• 대한금속재료학회지
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• 제48권12호
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• pp.1078-1083
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• 2010

In this study, high temperature oxidation behavior of Alloy 617 was investigated to evaluate the effect of grain size for Alloy 617. The grain size of grain-refined Alloy 617 (GR617) was reduced to $5{\mu}m$ from $71{\mu}m$ for as-received Alloy 617 (AR617) by recrystallization after cold rolling. After high temperature aging, the oxide layers of AR617 and GR617 consisted of $Cr_2O_3$ external oxide scale and $Al_2O_3$ internal oxide. The external oxide scale resulted in a Cr-depleted zone and a carbide free zone below the scale. The depth of the carbide free zone was deeply formed in GR617. On the other hand, the depth of the internal oxide layer in GR617 was shorter than that in AR617. After a 3-point bending test, crack propagation of GR617 was more restricted than that of AR617 because of the different microstructure of the internal oxide.

• Journal of Welding and Joining
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• 제33권5호
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• pp.31-34
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• 2015

Microstructure and tensile property in the weld heat-affected zone (HAZ) of austenitic Fe-Mn-Al-C low density steels were investigated through transmission electron microscopy analysis and tensile tests. The HAZ samples were prepared using Gleeble simulation with high heat input welding condition of 300 kJ/cm, and the HAZ peak temperature of $1200^{\circ}C$ was determined from differential scanning calorimetry (DSC) test. The strain- stress responses of base steels showed that the addition of V improved the tensile and yield strength by grain refinement and precipitation strengthening. Tensile strength and elongation decreased in the weld HAZ as compared to the base steel, due to grain growth, while V-added steel had a higher HAZ strength as compared than V-free steel.

• International Journal of Precision Engineering and Manufacturing
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• 제9권4호
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• pp.3-10
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• 2008

Micro-electrical discharge machining (micro-EDM) is an effective method for machining all types of conductive materials regardless of hardness. Since micro-EDM is an electro-thermal process, the energy supplied by the pulse generator is an important factor in determining the effectiveness of the process. In this study, an investigation was conducted on the micro-EDM of tungsten carbide (WC) to compare the performance of transistor and resistance/capacitance (RC) pulse generators in obtaining the best quality micro-hole. The performance was measured by the machining time, material removal rate, relative tool wear ratio, surface quality, and dimensional accuracy. The RC generator was more suited for minimizing the pulse energy, which is a requirement for fabricating micro-parts. The smaller-sized debris formed by the low-discharge energy of RC micro-EDM could be easily flushed away from the machined zone, resulting in a surface free of burrs and resolidified molten metal. The RC generator also required much less time to obtain the same quality micro-hole in WC. Therefore, RC generators are better suited for fabricating micro-structures, producing good surface quality and better dimensional accuracy than the transistor generators, despite their higher relative tool wear ratio.

• Journal of Mechanical Science and Technology
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• 제18권2호
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• pp.221-229
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• 2004

In this work, an elastic-plastic stress analysis has been conducted for silicon carbide fiber reinforced magnesium metal matrix composite beam. The composite beam has a rectangular cross section. The beam is cantilevered and is loaded by a single force at its free end. In solution, the composite beam is assumed perfectly plastic to simplify the investigation. An analytical solution is presented for the elastic-plastic regions. In order to verify the analytic solution results were compared with the finite element method. An rectangular element with nine nodes has been choosen. Composite plate is meshed into 48 elements and 228 nodes with simply supported and in-plane loading condations. Predictions of the stress distributions of the beam using finite elements were overall in good agreement with analytic values. Stress distributions of the composite beam are calculated with respect to its fiber orientation. Orientation angles of the fiber are chosen as $0^{circ},\;30^{circ},\;45^{circ},\;60^{circ}\;and\;90^{circ}$. The plastic zone expands more at the upper side of the composite beam than at the lower side for $30^{circ},\;45^{circ}\;and\;60^{circ}$ orientation angles. Residual stress components of ${\sigma}_{x}\;and \;{\tau}_{xy}$ are also found in the section of the composite beam.

• 한국재료학회지
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• 제33권2호
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• pp.77-86
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• 2023

High-temperature oxidation of a Ni-based superalloy was analyzed with samples taken from gas turbine blades, where the samples were heat-treated and thermally exposed. The effect of Cr/Ti/Al elements in the alloy on high temperature oxidation was investigated using an optical microscope, SEM/EDS, and TEM. A high-Cr/high-Ti oxide layer was formed on the blade surface under the heat-treated state considered to be the initial stage of high-temperature oxidation. In addition, a PFZ (γ' precipitate free zone) accompanied by Cr carbide of Cr₂₃C₆ and high Cr-Co phase as a kind of TCP precipitation was formed under the surface layer. Pits of several ㎛ depth containing high-Al content oxide was observed at the boundary between the oxide layer and PFZ. However, high temperature oxidation formed on the thermally exposed blade surface consisted of the following steps: ① Ti-oxide formation in the center of the oxide layer, ② Cr-oxide formation surrounding the inner oxide layer, and ③ Al-oxide formation in the pits directly under the Cr oxide layer. It is estimated that the Cr content of Ni-based superalloys improves the oxidation resistance of the alloy by forming dense oxide layer, but produced the σ or µ phase of TCP precipitation with the high-Cr component resulting in material brittleness.

