• Title/Summary/Keyword: chemical image

Search Result 502, Processing Time 0.027 seconds

Influence of kneading ratio on the binding interaction of coke aggregates on manufacturing a carbon block

  • Kim, Jong Gu;Kim, Ji Hong;Bai, Byong Chol;Choi, Yun Jeong;Im, Ji Sun;Bae, Tae-Sung;Lee, Young-Seak
    • Carbon letters
    • /
    • v.28
    • /
    • pp.24-30
    • /
    • 2018
  • Coke aggregates and carbon artifacts were produced to investigate the interactions of coke and pitch during the kneading process. In addition, the kneading ratio of the coke and binder pitch for the coke aggregates was controlled to identify the formation of voids and pores during carbonization at $900^{\circ}C$. Experiments and thermogravimetric analysis revealed that carbon yields were improved over the theoretical yield calculated by the weight loss of the coke and binder pitch; the improvement was due to the binding interactions between the coke particles and binder pitch by the kneading process. The true, apparent, and bulk densities fluctuated according to the kneading ratio. This study confirmed that an excessive or insufficient kneading ratio decreases the density with degradation of the packing characteristics. The porosity analysis indicated that formation of voids and pores by the binder pitch increased the porosity after carbonization. Image analysis confirmed that the kneading ratio affected the formation of the coke domains and the voids and pores, which revealed the relations among the carbon yields, density, and porosity.

Fabrication of Size-Controlled Hole Array by Surface-Catalyzed Chemical Deposition (표면 촉매 화학 반응을 이용한 크기 조절이 가능한 홀 어레이 제작)

  • Park, Hyung Ju;Park, Jeong Won;Lee, Dae-Sik;Pyo, Hyeon-Bong
    • Journal of Sensor Science and Technology
    • /
    • v.27 no.1
    • /
    • pp.55-58
    • /
    • 2018
  • Low-cost and large-scale fabrication method of nanohole array, which comprises nanoscale voids separated by a few tens to a few hundreds of nanometers, has opened up new possibilities in biomolecular sensing as well as novel frontier optical devices. One of the key aspects of the nanohole array research is how to control the hole size following each specific needs of the hole structure. Here, we report the extensive study on the fine control of the hole size within the range of 500-2500 nm via surface-catalyzed chemical deposition. The initial hole structures were prepared via conventional photo-lithography, and the hole size was decreased to a designed value through the surface-catalyzed chemical reduction of the gold ion on the predefined hole surfaces, by simple dipping of the hole array device into the aqueous solution of gold chloride and hydroxylamine. The final hole size was controlled by adjusting reaction time, and the optimal experimental condition was obtained by doing a series of characterization experiments. The characterization of size-controlled hole array was systematically examined on the image results of optical microscopy, field emission scanning electron microscopy(FESEM), atomic-force microscopy(AFM), and total internal reflection microscopy.

Preparation of Pt Catalysts Supported on ACF with CNF via Catalytic Growth

  • Park, Sang-Sun;Rhee, Jun-Ki;Jeon, Yu-Kwon;Choi, Sung-Won;Shul, Yong-Gun
    • Carbon letters
    • /
    • v.11 no.1
    • /
    • pp.38-40
    • /
    • 2010
  • Carbon supported electrocatalysts are commonly used as electrode materials for polymer electrolyte membrane fuel cells(PEMFCs). These kinds of electrocatalysts provide large surface area and sufficient electrical conductivity. The support of typical PEM fuel cell catalysts has been a traditional conductive type of carbon black. However, even though the carbon particles conduct electrons, there is still significant portion of Pt that is isolated from the external circuit and the PEM, resulting in a low Pt utilization. Herein, new types of carbon materials to effectively utilize the Pt catalyst are being evaluated. Carbon nanofiber/activated carbon fiber (CNF/ACF) composite with multifunctional surfaces were prepared through catalytic growth of CNFs on ACFs. Nickel nitrate was used as a precursor of the catalyst to synthesize carbon nanofibers(CNFs). CNFs were synthesized by pyrolysising $CH_4$ using catalysts dispersed in acetone and ACF(activated carbon fiber). The as-prepared samples were characterized with transmission electron microscopy(TEM), scanning electron microscopy(SEM). In TEM image, carbon nanofibers were synthesized on the ACF to form a three-dimensional network. Pt/CNF/ACF was employed as a catalyst for PEMFC. As the ratio of prepared catalyst to commercial catalyst was changed from 0 to 50%, the performance of the mixture of 30 wt% of Pt/CNF/ACF and 70wt% of Pt/C commercial catalyst showed better perfromance than that of 100% commercial catalyst. The unique structure of CNF can supply the significant site for the stabilization of Pt particles. CNF/ACF is expected to be promising support to improve the performance in PEMFC.

