The purpose of this study was to confirm the formation of hybrid layer and resin tags in dentin tissue and the possibility of bonding between luting cements used for the prosthesis and the resinous surface coated with resin bonding agents to prevent the dentin hypersensitivity after abutment preparation. Some resin bonding agents, which may have the possibility of bonding with polyacrylic acid as a liquid ingredient of polycarboxylate and glass ionomer cements, were selected. All-Blond desensitizer containing NTG-GMA and BPDM, Scotch-Bond Multipurpose plus containing HEMA, and XR-bond containing organophosphate were selected as a coating agent. Dental cements were zinc phosphate, polycarboxylate, and glass ionomer cement. After the exposed dentin surface of premolars was ethced with 10% phosphoric acid and coated with resin bonding agents, the morphology of treated surfaces and the resin tags and hybrid layers on sectioned surfaces were observed by SEM. Shear bond strength between the resin bonding agents and 3 kinds of cements was measured 24 hours after bonding. On the debonded surfaces of the shear bond strength tested specimens, the cement tags and the bonding sites between the resin materials and cements were examined by SEM. Following conclusions were drawn : 1. Coating of dentin with resin bonding agents had no effect on the shear bond strength of zinc phosphate cement. 2. Both of polycarboxylate and glass ionomer cements showed the increased shear bond strength by the dentinal coating with Scotch-Bond Multipurpose plus containing HEMA. However, in the case of dentinal coating with some agents containing NTG-GMA and BPDM or organophosphate, polycarboxylate cement exhibited the lowered shear bond strength, and glass ionomer cement showed the unchanged shear bond strength. 3. Complete obstructions of dentinal tubules were observed on the dentin coated with All-Bond desensitizer or XR-bond, but distinct shape of the orifices of dentinal tubules was observed consistently on the dentin coated with Scotch-Bond Multipurpose plus. 4. The hybrid layer was thickest on the dentin coated with All-Bond desensitizer, and the length of resin tags was longest on the dentin coated with Scotch-Bond Multipurpose plus. 3. On the debonded specimens which had been bonded with polycarboxylate cement or glass ionomer cement after coating with Scotch-Bond Multipurpose plus, the cement tags and the bonding sites between the resinous surface and the cements could be examined.
International Journal of Concrete Structures and Materials
/
v.9
no.4
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pp.391-399
/
2015
This study modeled the compressive strength and elastic modulus of hardened cement that had been treated with an expansive additive to reduce shrinkage, in order to determine the mechanical properties of the material. In hardened cement paste with an expansive additive, hydrates are generated as a result of the hydration between the cement and expansive additive. These hydrates then fill up the pores in the hardened cement. Consequently, a dense, compact structure is formed through the contact between the particles of the expansive additive and the cement, which leads to the manifestation of the strength and elastic modulus. Hence, in this study, the compressive strength and elastic modulus were modeled based on the concept of the mutual contact area of the particles, taking into consideration the extent of the cohesion between particles and the structure formation by the particles. The compressive strength of the material was modeled by considering the relationship between the porosity and the distributional probability of the weakest points, i.e., points that could lead to fracture, in the continuum. The approach used for modeling the elastic modulus considered the pore structure between the particles, which are responsible for transmitting the tensile force, along with the state of compaction of the hydration products, as described by the coefficient of the effective radius. The results of an experimental verification of the model showed that the values predicted by the model correlated closely with the experimental values.
İzmir Bay reserves high amount of residual alluvial deposits generated by Meles River at its stream mouth. These carried sediments with high water content and low bearing capacity are unsuitable in terms of engineering purposes. In-situ soil stabilization with deep soil mixing method is considered to improve properties of soil in this location. This method is widely used especially over Scandinavia, Japan and North America. Basically, the method covers mixing appropriate binder into the soil to improve soil profile according to the engineering needs. For this purpose, soil samples were initially provided from the site, classification tests were performed and optimum ratios of lime and cement binders were determined. Following, specimens representing the in-situ soil conditions were prepared and cured to be able to determine their engineering properties. Unconfined compression tests and vane shear tests were applied to evaluate the stabilization performance of binders on samples with different curing periods. Scanning electron microscope was used to observe time-dependent bonding progress of binders in order to validate the results. Utilization of 4% lime and 4% cement mixture for the long-term performance and 8% lime and 8% cement mixture for short term performance were suggested for the stabilization of Meles Delta soils. Development of CSH and CAH in a gel form as well as CSH crystals were clearly observed on SEM images of treated specimens.
