• Title/Summary/Keyword: carbide analysis

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A Study on the TiC Coating Using Hollow Cathode Discharge Ion Plating (HCD 이온 플레이팅 방법을 이용한 TiC 코팅에 관한 연구)

  • Kim, In-Cheol;Seo, Yong-Woon;Whang, Ki-Whoong
    • Proceedings of the KIEE Conference
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    • 1991.11a
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    • pp.261-264
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    • 1991
  • Titanium carbide(TiC) films were deposited on stainless-steel sheets using HCD(Hollow Cathode Discharge) reactive ion plating. Acetylene gas was used as the reactant gas. The characteristics of TiC films were examined by X-Ray diffraction, $\alpha$-step, ESCA(Electron Spectroscopy for Chemical Analysis), and, AES(Auger Electron Spectroscopy). The results were discussed with regard to various deposition conditions(bias voltage, acetylene flow rate, temperature).

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Microstructure and Mechanical Property in the Weld Heat-affected Zone of V-added Austenitic Fe-Mn-Al-C Low Density Steels

  • Moon, Joonoh;Park, Seong-Jun
    • Journal of Welding and Joining
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    • v.33 no.5
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    • pp.31-34
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    • 2015
  • Microstructure and tensile property in the weld heat-affected zone (HAZ) of austenitic Fe-Mn-Al-C low density steels were investigated through transmission electron microscopy analysis and tensile tests. The HAZ samples were prepared using Gleeble simulation with high heat input welding condition of 300 kJ/cm, and the HAZ peak temperature of $1200^{\circ}C$ was determined from differential scanning calorimetry (DSC) test. The strain- stress responses of base steels showed that the addition of V improved the tensile and yield strength by grain refinement and precipitation strengthening. Tensile strength and elongation decreased in the weld HAZ as compared to the base steel, due to grain growth, while V-added steel had a higher HAZ strength as compared than V-free steel.

Synthesis of poly(dialkyl or monoalkyl)silanes as silicon carbide precursors for ceramic matrix composites (탄화규소 선구물질로서의 폴리(디알킬 또는 모노알킬)실란들의 합성과 세라믹 복합체 응용)

  • Lee, Gyu-Hwan
    • Analytical Science and Technology
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    • v.26 no.1
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    • pp.27-33
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    • 2013
  • Polyalkylsilanes such as poly(dialkyl)silanes and poly(monoalkyl)silanes were synthesized by sonochemical dechlorination-condensation method from (dialkyl or monoalkyl)chlorosilanes with sodium metal. Those polyalkylsilanes were analyzed for the properties such as thermal behaviors from TGA analysis and obtained ceramic yields of 10-20% for poly(dialkyl)silanes and 40-60% for poly(monoalkyl)silanes. Ceramic composite discs were prepared by the combined mixture of polyalkylsilanes and SiC powder and were tested by TGA and analyzed by SEM and XRD for the application as binder for ceramic composite precursors.

The Determination of Stress Distribution in WC-Ni Cemented Carbide Composites by Neutron Diffraction

  • Seol, Kyeongwon
    • Korean Journal of Materials Research
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    • v.5 no.2
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    • pp.232-238
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    • 1995
  • The thermal stress distribution of WC and Ni binder phases In WC-26st.%Ni and WC-6wt.%Ni composites has been investigated over the temperature range 100-900 K using a time-of-flight neutron diffractometer. To determine the stress distribution, the breadths of WC and Ni peaks in the reference powder and the composites were analyzed. The peak breadths were corrected for particle size effect using a procedure based on the integral peak breadth method of particle size-strain analysis. The result shows a broad range of strain, and thus stress, is present in the WC and Ni binder phases of the composites. The strain distribution of both phases broadens as the temperature decreases, and some fraction of total strain distribution of the WC phase remains tensile regardless of the temperature. The strain distribution of the WC phase broadens as the binder content increases, and that of Ni binder phase broadens as the binder content decreases, which means the strain distribution broadens as the absolute value of residual stress increase.

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A Study on the Design of the Prestressed Precision Cold Forging Die (예압된 정밀 냉간단조 금형설계에 관한 연구)

  • Yeo, H. T.;Choi, Y.;Hur, K. D.
    • Proceedings of the Korean Society of Precision Engineering Conference
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    • 2000.11a
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    • pp.377-380
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    • 2000
  • The dimensional accuracy of the cold forged part is depended on the elastic characteristics of the die. To obtain the high stiffness of the prestressed die, the first stress ring of the tungsten carbide material is considered. For the design, Lam 's equation is used. The design of the prestressed die has been compared with the conventional that. For the comparison, the FE-analysis using ANSYS has been performed. The results indicate that the prestressed die with the high stiffness can be obtained by the using the high stiffness material as the first stress ring.

