• 대한금속재료학회지
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• 제46권4호
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• pp.199-208
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• 2008

This study is concerned with effects of complex oxides on Charpy impact toughness of heat affected zone (HAZ) of API X80 linepipe steels. Three kinds of steels were fabricated by varying alloying elements such as Ti, Al, and Mg and hot-rolling conditions to form complex oxides, and their microstructures and Charpy impact properties were investigated. The number of complex oxides present in the steel containing excess Ti, Al, and Mg was twice larger than that in the conventional steels, while their size ranged from 1 to $3{\mu}m$ in the three steels. After the HAZ simulation test, the steel containing a number of oxides contained about 20 vol.% of acicular ferrite in the simulated HAZ, together with bainitic ferrite and martensite, whereas the HAZ microstructure of the conventional steels consisted of bainitic ferrite and martensite with a small amount of acicular ferrite. This formation of acicular ferrite in the oxide-containing steel was associated with the nucleation of acicular ferrite at complex oxides, thereby leading to the great (five times or more) improvement of Charpy impact toughness over the conventional steels.

• 한국재료학회지
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• 제31권9호
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• pp.519-524
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• 2021

The impact properties of two austenitic Fe-23Mn-0.4C steels with different Al contents for cryogenic applications are investigated in this study. The 4Al steel consists mostly of austenite single-phase microstructure, while the 5Al steel exhibits a two-phase microstructure of austenite and delta-ferrite with coarse and elongated grains. Charpy impact test results reveal that the 5Al steel with duplex phases of austenite and delta-ferrite exhibits a ductile-to-brittle transition behavior, while the 4Al steel with only single-phase austenite has higher absorbed energy over 100 J at -196 ℃. The SEM fractographs of Charpy impact specimens show that the 4Al steel has a ductile dimple fracture regardless of test temperature, whereas the 5Al steel fractured at -100 ℃ and -196 ℃ exhibits a mixed fracture mode of both ductile and brittle fractures. Additionally, quasi-cleavage fracture caused by crack propagation of delta-ferrite phase is found in some regions of the brittle fracture surface of the 5Al steel. Based on these results, the delta-ferrite phase hardly has a significant effect on absorbed energy at room-temperature, but it significantly deteriorates low-temperature toughness by acting as the main site of the propagation of brittle cracks at cryogenic-temperatures.

• 대한용접접합학회:학술대회논문집
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• 대한용접접합학회 2009년 추계학술발표대회
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• pp.51-51
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• 2009

In order to understand the properties of high heat input welds made by electro gas welding, two kinds of low temperature steel were welded. Welding heat inputs were controlled by width of root gap and ranged from 118 to 143kJ/cm. Chemical composition and micro-structural analysis were performed. To understand low temperature impact properties, Charpy impact test was conducted at several temperatures. The results were summarized as follows; 1) Grain size of weld metal and heat affected zone was increased with an increase in welding heat input. 2) Impact test values at fusion line were severely fluctuated regardless of base metals, showing enormous difference among the values at the same test temperature.

• 한국산학기술학회논문지
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• 제5권3호
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• pp.204-209
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• 2004

금형부품으로 사용되는 STD11과 STS3의 열처리에 따른 물리적 특성을 비교하여 금형부품으로 사용시 약점으로 지적되어온 물성을 개선시키고자 하였다. STS3와 STD11의 잔류 austenite의 측정과 촉진시효변형시험, Charpy 충격시험결을 실시한 결과 목표경도를 얻기 위한 심냉처리의 효과, 작업안정성과 칫수안정성면에서 STD11이 STS3보다 우수한 것으로 나타났다. STS3에서는 심냉처리에 의한 잔류 austenite의 감소량은 크게 나타나지 않았으며 또한, 변형을 최소화시켜야 하는 금형에서는 심냉처리가 필수적이라는 것을 확인하였다.

• Journal of Welding and Joining
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• 제4권3호
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• pp.58-71
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• 1986

Mechanical and corrosion property of duplex stainless steel weldments made by the GTAW and SMAW process were studied. Fracture toughness, general and local corrosion resistance of GTAW and SMAW weldments were evaluated in terms of Charpy V notch impact test, anodic polarization diagram, pitting corrosion rate, respectively. SMA weld metal showed much lower impact toughness and higher ductile-brittle transition temperature than GTA weld metal. Fractographic and EDX analysis on fracture surface of SMA weld metal demonstrated the existence of (Si, Ti), oxide in large amounts. Potentiodynamic anodic polarization diagram of GMA weld metal showed much lower passive current density than SMA weld metal in 4% $H_2/SO_4$ solution. And pitting corrosion rate test showed the same tendency. Relating the microstructure, chemistry and property, it can be concluded that GTA weld metal gives better toughness due to lower oxygen content, i.e. lower inclusion content, and better corrosion resistance due to higher Pitting Index(PI) than SMA weld metal.