An endodontically treated tooth is likely to be brittle than a vital tooth. Internal structure of the tooth has been weakened due to a significant removal of dentin by coronal access, canal preparation. There are many controversies concerning with various methods of reinforcing an intact anterior tooth that has endodontic treatment. In this experiment, 128 extracted maxillary anterior teeth were endodontically treated, and prepared with 4 methods of restorations; Composite resin filling with zinc phosphate cement, composite resin filling without zinc phosphate cement, composite resin filling with post, and metal crown with post. An Instron testing machine was used to measure the fracture loads of the specimens. The means of the failure loads for the 4 groups were compared by F-test statistically and the failure modes were observed. The results were as follows; 1. There were no statistically significant difference between the failure loads of the four methods of restoration. 2. Teeth without post were fractured in a horizontal or oblique plane through upper or middle third of the root. 3. In the posted teeth, fractures were occurred around the post. 4. In the metal crowned teeth with post, the fracture were occurred around the post or coronal area.
Objectives: The aim of the study was to evaluate the clinical and radiographic success of the Hall technique (HT) and atraumatic restorative treatment (ART) restorations using high-viscosity glass-ionomer cement for the management of occlusal carious lesions in primary molars. Materials and Methods: This randomized clinical study observed 40 children (aged 5-6 years). For each child, one tooth was treated with HT and one with ART. The primary outcome measures for HT restorations were successful, minor, and major failure rates. Clinical evaluations of ART restorations were performed according to the modified United States Public Health Service criteria during 18-month follow-up. McNemar test was used for statistical analysis. Results: Thirty of 40 (75%) participants returned for 18 months of follow-up. In the clinical evaluations of teeth that were treated with HT, the patients did not have complaints of pain or other symptoms, all crowns remained in the oral cavity, the gums were healthy, and the teeth were functional in all evaluations. At the end of the 18-month follow-up, the surface texture and marginal integrity criteria of ART restorations were recorded as 26.7% and 33.3%, respectively. In the radiographic evaluation of 30 patients treated with ART and HT, all restorations were considered successful. Conclusions: The 18-month clinical and radiographic results after treatments applied to single-surface cavities in anxious children showed that both treatment methods were successful.
Soilcrete has been a traditional material for pavement and soft ground improvement techniques. However, since the durability is not excellent and the quality is not consistent, it has not been used for various purposes up to date. However, with the increase of naturally oriented needs for light traffic roads such as pedestrian roads of garden, golf courses and sidewalks, the cases of the high strength soilcrete paving have been increased lately. This study aims at making a reference table of mix design in accordance with the required design specifications fur the high strength soilcrete admixtured with the pozzolanic cement by using a statistical experimental method. The treated soil is the clay which is widely found in Korea. As the results of this study, we could derive an effective reference mix design table for the clay treated with the pozzolanic cement stabilizer in accordance with the compressive strength of $50~150kg/cm^2$ soilcrete.
Yoon, Gil Lim;Bae, Yoon Shin;Yoon, Yeo Won;Kim, Suk Hyun
KSCE Journal of Civil and Environmental Engineering Research
/
v.30
no.2C
/
pp.119-131
/
2010
In this study, beneficial use of ocean contaminated sediments were investigated by laboratory and environmental tests, and their prototypes were released. Dredged material from Ulsan port is used for making cement treated samples and lightweight foamed samples, and various engineering tests were performed to identify the compressibility and stress-strain behaviors. Environmental tests were also performed for the beneficial uses. The values of Cu are a little higher than the suggested standard possible for reusing dredged material and equal to the suggested standard alarming for reusing dredged material, which shows environmental harmfulness for the reuse of construction material. In addition, particle size distribution, compaction test, Atterberg limit tests, specific gravity test, and unit weight test were performed to investigate the use of landfill cover materials. The shear strengths of cement treated soils were found to be enough for reclamation works.
