• Title/Summary/Keyword: carbon composites

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A Study on Characterization for Stacking Fault Evaluation of CFRP Composite Laminates Using an EMAT Ultrasonics (전자기 초음파를 이용한 CFRP 복합적층판의 적층배향 특성평가에 관한 연구)

  • Im, Kwang-Hee;Na, Seung-Woo;Kim, Ji-Hoon;Lee, Chang-Ro;Hsu, David K.;Yang, In-Young
    • Transactions of the Korean Society of Automotive Engineers
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    • v.13 no.2
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    • pp.83-92
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    • 2005
  • An electromagnetic acoustic transducer (EMAT) is a unique probe that does not require a couplant or gel and also can usually generate or detect an ultrasonic wave into specimens across a small gap. It, therefore can be applied in a noncontact mode with a high degree of reproducibility. Especially stiffness of composites depends on layup sequence of CFRP(carbon fiber reinforced plastics) laminates. It is very important to evaluate the layup errors in prepreg laminates. A nondestructive technique can therefore serve as a useful measurement for detecting layup errors. This shear wave for detecting the presence of the errors is very sensitive. A decomposition model has been used in the interpretation and prediction of test results. Test results have been com pared with model data. It is found that the high probability shows between tests and the model utilized in characterizing cured layups of the laminates. Also a C-scan method was used for detecting layup of the laminates because of extracting fiber orientation information from the ultrasonic reflection caused by structural imperfections in the laminates. Therefore, it was found that interface C-scan images show the fiber orientation information by using two-dimensional fast Fourier transform (2-D FFT).

An Experimental Evaluation of Mechanical Properties and Failure Processing in Composite Laminate (복합재료의 기계적 성질 및 파손과정 평가)

  • J.W.,Ong;K.H.,Song;R.W.,Sung;B.S.,Shim
    • Bulletin of the Society of Naval Architects of Korea
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    • v.25 no.4
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    • pp.58-68
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    • 1988
  • This paper is concerned with mechanical properties of unidirectional laminate $[(0^{\circ})_{8T},\;(90^{\circ})_{8T}]$, composed of angle plies $[({\pm}15^{\circ})_{2S},\;({\pm}30^{\circ})_{2S},\;({\pm}45^{\circ})_{2S},\;({\pm}60^{\circ})_{2S},\;({\pm}75^{\circ})_{2S}$ and laminate $[(9^{\circ}/90^{\circ})_{2S},\;(90^{\circ}/{\pm}45^{\circ}/0^{\circ})_S,\;({\pm}45^{\circ}/0^{\circ}/{\pm}90^{\circ})_S,\;({\pm}45^{\circ}/90^{\circ}/0^{\circ})_S,\;(0^{\circ}/90^{\circ}/{\pm}45^{\circ})_S,\;(90^{\circ}/0^{\circ}/{\pm}45^{\circ})_S]$ under the condition of uniform strain tension. Also, experimental investigation was conducted $[10]_{8T}$, off-axis tensile test for intralaminar shear characterization. The experimental data on the failure criterion of tensor polynomial were compared with those from the classical laminate theory. Acoustic Emission experiments have been carried out to investigate the changes of the amplitude distributions of Acoustic Emission monitored during failure of tensile tests on Carbon/Epoxy composites.

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Preparation and Properties of Modified Silicon-containing Arylacetylene Resin with Bispropargyl Ether

  • Zhang, Jian;Huang, Jianxiang;Yu, Xiaojiao;Wang, Canfeng;Huang, Farong;Du, Lei
    • Bulletin of the Korean Chemical Society
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    • v.33 no.11
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    • pp.3706-3710
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    • 2012
  • A novel silicon-containing arylacetylene resin (MSAR) modified by dipropargyl ether of bisphenol A (DPBPA) and dipropargyl ether of perfluorobisphenol A (DPPFBPA) was prepared separately. The curing behaviors of modified resins, DPBPA/MSAR and DPPFBPA/MSAR, were characterized with differential scanning calorimeter (DSC). The kinetic parameters of modified resins were obtained by the Kissinger and Ozawa methods. The results of dynamic mechanical analysis (DMA) revealed that the glass transition temperature ($T_g$) of the cured DPBPA/MSAR reached $486^{\circ}C$. According to the thermogravimetric analysis (TGA), the decomposition temperature ($T_{d5}$) of the cured resins and char yield ($Y_c$, $800^{\circ}C$) decreased as the dipropargyl ether loadings increased, especially in air. With the same weight loading, thermal stability of DPBPA/MSAR was better than that of DPPFBPA/MSAR. The carbon fiber (T300) reinforced composites exhibited excellent flexural properties at room temperature with a high property retention at $300^{\circ}C$.