• The Korean Journal of Ceramics
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• 제2권1호
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• pp.19-24
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• 1996

The phase distribution and interface chemistry by the solid-state reaction between SiC and nickel were studied at temperatures between $550 \;and\; 1250^{\circ}C$ for 0.5-100 h. The reaction with the formation of silicides and carbon was first observed above $650^{\circ}C$. At $750^{\circ}C$, as the reaction proceeded, the initially, formed $Ni_3Si_2$ layer was converted to $Ni_2$Si. The thin nickel film reacted completely with SiC after annealing at $950^{\circ}C$ for 2 h. The thermodynamically stable $Ni_2$Si is the only obsrved silicide in the reaction zone up to $1050^{\circ}C$. The formation of $Ni_2$Si layers with carbon precipitates alternated periodically with the carbon free layers. At temperatures between $950^{\circ}C$ and $1050^{\circ}C$, the typical layer sequences in the reaction zone is determined by quantitative microanalysis to be $SiC/Ni_2$$Si+C/Ni_2$$Si/Ni_2$$Si+C/…Ni_2$Si/Ni(Si)/Ni. The mechanism of the periodic band structure formation with the carbon precipitation behaviour was discussed in terms of reaction kinetics and thermodynamic considerations. The reaction kinetics is proposed to estimate the effective reaction constant from the parabolic growth of the reaction zone.

• 생태와환경
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• 제39권1호통권115호
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• pp.85-92
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• 2006

팔당호에서 대형수생식물에 의한 일차생산과 영양염류의 흡수량 등을 조사하기 위하여 2004년 8월부터 11월까지 애기부들, 줄, 갈대, 마름, 연 및 생이가래 등 6종의 우점 대형수생식물종을 선정하여 서식면적과 건중량, 원소 함량을 측정하였다. 팔당호 전체에서 6종의 대형수생식물이 서식하는 총 면적은 약 1.37 $km^2$이었고 그 중 애기부들이 팔당호 연안수역 식생면적의 46.7%를 차지하며 가장 우점하는 것으로 나타났다. 수계별로는 남한강의 대형수생식물 서식면적이 0.458 $km^2$로 가장 많았고 그다음으로는 북한강, 경안천 및 합류 수역의 순으로 나타났다. 조사대상 대형수생식물을 대상으로 식물체내 탄소, 질소, 인의 함량을 조사한 결과, 각 대형수생식물별 탄소함량은 정수식물인 줄, 애기부들 및 갈대에서 다른 생활형에 비해 높게 나타났으며 그중 특히 줄이 가장 높은 함량을 나타내었고 마름이 가장 낮았다. 대형수생식물 종별 질소 함량은 부유식물인 생이가래가 가장 높게 나타났고 정수식물인 애기부들이 가장 낮았다. 대형수생식물종별 인 함량은 마름이 가장 높았고 정수식물인 줄과 갈대가 다른 대형수생식물군보다 적은 인 함량을 보였다. 팔당호에서 대형수생식물에 의한 2004년도 연간 물질순생산량을 산정한 결과 1차생산량은 758.4 ton C ${\cdot}$ $yr^{-1}$로 나타났고, 질소의 순흡수량은 16,921 kg ${\cdot}$ $yr^{-1}$, 인의순흡수량은 1,841,0 kg P ${\cdot}$ $yr^{-1}$로 나타났다. 같은 시기에 조사된 팔당호의 물질 수지와 비교한 결과 팔당호에서 대형수생식물에 의한 1차생산량 및 물질 흡수량은 전체1차생산량 및 유입량에 비해 미미한 것으로 조사되었다.이다.원에서 오폐수처리를 통해 하천 수질이 휴양용수로서 사용하는 데에 적합하도록 충분한 차집시설과 환경 기초시설의 설치 운영이 필요할 것으로 판단된다.TEX>$K_s$값이 높고 $V_m/K_s$비율은 낮아 수게에서 질소가 저농도 일 때에는 다른 미세조류와 비교하면 경쟁력이 떨어지고 질소에 대한 기질 친화력은 약한 것으로 나타났다. 낙동강 하류지역에서 M. aeruginosa가 대발생하는 시기에 수중 영양염의 농도 변동은 M. aeruginosa의 영양생리 kinetics 특성과 잘 부합하는 것으로 나타났다.부분을 보완하기 위한 연구가 이루어져야 할 것으로 보인다. 연마방법 간에 상호 연관성이 없었다. FE-SEM관찰에서 레진전색제를 적용한 후의 표면은 모든 군에서 대체적으로 평활한 표면을 나타내었다. 4. 동일한 복합레진과 연마방법으로 처리된 군에서 레진전색제 적용 전과 후의 표면조도 값은 M1B군이 M1군보다, S1B군이 S1군보다 통계학적으로 높게 나타났으며, M4B군과 M5B군은 각각 M4군과 M5군 보다. 그리고 S5B군은 S5군 보다 통계학적으로 낮게 나타났다 (p<0.05). 본 연구를 종합하여 보면, 복합레진의 종류에 따라 표면조도의 순서는 다르게 나타났고, polyester strip 하에서 복합레진이 중합된 경우 가장 낮은 표면조도 값과 평활한 표면을 제공하였으며 전반적으로 anishing bur는 가장 높은 Ra값과 거친 표면을 제공하였다. Enhance, Astropol, carbide finishing bur로 연마한 표면은 레진전색제의 사용으로 평활한 표면을 얻을 수 있었지만, polyester strip과 Sof-Lex disc로 얻어진 표면은 레진전색제의 사용으로 표면조도의 개선이 이루어지지 않았다.^{11}C]raclopride$ PET을 이용하여 비흡연 정상인에서 흡연에 의한 도파민 유리를 영상화 및 정량화