• 제목/요약/키워드: chemical analyses

검색결과 1,767건 처리시간 0.031초

Molecular Recognition : ${\alpha}$-Cyclodextrin and Aspirin Inclusion Complexation

  • Hee Sook Choi
    • Bulletin of the Korean Chemical Society
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    • 제13권5호
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    • pp.474-479
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    • 1992
  • Molecular interaction between ${\alpha}$-cyclodextrin and aspirin was studied by UV, $^2H$-NMR and $^2H$-NMR spectroscopy analyses for solution complex and by FT-IR analyses for solid complex. The inclusion structure provides a basic understanding of the aspirin and ${\alpha}$-cyclodextrin interaction.

특정환경조건하에서의 콘크리트 내 이차광물생성과 그에 수반된 성능저하현상 (Secondary Mineral Formation and Concrete Deterioration Caused by Certain Environmental Conditions)

  • 이효민;황진연;진치섭;이진성;전쌍순
    • 한국콘크리트학회:학술대회논문집
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    • 한국콘크리트학회 2003년도 봄 학술발표회 논문집
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    • pp.651-656
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    • 2003
  • Durability of concrete is possibly related to externally-induced chemical attacks in addition to internally-induced deterioration. Externally-induced chemical attacks can be derived from various sources according to environmental conditions under which concrete structures are existing. The present study investigates the characteristic concrete deterioration and formation of secondary minerals by external chemical attacks under certain environmental condition. Petrographic microscope, SEM, EDAX, XRD analyses were conducted to identify secondary mineral formation and micro-structural analyses.

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Effect of Grinding on Color and Chemical Composition of Pork Sausages by Near Infrared Spectrophotometric Analyses

  • Kang, J.O.;Park, J.Y.;Choy, Y.H.
    • Asian-Australasian Journal of Animal Sciences
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    • 제14권6호
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    • pp.858-861
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    • 2001
  • Near Infrared spectroscopy was applied to the samples of processed pork to see the effect of grinding on chemical components analyses. Data from conventional chemical analyses of moisture, fat, protein, NaCl were put into calibration model by NIR of reflectance mode. The other properties observed were pH and color parameters ($L^*,\;a^*,\;b^*$). Spectral ranges of 400~2500 nm and 400~1100 nm were compared for color parameters. Spectral ranges of 400~2500 nm and 1100~2500 nm were compared for chemical components and pH. Different spectral ranges caused little changes in the coefficients of determination or standard errors. $R^{2,}s$ of calibration models for color parameters were in the range of 0.97 to 1.00. $R^{2,}s$ of calibration models of intact sausages for moisture, protein, fat, NaCl and pH were 0.98, 0.89, 0.95, 0.73 and 0.77, respectively using spectra at 1100~2500 nm. $R^{2,}s$ of calibration models of ground sausages for moisture, protein, fat, NaCl and pH were 0.97, 0.91, 0.97, 0.42 and 0.56, respectively using spectra at 1100~2500 nm.

유체와 온도 조절을 이용한 생화학 물질 반응용 마이크로칩의 개발 (BEAD BASED CHEMICAL REACTION SYSTEM USING TEMPERATURE AND FLUID CONTROL FOR CANCER DETECTION)

  • 김민수;이보람;윤효진;김병기;이윤식;김용권
    • 대한전기학회:학술대회논문집
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    • 대한전기학회 2008년도 제39회 하계학술대회
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    • pp.1466-1467
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    • 2008
  • We describe here a novel micro total analysis system for the purification and identification of the affinity-captured proteins. Also we demonstrated the mass analysis of the Carcinoembrionic antigen (CEA) and Alpha femtoprotein which were chosen as the target cancer marker. For MALDI-TOF analyses, the proteins should to be separated from a protein mixture and be concentrated when needed. This procedure usually takes a long time even before protease-digested samples are to be obtained from them. Here, we describe integrated and efficient micro chip for protein purification and digestion for MALDI-TOF analyses. At first, disease protein is purified by passing the micro chamber from a protein mixture or human whole serum and released from the micro affinity beads by thermal heating. Purified protein is then transfer to the hole for trypsin digestion. The final sample is analyzed by MALDI-TOF. All the processes could be finished successfully within one hour, which renders MALDI-TOF analyses of a target protein quite simple.