• 한국정밀공학회:학술대회논문집
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• 한국정밀공학회 1995년도 추계학술대회 논문집
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• pp.728-731
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• 1995

Miniaturzed specimen technology permits mechanical bechanical behavior to be determined using a minimum volume of material. because it is almost impossible to sample the conventional specimen for the fracture toughness test without damage to the rotor. In addition, it is different to collect a large amount of actual turbine rotor steels. Hence seven kinds of specimen with different degradation levels were prepared by isothermal aging heat treatment at 630 .deg. C. Test material was 1Cr-1Mo-0.25V steel which was widely used for turbine rotor material. The relation between fracture toughness and DBTT was investigated The characteristics of minaturized impact speciments technique was discussed. Finally, the estimating method of fracture toughness using a single impact specimen was introduced.

• 대한기계학회논문집A
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• 제24권8호
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• pp.1910-1916
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• 2000

The five classes of the thermally aged CF8M specimen are prepared using an artificially accelerated aging method. Namely, after the specimens are held for 100, 300, 900, 1800, and 3600hrs at 430$^{\circ}C$ respectively, the specimens are water-cooled to room temperature. The impact energy variations are measures for both the aged and virgin specimens through the Charpy impact tests in addition to the microstructure observation, tensile, hardness and fatigue crack growth tests. From the present investigation the following results are obtained : 1) The difference among the thermally degraded specimens can be distinguished through their microstructures, 2) Hardness and tensile strength are increased to 300hrs, degradation specimen, while elongation and reduction area are decreased to 3600hrs degradation specimen, and impact energy is decreased to 1800hrs degradation specimen, 3) The FCG rates for thermally degraded specimens are larger than that of the virgin specimen.

• Nuclear Engineering and Technology
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• 제44권5호
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• pp.543-550
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• 2012

The decrease in the fracture toughness of ferritic steels in a reactor pressure vessel is an important factor in determining the lifetime of a nuclear power plant. A surveillance program has been in place in Korea since 1979 to assess the structural integrity of RPV steels. In this work, the surveillance data were collected and analyzed statistically in order to derive the empirical relationship between the embrittlement and strengthening of irradiated reactor pressure vessel steels. There was a linear relationship between the yield strength change and the transition temperature shift change at 41 J due to irradiation. The proportional coefficient was about $0.5^{\circ}C$/MPa in the base metals (plate/forgings). The upper shelf energy decrease ratio was non-linearly proportional to the yield strength change, and most of the data lay along the trend curve of the US results. The transition regime temperature interval, ${\Delta}T_T$, was less than the US data. The overall change from irradiation was very similar to the US results. It is expected that the results of this study will be applied to basic research on the multiscale modeling of the irradiation embrittlement of RPV materials in Korea.

• 한국해양공학회지
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• 제2권1호
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• pp.150-162
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• 1988

The dynamic fracture toughness, $K_{Id}$,is measured in the heat-treated and ion-nitrided Cr-Mo, Ni-Cr-Mo steel using standard and Precracked Charpy specimens an imstrumented impact machine. The value of $K_{Id}$and both the energy of initiate fracture, and the total energy of fracture. Since the $K_{Id}$values of the precraked impact specimens are in accord with their theoretical ones, this testing method is sufficently practical. The effect of ion-nitriding are found to be larger than the heat-treaded specimen.

• 대한기계학회논문집A
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• 제24권2호
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• pp.303-310
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• 2000

Fracture toughness of five different reactor pressure vessel steels was characterized in the transition temperature region by the ASTM E1921-97 standard method using Charpy-sized small specimens. T he predominant fracture mode of the tested steels was transgranular cleavage in the test conditions. A statistical analysis based on the Weibull distribution was applied to the interpretation of the scattered fracture toughness data. The size-dependence of the measured fracture toughness values was also well predicted by means of the Weibull probabilistic analysis. The measured fracture toughness transition curves followed the temperature-dependence of the ASTM master curve within the expected scatter bands. Therefore, the fracture toughness characteristics in the transition region could be described by a single parameter, so-called the reference temperature (T。), for a given steel. The determined reference temperatures of the tested materials could not be correlated with the conventional index temperatures from Charpy impact tests.