The Effect of the Purity of Raw Materials on the Purity of Silicon Extracted by Solvent Refining and Centrifugation (용매정제법과 원심분리법으로 추출한 Si의 순도에 미치는 장입 원재료 순도의 영향)

  • Cho, Ju-Young;Seo, Kum-Hee;Kang, Bok-Hyun;Kim, Ki-Young
    • Korean Journal of Metals and Materials
    • /
    • v.50 no.12
    • /
    • pp.907-911
    • /
    • 2012
  • High purity silicon can be obtained from Al-Si alloys by a combination of solvent refining and centrifugation. Silicon purification by crystallization of silicon from an Al-Si alloy melt was carried out using 2N and 4N purity aluminum and 2N purity silicon as raw materials. The effect of the purity of raw materials on the final silicon ingot purity by centrifugation was investigated for an Al-50 wt% Si alloy. Alloys were melted using an electrical resistance furnace, and then poured into a centrifuging apparatus. A silicon lump like foam was obtained after centrifugation and was leached by an acid in order to get pure silicon flakes. Then silicon flakes were melted to make a silicon ingot using an induction furnace. The purities of the silicon flakes and silicon ingot were enhanced significantly compared to those of the raw materials of silicon and aluminum. The silicon ingot made of 4N aluminum and 2N silicon showed the lowest impurities.

A Study on the Environmental Application of Image Radar for Expanding the Use of Next Generation Medium Satellite 5 (차세대중형위성 5호 활용 확대를 위한 영상레이더의 환경분야 활용 방안 연구)

  • Han, Hyeon-gyeong;Lee, Moungjin
    • Korean Journal of Remote Sensing
    • /
    • v.35 no.6_3
    • /
    • pp.1251-1260
    • /
    • 2019
  • Existing environmental spatial information, which has been concentrated on spatial resolution, has limitations in solving realistic environmental problems that must be accompanied by physical and chemical characterization. Accordingly, there is a need for an image radar capable of identifying physical characteristics of an object regardless of weather conditions, day and night, and sunlight. Image radar is used in various fields in the United States and Europe. The next generation of medium-sized satellite No. 5 in Korea, which is under development with the aim of monitoring water disasters, is also looking for ways to expand the scope to various applications based on the existing application range. To this end, we analyzed domestic and international papers (100 works) using image radar, and reviewed KEI 2016 report, domestic papers, and foreign papers. Based on this, various environmental issues were summarized and the effects of when the image radar was used were analyzed and land cover was selected as an environmental issue. In the future, we will embody the technology to improve the accuracy of the land cover map, which is the environmental issue selected in this study, and build the foundation system for the stable use of the land cover map.