Procedures for treatment of molar furcation invasion defects range from open flap debridement, apically repositioned flap surgery, hemisection, tunneling or extraction, to regenerative therapies using bone grafting or guided tissue regenerative therapy, or a combination of both. Several clinical evaluations using regenerative techniques have reported the potential for osseous repair of treated furcation invasions. Regenerative treatment of maxillary molars are more difficult due to the multiple root anatomy and multiple furcation entrances therefore, purpose of this study was to evaluated histologically self-curing glass-ionomer cement and light-curing glass-ionomer cement as a barrier in the treatment of a bi-furcated maxillary premolar. Five adult beagle dogs were used in this experiment. With intrasulcular and crestal incision, mucoperiosteal flap was elevated. Following decortication with 1/2 high speed round bur, degree II furcation defect was made on maxillary third(P3), forth(P4) and fifth(P5) premolar. 2 month later experimental group were self-curing glassionomer cement and light-curing glassionomer cement. After 4, 8 weeks, the animals were sacrificed by vascular perfusion. Tissue block was excised including the tooth and prepared for light microscope with Gomori's trichrome staining. Results were as follows. 1. In all experiment group, there were not epithelial down growth and glass ionomer cement were encapsulated connective tissue. 2. In 4 weeks experiment I group slighly infiltrated inflammatory cells but not disturb the new bone or new cementum formation. 3. In 8 weeks, experiment groups I, II were encapsulated fine connective tissue. 4. Therefore glass-ionomer cement filling to the grade III maxillary furcations with multiple root anatomy and multiple furcation entrances were possible clinical methods and this technique is useful method for Maxillary furcation involvement.
Park, Chan;Yoo, Seung-Hwan;Park, Sang-Won;Yun, Kwi-Dug;Ji, Min-Kyung;Shin, Jin-Ho;Lim, Hyun-Pil
The Journal of Advanced Prosthodontics
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v.9
no.2
/
pp.118-123
/
2017
PURPOSE. To investigate the effect of non-thermal atmospheric pressure plasma (NTAPP) treatment on shear bond strength (SBS) between resin cement and colored zirconia made with metal chlorides. MATERIALS AND METHODS. 60 zirconia specimens were divided into 3 groups using coloring liquid. Each group was divided again into 2 sub-groups using plasma treatment; the experimental group was treated with plasma, and the control group was untreated. The sub-groups were: N (non-colored), C (0.1 wt% aqueous chromium chloride solution), M (0.1 wt% aqueous molybdenum chloride solution), NP (non-colored with plasma), CP (0.1 wt% aqueous chromium chloride solution with plasma), and MP (0.1 wt% aqueous molybdenum chloride solution with plasma). Composite resin cylinders were bonded to zirconia specimens with MDP-based resin cement, and SBS was measured using a universal testing machine. All data was analyzed statistically using a 2-way ANOVA test and a Tukey test. RESULTS. SBS significantly increased when specimens were treated with NTAPP regardless of coloring (P<.001). Colored zirconia containing molybdenum showed the highest value of SBS, regardless of NTAPP. The molybdenum group showed the highest SBS, whereas the chromium group showed the lowest. CONCLUSION. NTAPP may increase the SBS of colored zirconia and resin cement. The NTAPP effect on SBS is not influenced by the presence of zirconia coloring.
The practical usage of underground space and demand for vehicular tunnels necessitate the construction of non-circular wide rectangular tunnels. However, constructing large tunnels in soft clayey soil conditions with no ground improvement can lead to excessive ground deformations and collapse. In recent years, in situ ground improvement techniques such as jet grouting and deep cement mixing are often utilized to perform cement-stabilisation around the tunnel boundary to prevent large deformations and failure. This paper discusses the stability characteristics and failure behaviour of a wide rectangular tunnel in cement-treated soft clays. First, the plane strain finite element model is developed and validated with the results of centrifuge model tests available in the past literature. The critical tunnel support pressures computed from the numerical study are found to be in good agreement with those of centrifuge model tests. The influence of varying strength and thickness of improved soil surround, and cover depth are studied on the stability and failure modes of a rectangular tunnel. It is observed that the failure behaviour of the tunnel in improved soil surround depends on the ratio of the strength of improved soil surround to the strength of surrounding soil, i.e., qui/qus, rather than just qui. For low qui/qus ratios,the stability increases with the cover; however, for the high strength improved soil surrounds with qui >> qus, the stability decreases with the cover. The failure chart, modified stability equation, and stability chart are also proposed as preliminary design guidelines for constructing rectangular tunnels in the improved soil surrounded by soft clays.
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