• Journal of Pharmaceutical Investigation
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• v.40 no.4
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• pp.237-244
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• 2010

This study investigated basic material properties and compressibility of commonly used pharmaceutical excipients. Five classes of excipients are selected including starch, lactose, calcium phosphate, microcrystalline cellulose (MCC), and povidone. The compressibility was evaluated using compression parameters derived from Heckel and Kawakita equation. The Heckel plot for lactose and dicalcium phosphate showed almost linear relationship. However, for MCC and povidone, curves in the initial phase of compression were observed followed by linear regions. The initial curve was considered as particle rearrangement and fragmentation and then plastic deformation at the later stages of the compression cycle. The Kawakita equation showed MCC exhibited higher compressibility, followed by povidone, lactose, and calcium phosphate. MCC undergoes significant plastic deformation during compression bringing an extremely large surface area into close contact and facilitating hydrogen bond formation between the plastically deformed, adjacent cellulose particles. Lactose compacts are consolidated by both plastic deformation and fragmentation, but to a larger extent by fragmentation. Calcium phosphate has poor binding properties because of its brittle nature. When formulating tablets, selection of suitable pharmaceutical excipients is very important and they need to have good compression properties with decent powder flowability. Material properties tested in this study might give a good guide how to select excipients for tablet formulations and help the formulation scientists design the optimum ones.

• Journal of the Korean Society of Safety
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• v.20 no.4 s.72
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• pp.14-19
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• 2005

One area in which composites have been used rather extensively is for fabricating pressure vessel. These structures can be readily manufactured by filament winding, which is, as far as composite fabrication techniques are concerned, a relatively inexpensive method for producing composite structures. Unfortunately, the higher strength material and fabrication costs are not the only disadvantages of fiber-reinforced polymer composites when they are compared to metals. Additionally, these materials tend to exhibit brittle behavior. This is of particular concern when they are subjected to a low-velocity impact during routine handling a significant amount of structural damage can be introduced into the composites. The goals of this paper are to understand the impact damage behavior and identify the effect of surface coating materials on impact resistance in filament wound composite pressure vessels. For these, a series of low velocity impact tests was performed on specimens cutting from the full scale pressure vessel by the instrumented impact testing machine. The specimens are classified into two types with and without surface protective material. The visualization for impact damage is made by metallurgical microscope. Based on the impact force history and damage, the resistance parameters were employed and its validity in identifying the damage resistance of pressure vessel was reviewed. As the results, the impact resistance of the filament wound composites and its dependency on the protective material were evaluated quantitatively.

• Steel and Composite Structures
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• v.25 no.6
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• pp.639-648
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• 2017

Fracture energy values KV have been measured on cast steel, used in the container manufacture, by instrumented Charpy impact testing. This material has a large ductility on the upper transition region at $+20^{\circ}C$ and a ductile tearing with an expended plasticity before a brittle fracture on the lower transition region at $-20^{\circ}C$. To assess the fracture toughness of this material we use, the $K_{IC}$-KV correlations to measure the critical stress intensity factor $K_{IC}$ on the lower transition region and the dynamic force - displacement curves to measure the critical fracture toughness $J{\rho}_C$, the essential work of fracture ${\Gamma}_e$ on the upper transition region. It is found, using the $K_{IC}$-KV correlations, that the critical stress intensity factor $K_{IC}$ remains significant, on the lower transition region, which indicating that our testing material preserves his ductility at low temperature and it is apt to be used as a container's material. It is, also, found that the $J_{\rho}-{\rho}$ energetic criterion, used on the upper transition region, gives a good evaluation of the fracture toughness closest to those found in the literature. Finally, we show, by using the ${\Gamma}_e-K_{IC}$ relation, on the lower transition region, that the essential work of fracture is not suitable for the toughness measurement because the strong scatter of the experimental data. To complete this study by a numerical approach we used the ANSYS code to determine the critical fracture toughness $J_{ANSYS}$ on the upper transition region.