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ligand Field Analyses of Tris(biuret)chromium(Ⅲ) Chloride and Hexaureachromium(Ⅲ) Bromide

  • 박성진;오병근;박영동;이규왕
    • Bulletin of the Korean Chemical Society
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    • 제20권8호
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    • pp.943-947
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    • 1999
  • Ligand field analyses for tris(biuret)chromium(III) chloride and hexaureachromium(III) bromide were performed and compared to understand the ligand field properties of both ligands. The optimized eσO and eπO values indicate that coordinated oxygen atom in biuret ligand is a moderate s- and strong p-donor, while that in urea ligand is a weak σ- and moderate π-donor. The electronic structures of those two complexes are quite different and they were well accounted by inclusion of an anisotropic p bonding.

Seawater Quality And Red Tides In Jinhae Bay:I. Relationships Between Water Quality Parameters And Red Tides

  • Lee, Kwang Woo;Hong, Gi-Hoon;Yang, Dong-Beom;Lee, Soo-Hyung
    • 한국해양학회지
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    • 제16권2호
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    • pp.43-48
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    • 1981
  • To carry out baseline studies on monitoring systems for red tides in Jinhae bay, measurements and analyses were made on seawater samples from 15 sampling stations during 15 months from July, 1979. Water quality parameters studied are temperature, pH, DO, salinity, COD, SS, NO$\sub$3/, NO$\sub$2/, PO$\sub$4/, SiO$\sub$2/, Ca, Mg, Cd, Cu, Pb, Zn, Chlorophyll ${\alpha}$, diatoms and dinoflagellates. Multiple regression analyses were undertaken with chlorophyll ${\alpha}$, cell numbers of diatoms and dinoflagellates as the dependent variables and water quality parameters as the independent variables. The results showed that biomass, expressed as total cell numbers of diatoms and dinoflagellates, was largely influenced by COD, salinity and nutrients.

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한국 온천수의 수질적 특성(I) (Characteristics of Mineral and Thermal Waters in South Korea)

  • 임정웅
    • 기술사
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    • 제32권6호
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    • pp.60-67
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    • 1999
  • 299 chemical analyses are used to study the characteristics of mineral and thermal waters in South Korea. Even though the concentration of chemical components in thermal waters are generally very low, mineral waters having components more than 1,000 ppm of dissolved total solid(TDS) are reached up to 19% total analyses data, In Germany, Japan or some other countries, mineral and thermal waters are detined not only by water temperature, but also by chemical components. The principle of Law in Japan in also almost same with the German regulations. However, the Law for thermal spring In Korea permit thermal water to be qualifiled only by water temperature. For including chemical characters into the regulations or Law of thermal spring, the limit values of TDS and other 9 micro components related to mineral and thermal waters was selected through this study.

혼합 액체 연료의 화학반응 인자 계측에 관한 실험적 연구 (An Experimental Study on Measurement of Chemical Kinetic Parameters of a Liquid Fuel with Various Components)

  • 최효현;임준석;김철진;손채훈
    • 한국연소학회지
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    • 제16권3호
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    • pp.21-26
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    • 2011
  • Thermal analyses are conducted to measure chemical kinetic parameters of an unknown liquid fuel with various components. Thermal Analyses are divided into two different methods such as TGA(Thermo-Gravimetric Analysis) and DSC(Differential Scanning Calorimety). Non-isothermal experimental results are analyzed by adopting TGA and they are filtered by Freeman-Carroll method. As a results of the analysis, chemical parameters of the activation temperature and the reaction order are measured to be 6128.2 K and 1.4, respectively. Furthermore, the chemical kinetic parameters are obtained by a variety of mathematical processing methods. It has been found that they show a little difference depending on the processing method.