Effect of Surface Film on Void Behavior in Composite Integrated Structure (표면접착필름이 복합재 일체형 구조물에서의 기공 거동에 미치는 영향)

  • Park, Dong-Cheol;Kim, Yun-Hae
    • Composites Research
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    • v.33 no.3
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    • pp.147-152
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    • 2020
  • In this study, void behavior of composite laminate by local internal pressure gradient due to structural geometry and surface film application condition was experimentally evaluated through fabrication of spar/skin integrated structure specimens. Viscosity comparison and thermal analysis for both carbon fiber prepreg and surface film were conducted and cure characteristic and rate difference were analyzed. 2 types of spar/skin integrated structural specimens were prepared based on different application condition of surface film. Subsequently, those specimens were evaluated through visual surface inspection, non-destructive and destructive inspection. In a specimen #1 with full application of surface film, low pressurized area of composite laminate created by pressure gradient of structural geometry had voids. It exhibited that voids could not be evacuated and were locked in cured laminate by the influence of pre-cured surface film with relatively faster cure rate. In a specimen #2 without surface film, it revealed that all internal voids disappeared in the cured laminate. Therefore, it is verified that surface film acts as barrier film preventing void movement and evacuation during autoclave cure.

Effect of Calcium Sulfate Dihydrate (Gypsum) on the Fundamental Properties of Slag-based Mortar (이수석고가 고로슬래그 미분말 베이스 무시멘트 모르타르의 기초물성에 미치는 영향)

  • Baek, Byung Hoon;Han, Cheon Goo
    • Journal of the Korea Institute of Building Construction
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    • v.14 no.3
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    • pp.252-258
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    • 2014
  • With the vision of 'a low carbon green develop' various industrial by-products were used as replacement of cement, in order to reduce $CO_2$ emissions from the manufacturing process of cement. Blast furnace slag is one of the industrial by-products. Due to the similar chemical compositions to ordinary Portland cement, blast furnace slag have been widely used in concrete with minimum side effects. Hence, in recent years, alkali activated slag-based composites are extensively studied by many researchers. However, the alkali activator can cause a number of problems in practice. Therefore, in this study, an alternative way of activating the slag was investigated. To activate the slag without using an alkali activator, calcium sulfate dihydrate was chosen and mixed with natural recycled fine aggregate. Fundamental properties of the slag-based mortar were tested to evaluate the effect of calcium sulfate dihydrate.

Hydration and Electrical Resistance of Cement Composites Containing MWCNTs (MWCNT가 첨가된 시멘트복합체의 수화 및 전기저항 특성)

  • Lee, Gun-Cheol;Kim, Young-Min
    • Journal of the Korea Institute of Building Construction
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    • v.20 no.1
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    • pp.11-18
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    • 2020
  • Carbon nanotubes are used in various industries with their excellent mechanical properties and electrical conductivity. In the construction industry, research is being conducted to give self-sensing capabilities to structures, but the results of experiments vary among researchers, and the analysis is insufficient. Therefore, in this study, the hydration and electrical properties of MWCNT-added cement pastes were measured. The electrical resistance values of hydration heat, porosity, Rietveld quantitative analysis, compressive strength, and distance were measured.. The heat resistance, porosity, Rietvelt quantitative analysis, compressive strength and distance were measured according to electrical resistance. Experimental results showed that the heat of hydration decreased with increasing MWCNT. XRD Rietveld quantitative analysis showed that there was no significant difference in the amount of hydration products with increasing addition rate of MWCNT. As a result of SEM analysis, the MWCNT is agglomerated by van der Waals forces, and this area is considered to be caused by voids and weak areas. The electrical resistance value decreases as the addition rate is increased, and thus may play a role for magnetic sensing in the future.

Study of Cure Kinetics of Vacuum Bag Only Prepreg Using Differential Scanning Calorimetry (시차주사열량계를 이용한 진공백 성형 프리프레그의 경화 거동 연구)

  • Hyun, Dong Keun;Lee, Byoung Eon;Shin, Do Hoon;Kim, Ji Hoon
    • Composites Research
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    • v.33 no.2
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    • pp.44-49
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    • 2020
  • The cure kinetics of carbon fiber-reinforced prepreg for Vacuum Bag Only(VBO) process was studied by differential scanning calorimetry (DSC). The total heat of reaction (ΔHtotal = 537.1 J/g) was defined by the dynamic scanning test using prepregs and isothermal scanning tests were performed at 130℃~180℃. The test results of isothermal scanning were observed that the heat of reaction was increased as the temperature elevated. The Kratz model was applied to analyze the cure kinetics of resin based on the test results. To verify the simulation model, the degree of cure from panels using different cure cycles were compared with the measurement. The simulation model showed that the error against the experimental value was less than 3.4%.

