• 한국결정성장학회지
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• 제15권5호
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• pp.202-207
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• 2005

Kaolin과 규석 및 $Mg(OH)_2$등의 원료로 만들어진 slip을 casting 할 때 slip의 점도가 slip casting 속도와 소결체의 미세조직에 미치는 영향을 보면 slip-casting속도는 slip의 점도가 낮을 경우 감소하였으며 slip의 점도범위는 $3.0\~17.0\;cP$가 적당하였다. Slip의 점도를 조절하면 표면층, 표면 내부층, 중간층, 내면층의 미세조직을 비교적 균일하게 casting 할 수 있다 소성온도 $1350^{\circ}C$에서 시편의 구성광물은 cordierite 결정만으로 되어있었다.

• 한국세라믹학회지
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• 제31권12호
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• pp.1467-1474
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• 1994

The effects of the dispersion, drying, and binder burning-out on the green-microstructures of gelcasted alumina were studied. The slip consisting of 55 vol% alumina powder and 5 wt% organic materials was well-dispersed by adding 0.28 wt% polyelectrolyte polymer. Green bodies were dried at >85% relative humidity at room temperature. Green-microstructures were observed to be depended on the heating rate during binder burnout. Constant drying rate was not observed in drying process of gelcasted alumina. Sintered body showed its relative density higher than 99% when it was sintered at 1$600^{\circ}C$ for 2 hours.

• 한국세라믹학회지
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• 제48권5호
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• pp.348-353
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• 2011

By gel-casting, the silicon-polymer green bodies were prepared for silicon nitride ceramics, sintered by microwave gas phase reaction. Considering the viscosity and the idle time of slurries, we decided the operational conditions of related processes, and the optimum concentrations of raw materials powders, organic monomers, cross-linker, dispersant, initiator, and catalyst. So we could get the machinable green bodies, having about 50 MPa of bending strength without cracks by selecting drying conditions carefully.

• 한국세라믹학회지
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• 제31권6호
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• pp.595-600
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• 1994

Ni0.3Zn0.7Fe2O4 ferrite specimens were fabricated by dry pressing and tape casting method. The properties of each specimen were measured and compared. In order to design and manufacture the chip devices effectively, one important criterion can be that the sintered density of the laminated body should approach close to that of the dry pressed body which is regarded as standard. This requirement could be satisfied by controlling the solid loading of the ferrite sheet, lamination temperature and pressure. Using the optimum conditions (solid loading 55 wt%, lamination temperature 6$0^{\circ}C$, lamination pressure 400 kg/$\textrm{cm}^2$, sintered at 125$0^{\circ}C$ 2h) a sintered ferrite, with the density of 5.18g/㎤ and permeability of 1390 at 0.5 MHz, were obtained.

• 대한치과기공학회지
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• 제21권1호
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• pp.87-96
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• 1999

In order to examine the influence of sprue(used to make crown supplements) on casting, 3 kinds of sprue materials(wax, wood, plastic) and 3 types of sprue(round, square, triangle) were made and buried and cast, then the comparison and analysis of casting characters among sprue materials and among sprue type show the following results : 1. The comparison of casting characters in accordance with sprue materials shows wax sprue of 83.3%, wood sprue 81.3%, and plastic sprue of 80.7%, Wax sprue was the bast materials for casting, However there was no statistically significant difference of casting characters among was, plastic and wood. 2. The comparison of casting in accordance with sprue types shows square sprue of 94.0%, round sprue of 86.9% and triangle sprue of 84.2%. square sprue had a best casting character. 3. When a ring cast using wood sprue was classified from burying materials. its cutting of casting body and sprue indicated much more than any other sprue material. It seems to be caused by the influence of wood residuals and carbon occurrence.

• 한국세라믹학회지
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• 제34권5호
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• pp.528-534
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• 1997

There have been many studies on the preparation of slip, forming and drying in the slip casting process. However, is has not been yet on the rheological properties of consolidated body which largely affect on the workability. It was investugated that the rheological properties of the consolidated bodies formed by slip casting in the form of cakes from well dispersed(slip C) and weakly agglomerated slip(slip B) in the clay and clay-fly ash systems. The state of dispersion of slip was found to affected the critical moisture content which was largely affected by the pore and moisture distribution of the consolidated body. The cake C show lower critical moisture content than cake B in the clay system. However, the cake B gives lower critical moisture content than cake C in the clay-fly ash system.