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Oxidation Behavior of $SiC/MoSi_2$ Composites Prepared by Reaction Sintering Method (반응소결에 의하여 제조된 $SiC/MoSi_2$ 복합체의 산화 거동)

  • 양준환;한인섭;우상국;서동수
    • Journal of the Korean Ceramic Society
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    • v.31 no.12
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    • pp.1588-1598
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    • 1994
  • The SiC/MoSi2 composite materials were fabricated by infiltrating the mixture of molybdenum disilicide and metal silicon(MoSi2+Si=100) to a porous compact of silicon carbide and graphite under the vacuum atmosphere of 10-1 torr. The specimen were oxidized in dry air under 1 atm at 130$0^{\circ}C$~150$0^{\circ}C$ for 240 hours. The oxidation behavior was evaluated by the weight gain and loss per unit area of the oxidized samples. Also, SEM and XRD analysis of the oxidized surface of the samples were carried out. With increasing the MoSi2 content and oxidation temperature, the passive oxidation was found. The trend of weight gain of all samples was followed the parabolic rate law with the formation of a protective layer of cristobalite on the surface.

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The Study on Interrupted Cutting Tool Life of Cermet and CBN in Ductile Cast Iron(FCD500) (구상흑연주철(FCD500)의 단속가공에서 서멧과 CBN의 공구수명에 관한 연구)

  • Oh, Sung-Hoon
    • Journal of the Korean Society of Manufacturing Process Engineers
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    • v.11 no.5
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    • pp.8-12
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    • 2012
  • Recently, a wide range of industrial production area has a competitive advantage through cost reduction. Moreover with the development of industrial technology, base material and cutting tool help the machining technology. But most of the machining enterprises have not hold the R&D facilities and human resources. This mainly disturbs the industrial development and th increase of production efficiency. Especially in the interrupted machining process, it showed different behavior with continuous machining process. So it needs to research and develop the tool life and tool wear mechanism analysis.

A Study on the effect of cutting parameters in face turning based on the Taguchi method (다구찌 방법에 기초한 단면절삭에서 절삭파라미터 영향에 관한 연구)

  • 장성민;조명우
    • Proceedings of the Korean Society of Machine Tool Engineers Conference
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    • 2003.04a
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    • pp.111-116
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    • 2003
  • In this paper, object of experiment is to study on the effect of cutting parameters to obtain optimal surface toughness in face turning. Surface roughness is significantly important to be high quality of parts produced by turning process. For this purpose, the optimization of cutting parameters for fan Owning operation is investigated applying the Taguchi method. An orthogonal array, signal-to-noise ratio, and the analysis of variance are employed to evaluate effect of cutting parameters fir face turning. Also confirmation tests were performed to make a comparison between the results predicted from the mentioned correlations and the theoretical results. Cutting experiment is performed without cutting fluid using coated tungsten carbide inserts about workpieces of SM45C.

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Development of Grinding Dressing System by Using Inprocess Electrelytic Dressing (정밀연삭기의 전해드레싱 시스템 개발사례)

  • 김정두
    • Proceedings of the Korean Society of Machine Tool Engineers Conference
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    • 1998.03a
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    • pp.196-202
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    • 1998
  • Recently, developments in the frontier industry have brought a rapid increase in the use of brittle materials such as silicon wafer, ferrite, sintered carbide, MgO single crystal and die steel. Because of high hardness and brittleness the cracking and chipping are apt to generate in the grinding of brittle materials, but have replaced gradually the high precision grinding. In this study, the optimum system of in-process electrolytic dressing controlled by computer was developed for improving the defects, and could maintain the optimum dressing condition at all times. The control of in-process dressing was simplified using this system, was able to maintain a stable dressing current and was unrelated to the change of dressing condition according to the variation of gap and oxide layer. Therefore, the optimum in-process electrolytic dressing system was constructed and the analysis of grinding mechanism with this system was studied.

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A Characteristic study of SiC Nanowires by RF-Sputtering (RF-Sputtering 법에 의한 SiC 나노와이어의 특성연구)

  • Jeong, Chang-Gu;Kim, Tae-Gyu
    • Journal of the Korean Society for Heat Treatment
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    • v.23 no.6
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    • pp.344-349
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    • 2010
  • Silicon carbide nanowires were grown by heat treatment of the films at $1200^{\circ}C$ after amorphous SiC thin films were deposited on graphite substrate by radio frequency magnetron sputtering at $600^{\circ}C$. It was confirmed that SiC nanowires with the diameter of 20-60 nm and length of about 50nm were grown from Field Emission Scanning Election Microscope (FE-SEM) and Transmission Election Microscope (TEM) observation. The diameter of nanowires was increased as heat treatment time is increased. The nanowires were identified to ${\beta}$-SiC single crystalline from X-Ray Diffraction(XRD) analysis. It was observed from this study that deposition temperature of samples was critical to the crystallization of nanowires. On the other hand, the effect of deposition time was insignificant.