Eliminating concrete cover separation of NSM strengthened beams by CFRP end anchorage

  • Hosen, Md. Akter;Jumaat, Mohd Zamin;Islam, A.B.M. Saiful;Kamruzzaman, Mohamed;Huda, Md. Nazmul;Soeb, Mahmudur Rahman
    • Structural Engineering and Mechanics
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    • v.56 no.6
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    • pp.899-916
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    • 2015
  • Upgrading or strengthening of existing reinforced concrete (RC) infrastructure is an emerging demand nowadays. Near Surface Mounted (NSM) technique is very promising approach for flexural strengthening of RC members. However, premature failure such as concrete cover separation failure have been a main concern in utilizing this technique. In this study, U-wrap end anchorage with carbon fiber reinforced polymer (CFRP) fabrics is proposed to eliminate the concrete cover separation failure. Experimental programs were conducted to the consequence of U-wrap end anchorage on the flexurally strengthened RC beams with NSM-steel. A total of eight RC rectangular beam specimens were tested. One specimen was kept unstrengthened as a reference; three specimens were strengthened with NSM-steel bars and the remaining four specimens were strengthened with NSM-steel bars and U-wrap end anchorage using CFRP fabrics. A 3D non-linear finite element model (FEM) was developed to simulate the flexural response of the tested specimens. It is revealed that NSM-steel (with and without end-anchors) significantly improved the flexural strength; moreover decreased deflection and strains compared with reference specimen. Furthermore, NSM-steel with end anchorage strengthened specimens revealed the greater flexural strength and improve failure modes (premature to flexure) compared with the NSM-steel without end anchorage specimens. The results also ensured that the U-wrap end anchorage completely eliminate the concrete cover separation failure.

Thermo-oxidation behaviour of organic matrix composite materials at high temperatures

  • Cinquin, Jacques;Colin, Xavier;Fayolle, Bruno;Mille, Marion;Terekhina, Svetlana;Chocinski-Arnault, Laurence;Gigliotti, Marco;Grandidier, Jean-Claude;Lafarie-Frenot, Marie-Christine;Minervino, Matteo;Cluzel, Christophe;Daghia, Federica;Ladeveze, Pierre;Zhang, Fangzouh
    • Advances in aircraft and spacecraft science
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    • v.3 no.2
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    • pp.171-195
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    • 2016
  • The present paper is a review of the main activities carried out within the context of the COMPTINN' program, a joint research project founded by a FUI program (Fonds $Unifi{\acute{e}}s$ $Interminist{\acute{e}}riels$) in which four research teams focused on the thermo-oxidation behaviour of HTS-TACTIX carbon-epoxy composite at 'high' temperatures ($120^{\circ}C-180^{\circ}C$). The scientific aim of the COMPTINN' program was to better identify, with a multi-scale approach, the link between the physico-chemical mechanisms involved in thermo-oxidation phenomena, and to provide theoretical and numerical tools for predicting the mechanical behaviour of aged composite materials including damage onset and development.

Study for Reducement of Polymerization Time and Improvement of Stability in Manufacturing Carboxylated Styrene-butadiene Latex (카르복실화 스티렌-부타디엔 라텍스의 중합시간 단축과 안정성 개선을 위한 연구)

  • Cho, Ur-Ryong
    • Elastomers and Composites
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    • v.37 no.1
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    • pp.31-38
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    • 2002
  • Polymerization of carboxylated styrene-butadiene latex takes longer time than that of acrylic emulsion due to delocalization of radical in butadiene unit having conjugated double bond. A latex stability is the most important properties owing to use intact without separating polymer from base latex. For reducing polymerization time without decreasing any properties of latex, carbon tetra-chloride which has been used as the most popular chain transfer agent was replaced to combination of tert-dodecylmercaptane and ${\alpha}$-methylstyrene dimer. The replacement yielded reducement or 2 hr in polymerization time. In the increment step, charge amount of acrylic acid was limited to 0.3 part to restrain viscosity enhancement. Just after initial step, addition of 0.1 part acrylamide prevent polymer chain from diffusing between two region followed by giving hardness and final good adhesive force to latex particles.