advance, we should use automation to reduce labor and increase production. Consequently, there is a growing demand for sensing technologies that can automate the evaluation of insect quality. This study used short-wave infrared (SWIR) hyperspectral imaging to predict the proximate composition of dried BSFL, including moisture, crude protein, crude fat, crude fiber, and crude ash content. The larvae were dried at various temperatures and times, and images were captured using an SWIR camera. A partial least-squares regression (PLSR) model was developed to predict the proximate content. The SWIR-based hyperspectral camera accurately predicted the proximate composition of BSFL from the best preprocessing model; moisture, crude protein, crude fat, crude fiber, and crude ash content were predicted with high accuracy, with R2 values of 0.89 or more, and root mean square error of prediction values were within 2%. Among preprocessing methods, mean normalization and max normalization methods were effective in proximate prediction models. Therefore, SWIR-based hyperspectral cameras can be used to create automated quality management systems for BSFL.

Study on the Optical Characteristics of the Green Phosphor for PDP Application (PDP용 녹색 형광체의 광 특성 개선에 관한 연구)

  • Han, Bo Yong;Yoo, Jae Soo
    • Korean Chemical Engineering Research
    • /
    • v.47 no.2
    • /
    • pp.150-156
    • /
    • 2009
  • Plasma Display Panels(PDPs) require to have improved luminous efficiency, low manufacturing cost, and high image quality to compete with other flat display devices such as Liquid Crystal Displays(LCDs) and organic light-emitting diodes(OLEDs). In addition, the diversity of product line-up may be needed for high market share. In this paper, the optical characteristics of typical green phosphor for PDP application are reviewed and the problem-based solution will be proposed. We also shortly describe the principle of 3D-PDPs which are promising. Then, the requirement of green phosphor for 3D-PDP application is summarized and research achievement, as of now, is described. The typical problems of $Zn_2SiO_4:Mn$ phosphor, which is the most well-known, are the negatively charged surface property and the long decay time, which leads to unstable discharge in green cell and afterimage. These problems were solved by coating the phosphor surface with metallic oxide. It was found that $Al_2O_3$ would be the best material for $Zn_2SiO_4:Mn$ phosphor. It gives longevity as well as low operating voltage due to the charging effect in green cells. Also, new phosphors, $(Y,\;Gd)Al_3(BO_3)_4:Tb$ and $(Mg,\;Zn)Al_2O_4:Mn$ phosphor are proposed for increasing the luminance and reducing the decay time, which are capable to apply for 3D-PDP application.

Hexagonal Boron Nitride Monolayer Growth without Aminoborane Nanoparticles by Chemical Vapor Deposition

  • Han, Jaehyu;Yeo, Jong-Souk
    • Proceedings of the Korean Vacuum Society Conference
    • /
    • 2014.02a
    • /
    • pp.409-409
    • /
    • 2014
  • Recently hexagonal boron nitride (h-BN), III-V compound of boron and nitrogen with strong covalent $sp^2$ bond, is a 2 dimensional insulating material with a large direct band gap up to 6 eV. Its outstanding properties such as strong mechanical strength, high thermal conductivity, and chemical stability have been reported to be similar or superior to graphene. Because of these excellent properties, h-BN can potentially be used for variety of applications such as dielectric layer, deep UV optoelectronic device, and protective transparent substrate. Ultra flat and charge impurity-free surface of h-BN is also an ideal substrate to maintain electrical properties of 2 dimensional materials such as graphene. To synthesize a single or a few layered h-BN, chemical vapor deposition method (CVD) has been widely used by using an ammonia borane as a precursor. Ammonia borane decomposes into hydrogen (gas), monomeric aminoborane (solid), and borazine (gas) that is used for growing h-BN layer. However, very active monomeric aminoborane forms polymeric aminoborane nanoparticles that are white non-crystalline BN nanoparticles of 50~100 nm in diameter. The presence of these BN nanoparticles following the synthesis has been hampering the implementation of h-BN to various applications. Therefore, it is quite important to grow a clean and high quality h-BN layer free of BN particles without having to introduce complicated process steps. We have demonstrated a synthesis of a high quality h-BN monolayer free of BN nanoparticles in wafer-scale size of $7{\times}7cm^2$ by using CVD method incorporating a simple filter system. The measured results have shown that the filter can effectively remove BN nanoparticles by restricting them from reaching to Cu substrate. Layer thickness of about 0.48 nm measured by AFM, a Raman shift of $1,371{\sim}1,372cm^{-1}$ measured by micro Raman spectroscopy along with optical band gap of 6.06 eV estimated from UV-Vis Spectrophotometer confirm the formation of monolayer h-BN. Quantitative XPS analysis for the ratio of boron and nitrogen and CS-corrected HRTEM image of atomic resolution hexagonal lattices indicate a high quality stoichiometric h-BN. The method presented here provides a promising technique for the synthesis of high quality monolayer h-BN free of BN nanoparticles.

  • PDF

A Study on the Electroplating using Macroemulsion in High Pressure (고압 매크로에멀젼을 이용한 전해도금에 관한 연구)

  • Park, Ji-Young;Yang, Jun Youl;Suh, Dong Jin;Yoo, Ki-Pung;Lim, Jong Sung
    • Korean Chemical Engineering Research
    • /
    • v.43 no.1
    • /
    • pp.53-59
    • /
    • 2005
  • In this study, the supercritical electroplating was investigated by forming macroemulsion of electroplating solution using surfactant in supercritical $CO_2$. The fluorinated analogous AOT surfactant, sodium salt of bis (2,2,3,3,4,4,5,5-octafluoro-1-pentanol) sulfosuccinate which has both '$CO_2$ philic' chains and 'hydrophilic' head group was used as a surfactant, and Ni plate and Cu plate were used as the anode and the cathode, respectively. Electroplating was carried out in the conventional method and the supercritical macroemulsion and both results were compared. The supercritical electroplating was carried out in various concentration of surfactant such as 2, 4, 7 wt%, the volume ratio of Ni-plating solution to $CO_2$ was varied in the range of 10-70 vol%, and propane was used as a supercritical fluid instead of $CO_2$. According to the experimental results, the plated surface of Ni on Cu plate performed in supercritical macroemulsion was better than that, in conventional state. In the image of Ni surface plated on Cu plate in supercritical state, there were fewer pin-holes and pits comparing with that in the conventional process. The current and conductivity was increased as the volume ratio of Ni-plating solution to $CO_2$ was increased and the current and the amount of Ni plated on Cu plate were decreased as the concentration of surfactant become higher. In addition, in case of the continuous phase, using $CO_2$ was more effective than using $CO_2$.