The Accuracy of the Radiographic Method in Root Canal Length Measurement (근광장 측정에서 방사선 사진술의 정확도)

  • Jo Eun-Young;Park Chang-Seo
    • Journal of Korean Academy of Oral and Maxillofacial Radiology
    • /
    • v.28 no.2
    • /
    • pp.471-489
    • /
    • 1998
  • For the successful endodontic treatment, root canal should be cleaned thoroughly by accurate mechanical and chemical canal preparation and sealed completely with canal filling material without damaging the periapical tissues. The accuracy of the root canal length measurement is a prerequisite for the success of the endodontic treatment, and the root canal length is often determined by the standard periapical radiographs and digital tactile sense. In this study, the accuracy and the clinical usefulness of Digora/sup (R)/, an intraoral digital imaging processor and the conventional standard radiographs were compared by measuring the length from the top of the file to the root apex. 30 single rooted premolars were invested in a uniformly sized blocks and No.25 K-file was inserted into and fixed in each canal. Each block was placed in equal distance and position to satisfy the principle of the bisecting angle and paralleling techniques and Digora/sup (R)/ system's image and standard periapical radiographs were taken. Each radiograph was examined by 3 different observers by measuring the length from top of the file to the root apex and each data was compared and analyzed. The results were as follows; 1. In the bisecting angle technique, the average difference between the Digora/sup (R)/ system and standard periapical radiograph was 0.002 mm and the standard deviation was 0.341 mm which showed no statistically significant difference between the two systems(p>0.05). Also, in the paralleling technique, the average difference between these two system was 0.007 mm and the standard deviation was 0.323 mm which showed no statistically significant difference between the two systems(p>0.05). 2. In Digora/sup (R)/ system, the average difference between the bisecting angle and paralleling technique was -0.336 mm and the standard deviation was 0.472 mm which showed a statistically significant difference between the two techniques(p<0.05). Also, in the standard periapical radiographs, the average difference between the bisecting angle and paralleling technique was 0.328 mm and the standard deviation was 0.517 mm which showed a statistically significant difference between these two techniques(p<0.05). 3. In Digora/sup (R)/ system and the standard periapical radiographs. there was a statistically significant difference between the measurement using the bisecting angle technique and the actual length(p<0.05), But there was no statistically significant difference between the measurement using the paralleling technique and the actuallength(p>0.05). In conclusion. the determination of the root canal length by using the Digora/sup (R)/ system can give us as good an image as the standard periapical radiograph and using the paralleling technique instead of the bisecting angle technique can give a measurement closer to the actual canal length. thereby contributing to a successful result. Also. considering the advantages of the digital imaging processor such as decreasing the amount of exposure to the patient. immediate use of the image. magnification of image size. control of the contrast and brightness and the ability of storing the image can give us good reason to replace the standard periapical radiographs.

  • PDF

Three-Dimensional Analysis of the Mesophyll Plastids Using Ultra High Voltage Electron Microscopy (초고압전자현미경에 의한 엽육세포 색소체 미세구조의 3차원적 분석)

  • Kim, In-Sun;Park, Sang-Chan;Han, Sung-Sik;Kim, Eun-Soo
    • Applied Microscopy
    • /
    • v.36 no.3
    • /
    • pp.217-226
    • /
    • 2006
  • Image processing by ultra high voltage electron microscopy (UHVEM) and tomography has offered major contributions to research in the field of cellular ultrastructure. Furthermore, such advancements also have enabled the improved analysis of three-dimensional cellular structures in botany. In the present study. using UHVEM and tomography, we attempted to reconstruct the three-dimensional images of plastid inclusions that probably differentiate during photosynthesis. The foliar tissues were studied Primarily with the TEM and further examined with UHVEM. The spatial relationship between tubular elements and the thylakoidal membrane and/or starch grains within plastids mainly have been investigated in CAM-performing Sedum as well as in $C_4$ Salsola species. The inclusion bodies were found to occur only in early development in the former, while they were found only in mesophyll cells in the latter. The specimens were tilted every two degrees to obtain two-dimensional images with UHVEM and subsequently comparison has been made between the two types. Digital image processing was performed on the elements of the inclusion body using tilting, tomography, and IMOD program to generate and reconstruct three-dimensional images on the cellular level. In Sedum plastids, the inclusion bodies consisted of tubular elements exhibiting about 20 nm distance between elements. However, in Salsola, plastid inclusion bodies demonstrated quite different element structure, displaying pattern, and origin relative to those of the Sedum. The inclusion bodies had an integrative relationship with the starch grains in both species.

