• 한국전기전자재료학회논문지
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• 제34권6호
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• pp.461-465
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• 2021

A diffusion heat treatment process for YBa₂Cu₃O_7-y bulk superconductor in a Gd₂O₃ powder was attempted. As a result of measuring the critical temperature of the superconducting bulk, there was no change in the superconducting transition temperature as the Gd particles diffused into the YBa₂Cu₃O_7-y lattice, resulting in dense microstructure. As a result of measuring the critical current, the critical current density (J_c) of the superconducting bulk having treated by the Gd thermal diffusion treatment at 0 T increased to 3×10⁴ A/cm² at 0 T, which was higher than that of the superconducting bulk without thermal diffusion treatment. The surface magnetic force of the superconducting bulk with Gd thermal diffusion treatment was observed at the center of the superconducting bulk with the maximum trapped magnetic force (Hmax) of 1.51 kG. This result means that the Gd thermal diffusion treatment contributes to improving the critical current density Jc of YBa₂Cu₃O_7-y, and it is believed that Gd particles migrating into the superconducting bulk through thermal diffusion either fill the surface pores of YBa₂Cu₃O_7-y superconductors or act as a flux pinning center.

• Carbon letters
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• 제16권3호
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• pp.135-146
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• 2015

Graphite can be classified into natural graphite from mines and artificial graphite. Due to its outstanding properties such as light weight, thermal resistance, electrical conductivity, thermal conductivity, chemical stability, and high-temperature strength, artificial graphite is used across various industries in powder form and bulk form. Artificial graphite of powder form is usually used as anode materials for secondary cells, while artificial graphite of bulk form is used in steelmaking electrode bars, nuclear reactor moderators, silicon ingots for semiconductors, and manufacturing equipment. This study defines artificial graphite as bulk graphite, and provides an overview of bulk graphite manufacturing, including isotropic and anisotropic materials, molding methods, and heat treatment.

• 약학회지
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• 제42권3호
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• pp.284-289
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• 1998

The effect of reaction condition, solvent addition and thermal treatment on the bulk density, crystallinity and chemical properties of the freeze-dried cefazohn sodium was inves tigated to prepare the cefazolin sodium powder for injection with good flowability. Crystalline cefazolin sodium powder with high untapped-bulk density (about 45%) and low compressibility (about 40%) was obtained by solvent addition to the very highly concentrated cefazohn sodium solution followed by subsequent thermal treatment before freeze-drying. The desirable solvent was low substituted alcohol such as isopropyl alcohol and anhydrous ethanol with the final concentration of about 9%. The pH adjustment and nitrogen gas purging during the reaction did not give significant effect on the chemical properties such as content, color, transmittance and pH of the reconstituted cefazolin sodium aqueous solution.

• 한국전기전자재료학회논문지
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• 제34권5호
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• pp.333-336
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• 2021

Oxide YBCO bulk superconductors are manufactured using the melt process. Because seed crystal growth method utilizes a slow-spreading layer-by-layer reaction, a long-term heat treatment is required to manufacture a single-crystal specimen of several cm. In this study, the melt process method was applied to compensate for the shortcomings of the seed crystal growth method. The thickness of the upper and lower pellets of the YBCO bulk was molded to 40 mm, and YBCO superconductor was produced by heat treatment. The measurement results of capture magnetism was in line with the literature. This results in a relationship that the higher the growth of Y211 particle in the YBCO, the higher the superconducting properties. We analyzed the YBCO superconductor, focusing on the Y₂BaCuO₅ particle distribution.

• 제어로봇시스템학회:학술대회논문집
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• 제어로봇시스템학회 1992년도 한국자동제어학술회의논문집(국내학술편); KOEX, Seoul; 19-21 Oct. 1992
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• pp.67-70
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• 1992

1930년 스웨덴에서 개발에 성공, 네덜란드에서 더욱 발전시킨 ALC(Autoclaved Light-weignt Concrete의 약칭) 는 가볍고, 견고하고, 그리고 시공이 간편한 경제적인 요건들을 충족시키는 건축자재로 세계적으로 널리 사용되고 있으며 , 국내에서는 불과 수년 전부터 연구 개발되고 있는 실정이다. ALC 란 시멘트와 규사, 생석회등 무기질 원료를 고온,고압으로 증기 양생시킨 경량의 기포 콘크리트 제품을 통칭한 것이다. ALC공정은 bulk ALC를 생산하는 batch공정과 이 bulk ALC에 대한 처리 공정으로 크게 나눌 수가 있으며 여기에서는 bulk ALC 처리 공정을 side shield treatment, anti-corrosion treatment, curing grate transferer, cutting station, curing car transportation, autoclave traveling platform, 및 packing 의 공정으로 세분하여 각 공정개요 소개 및 PLC(Programmable Logic Controller의 약칭)를 이용한 제어 system에 대하여 설명하고자 한다.