• 한국세라믹학회지
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• 제52권6호
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• pp.449-454
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• 2015

The fabrication process of zirconia gel-casting was studied to obtain dense zirconia on a large scale or with complicated shapes. As an experimental parameter, two different particle sizes ($0.1{\mu}m$ and $0.7{\mu}m$) of zirconia powder were applied to the gel-casting process. The viscosity behavior of slurries incorporating 40 vol% of zirconia powder was examined as a function of the dispersant content and the solid load to determine the optimum dispersion conditions. In addition, the gelation time with an initiator, the de-binding behavior, and the main factors affecting densification were examined. The densification of the gel-casted zirconia green body depended on the mixing ratio between the monomer and the dimer and on the zirconia particle size. A green body with a small particle size of $0.1{\mu}m$ showed less densification, with a relative density of 93%. This may be due to the excess number of bubbles created through interactions between the larger particle surface and polymer additives during the ball-milling process.

• 한국세라믹학회지
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• 제55권4호
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• pp.352-357
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• 2018

The slip casting process is widely used to make green bodies from ceramic slips into dense compacts with homogeneous microstructure. However, stress may be generated inside the green body during drying, and can lead to cracking and bending during sintering. When starting from the spherical powders with mono-size distribution to make the close packed body, interstitial voids on octahedral and tetrahedral sites are formed. In this research, experiments were carried out with powders of three size types (host powder (H), octahedral void filling powder (O) and tetrahedral void filling powder (T)) controlled for average particle size by milling from two commercial alumina powders. Slips were prepared using three different powder batches from H only, H+O or H+O+T mixed powders. After manufacturing green compacts by solid-casting, compacts were dried at constant temperature and humidity and sintered at $1650^{\circ}C$. Alumina samples fabricated from the multi-sized powder mixture had improved compacted and sintered densities.

• 한국세라믹학회지
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• 제49권6호
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• pp.592-600
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• 2012

Conventional methods for preparing ceramic bodies, such as cold isostatic pressing, gypsum-mold slip casting, and filter pressing are not completely suitable for fabricating large and thick ceramic plates owing to disadvantages of these processes, such as the high cost of the equipment, the formation of density gradients, and differential shrinkage during drying. These problems can be avoided by employing a pressure-vacuum hybrid slip casting approach that considers not only by the compression of the aqueous slip in the casting room (pressure slip casting) but also the vacuum sucking of the dispersion medium (water) around the mold (vacuum slip casting). We prepared the alumina formed bodies by means of pressure-vacuum hybrid slip casting with stepwise pressure loading up to 0.5 MPa using a slip consisting of 40 vol% solid, 0.6 wt% APC, 1 wt% PEG, and 1 wt% PVA. After drying the green body at $30^{\circ}C$ and 80% RH, the green density of the alumina bodies was about 56% RD. The sintered density of an alumina plate created by means of sintering at $1650^{\circ}C$ for 4 h exceeded 99.8%.This method enabled us to fabricate a $110{\times}110{\times}20$ mm alumina plate without cracks and with a homogeneous density, thus demonstrating the possibility of extending the method to the fabrication of other ceramic products.

• 한국재료학회지
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• 제11권6호
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• pp.465-471
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• 2001

수용성 매체에서 젤-케스팅 공정을 이용하여 용융실리카를 기본으로 하는 다성분계 세라믹 코어 (中子)를 제조하고, 소결조건에 따른 제반 기계적 물성과 알칼리 부식용액에 의한 용출특성을 고찰하였다. 1000cP (at $50sec^{-1}$ ) 이하의 낮은 점도를 갖는 50vol%의 고농도 다성분계 세라믹 슬림의 제조가 가능하였다. 성형체는 안정화시킨 슬림을 몰드에 부어 상온에서 겔화시킨 후 $25^{\circ}C$, 80% 상대습도 분위기 하에서 48시간동안 건조시켜 제조하였으며 건조된 성형체에는 균열이 발생하지 않았다. 세라믹 코어 성형체의 소결온도가 상승할 수록 상온강도, 겉보기 밀도, 수축률은 시편의 기공도와 역비례하여 증가하였다. 세라믹 코어 소결체의 용출속도는 동일한 온도에서 알칼리 부식용액의 농도에 의존하였으며, 소결체의 기공도가 클수록 증가하였다.