A Study on the Analysis of Vegetation, Spatial Image and Visual Preference of Roadside Slopes in Chi-Ri Mt. National Park(I) (지리산 국립공원 도로비탈면의 식생과 경관분석에 관한 연구(I) -식 생조사분석-)

  • 서병수;김세천;이규완;박종민;이창헌
    • Journal of the Korean Institute of Landscape Architecture
    • /
    • v.19 no.2
    • /
    • pp.75-91
    • /
    • 1991
  • This study is one of studies on the analysis of vegetation spatial image and visual preference of roadside slopes in Chi-Ri Mt. national park. In this article, we analized the soil characteristics and the actual vegetation within slopes and forest lands contiguous to those. The results obtained were summarized as follows; The physical and chemical properties of soil in forest lands were better than slopes and Cheoneun temple - Seongsam pass was the best fertilized among 3 sector. In the structure of woody plants in forest lands, the high importance value species were Pinus denciflora, Quercus aliena within Ukmojeong-Deokdong sector, Q. aliena, Q. varabilis, Q. serrata within Banseon-Seongsam pass sector, and P. denciflora, Q. dentata within Cheoneun temple-Seongsam pass sector. And also, Aster scaber, Arundinella hirta, Pteridium aquilinum were the high importance value herbs within all sector. In slopes, the species diversity indices of woody plants were low, but that of herbs showed slightly high. By the cluster analysis used in similarity index, it was observed that woody plants structure between slopes and forest lands made little, but the herbs made slightly higher than woody plants.

  • PDF

Color Images of Purple Clothing (보라색 복식의 이미지 특성)

  • 김은경;김영인
    • Journal of the Korean Society of Clothing and Textiles
    • /
    • v.24 no.3
    • /
    • pp.373-384
    • /
    • 2000
  • This study is to demonstrate purple color characteristics by analyzing various purple clothing from Antiquity to modern fashion. In this respect, both documentary and investigative studies have been performed. Through, the documentary studies, the changes and examples of purple clothing were scrutinized, and images of purple were classified based on the Color Image Scale. Purple color samples applied during a period from 1993 to 1996, were collected from 33 women's domestic brands, and the colors were measured by the CE 7000 spectrophotometer and analyzed by Munsell HV/C. The results were shown as follows; 1. In Antiquity, the symbolic value of purple was heavenly color, because it was a bearer of light, a sign of the epiphany of the gods. 2. With the advent of synthetic dyes, purples were in the vanguard. This chemical synthesis gave purple, historically a regal prerogative, to the people, and enjoyed a memorable vogue in the mid-mineteenth century. 3. The purple images in fashion were changed by the factors such as culture-art, technological advances, political-economical situations, sports ect., and appears in modern fashion romantic, natural elegance, classic, gorgeous, chic, and dandy images. 4. In the result of analytical study on women's purple dress in domestic market, 10PB hue and P tone were mosetly used from 1993 to 1996.

  • PDF

Preparation and Electrochemical Behavior of MWNT and MWNT/DAAQ Nanocomposite Materials for Electrochemical Capacitor (전기화학캐패시터용 MWNT 및 MWNT/DAAQ 나노 복합체의 제조 및 전기화학적 거동)

  • Kim, Hong-Il;Park, Soo-Gil
    • Journal of the Korean Electrochemical Society
    • /
    • v.10 no.3
    • /
    • pp.169-174
    • /
    • 2007
  • MWNT/DAAQ(1,5-diaminoanthraquinone) composites were prepared by chemical polymerization of DAAQ onto MWNT and their capacitance was evaluated by means of cyclic voltammetry in 1M $H_2SO_4$ electrolyte. The performances of such cells have been compared with pure MWNT and DAAQ based electrodes. The SEM image shows that DAAQ was coated onto MWNT during polymerization and thermal stability from th TG analysis. The highest specific capacitance values of 97F/g were observed with AC-MWNT/DAAQ composite electrode. And MWNT/DAAQ based composite electrode also showed relatively good electrochemical behaviors better than MWNT electrode in sulfuric acid electrolyte.