• 한국결정성장학회지
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• 제30권5호
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• pp.168-173
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• 2020

AlN의 열 산화 공정에서 발생하는 거동 및 메커니즘을 확인하기 위해 bulk AlN 단결정에 대해 대기분위기에서 온도에 따라 열처리를 수행하였다. 800℃의 온도에서 bulk AlN의 본격적인 산화 및 Al-oxide 들의 성장이 일어난 것을 확인하였고, 온도가 증가함에 따라 산소 성분의 wt%가 증가하는 반면 질소 성분의 wt%는 감소하는 경향을 보였다. 900℃에서 열처리하는 경우, 성장 된 Al-oxide은 이웃한 Al-oxide와 merging되어 α-Al₂O₃ 다결정을 형성하기 시작했다. 1000℃의 온도에서 열처리하는 동안, 육각 피라미드 형 α-Al₂O₃ 다결정이 명확히 형성되었음을 확인하였다. X-선 회절 패턴 분석을 통해 bulk AlN의 온도에 따른 표면 결정 구조의 변화를 자세히 조사하였다.

• 한국분말재료학회지
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• 제23권1호
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• pp.8-14
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• 2016

A bulk-type Ta material is fabricated using the kinetic spray process and its microstructure and physical properties are investigated. Ta powder with an angular size in the range $9-37{\mu}m$ (purity 99.95%) is sprayed on a Cu plate to form a coating layer. As a result, ~7 mm-sized bulk-type high-density material capable of being used as a sputter material is fabricated. In order to assess the physical properties of the thick coating layer at different locations, the coating material is observed at three different locations (surface, center, and interface). Furthermore, a vacuum heat treatment is applied to the coating material to reduce the variation of physical properties at different locations of the coating material and improve the density. OM, Vickers hardness test, SEM, XRD, and EBSD are implemented for analyzing the microstructure and physical properties. The fabricated Ta coating material produces porosity of 0.11~0.12%, hardness of 311~327 Hv, and minor variations at different locations. In addition, a decrease in the porosity and hardness is observed at different locations upon heat treatment.

• 한국전기전자재료학회:학술대회논문집
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• 한국전기전자재료학회 2002년도 하계학술대회 논문집 Vol.3 No.2
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• pp.743-745
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• 2002

Pyroelectric and dielectric properties of modified PZT thin film and bulk ceramics were studied. In case of bulk specimens were prepared by conventional ceramic process and thin films with same composition and (111) preferred orientation were prepared by the sol-gel process. Their crystal structure, pyroelectric and dielectric properties were investigated after poling at $150^{\circ}C$ for 30 min for bulk ceramics and no poling treatment, respectively. Dielectric constants and losses of bulk and thin film were 600, 875 and 0.028, 0.025, respectively. Pyroelectric coefficients obtained were $50nC/cm^2K$ and $30nC/cm^2K$, respectively.

• 한국결정성장학회지
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• 제26권3호
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• pp.121-125
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• 2016

The effect of temperature and pressure in the nitrogen ambient furnace on bulk micro defect (BMD) and denuded zone (Dz) is experimentally investigated. It is found that as pressure increases, Dz depth increases with a small decrease of BMD density in the range of temperature, $100{\sim}300^{\circ}C$. BMD density with hot isostatic pressure treatment (HIP) at temperature of $850^{\circ}C$ is higher than that without HIP while Dz depth is lower due to much higher BMD density. As the pressure increases, BMD density is increased and saturated to a critical value, and Dz depth increases even if BMD density is saturated. The concentration of nitrogen increases near the surface with increasing pressure, and the peak of the concentration moves closer to the surface. The nitrogen is gathered near the surface, and does not become in-diffusion to the bulk of the wafer. The silicon nitride layer near the surface prevents to inject the additional nitrogen into the bulk of the wafer across the layer. The nitrogen does not affect the formation of BMD. On the other hand, the oxygen is moved into the bulk of the wafer by increasing pressure. Dz depth from the surface is extended into the bulk because the nuclei of BMD move into the bulk of the wafer.

• 한국작물학회지
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• 제50권spc1호
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• pp.104-107
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• 2005

보리를 산물처리하는 4개 RPC에서 건조, 저장, 출하시스템등 보리 수확후 관리실태를 조사한 결과는 아래와 같았다. J RPC는 쌀보리를 S RPC는 겉보리를 처리하였으며, 운반은 S RPC는 3종, J RPC는 7종, S RPC는 3종류의 운반수단을 사용하였다. 수확 후 관리는 원료곡의 투입에서 저장까지 8단계를 사용하였으며, J RPC는 제망기, 2대의 열풍기, 냉풍기를 사용하였고, S RPC는 가열은 하지 않고 송풍만으로 건조를 하였다. 계량은 S RPC는 차량계근과 투입시 계량등으로 2회 계량하여 중량에 대한 신뢰성을 높였다. 건조방법은 S RPC는 $20\%$ 이하의 수분에서는 연료비를 절감하면서 급격한 열풍건조에 의한 품질변화를 방지하기 위하여 송풍만으로 건조하였다. J RPC는 냉풍기를 사용하여 저장중 곡온을 $19^{\circ}C$이하로 유지하여 품질의 변화를 방지하고 있었다. 처리한 물량은 J RPC는 정맥후 1, 40kg단위로 년중 출하하고 S RPC는 원료곡을 산물로 9월 말 이전에 출하를 완료하였다. 본 조사의 결론은 보리 재배맥종이나 경영방향에 적합하게 보리 수확 후 관리 특성이 차이가 있었고, 농촌인구의 고령화에 따라 쉽게 보리농사를 지을 수 있는 보리산물처리에 대한 정책지원이 더 증가하여야 할 것으로 사료되었다.