• Transactions of Materials Processing
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• v.27 no.6
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• pp.370-378
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• 2018

Cold forging, carried out at room temperature, leads to high dimensional accuracy and excellent surface integrity as compared to other forging methods such as warm and hot forgings. In the cold forging process, WC-Co (Tungsten Carbide-Cobalt) alloy is the mainly used material as a core dies because of its superior hardness and strength as compared to other structural materials. For cold forging, die life is the most significant factor because it is directly related to the manufacturing cost due to periodic die replacement in mass production. To investigate die life of WC-Co alloy for cold forging, mechanical properties such as strength and fatigue are essentially necessary. Generally, uniaxial tensile test and fatigue test are the most efficient and simplest testing method. However, uniaxial tension is not efficiently application to WC-Co alloy because of its sensitivity to alignment of the specimen due to its brittleness and difficulty in thread machining. In this study, shape of specimen, tools, and testing methods, which are appropriate for uniaxial tensile test for WC-Co alloy, are proposed. The test results such as Young's modulus, tensile strength and stress-strain curves are compared to those in previous literature to validate the proposed testing methods. Based on the validation of test results it was concluded that the newly developed testing method is applicable to other cemented carbides like Titanium carbides with high strength and brittleness, and also can be utilized to carry out fatigue tests for further investigation on die life of cold forging.

• Journal of the Korean Academy of Esthetic Dentistry
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• v.25 no.2
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• pp.98-108
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• 2016

In recent days, perhaps the biggest driver in new material development is the desire to improve restorations esthetics compared to the traditional metal substructure based ceramics or all-ceramic restorations. Each material type performs differently regarding strength, toughness, effectiveness of machining and the final preparation of the material prior to placement. For example, glass ceramics are typically weaker materials which limits its use to single-unit restorations. On the other hand, zirconia has a high fracture toughness which enables multi-unit restorations. This material requires a long time sintering procedure which excludes its use for fast chair side production. Hybrid ceramic material developed for CAD/CAM system is contained improved nano ceramic elements. This new material, called a Resin Nano Hybrid Ceramic is unique in durability of function and aesthetic base compositions. The new nano-hybrid ceramic material is not a composite resin. It is also not a pure ceramic. The material is a mixture of both and consists of nano-ceramic fillers. Like a composite, the material is not brittle and is fracture resistant. Like a glass ceramic, the material has excellent polish retention for lasting esthetics. The material is easily machined by chair side or in a dental lab side, could be an useful restorative option.

• Journal of the Computational Structural Engineering Institute of Korea
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• v.28 no.3
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• pp.301-307
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• 2015

A bond-based peridynamic model has been shown to be capable of analyzing many of dynamic brittle fracture phenomena. However, there have been issued limitations on handling constitutive models of various materials. Especially, it assumes bonds act independently of each other, so that Poisson's ratio for 3D model is fixed as 1/4 as well as taking only account the bond stretching results in a volume change not a shear change. In this paper a state-based peridynamic model of dynamic brittle fracture is presented. The state-based peridynamic model is a generalized peridynamic model that is able to directly use a constitutive model from the standard theory. It permits the response of a material at a point to depend collectively on the deformation of all bonds connected to the point. Thus, the volume and shear changes of the material can be reproduced by the state-based peridynamic theory. For a linearly elastic solid, a plane stress model is introduced and the damage model suitable for the state-based peridynamic model is discussed. Through a convergence study under decreasing the peridynamic nonlocal region($\delta$-convergence), the dynamic fracture model is verified. It is also shown that the state-based peridynamic model is reliable for modeling dynamic crack propagatoin.

• Journal of the Korea Academia-Industrial cooperation Society
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• v.22 no.4
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• pp.396-402
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• 2021

A cross section in RC flexural members must be designed to satisfy flexural strength and ductility requirements simultaneously. In design provisions, ductile behavior is ensured by a sufficient reinforcement ratio or depth of the neutral axis. If the reinforcement ratio is less than the balanced reinforcement ratio, ductile behavior is secured, and this value is theoretically the maximum reinforcement ratio. But for a cross section with less steel, brittle failure can occur regardless of ductile behavior because of unqualifying a cracking moment. Recently, designs with a minimum steel ratio have been increasing along with the use of high-strength material, so in design provisions, a minimum amount of reinforcement is suggested. In the KCI(2012) standard, a minimum amount of reinforcement was suggested in terms of strength of steel and concrete. But in the revised KCI(2017) standard, a minimum amount of reinforcement was suggested by a relationship between the design flexural strength and cracking moment indirectly. This code can reflect the effect of cover thickness, but a material model must be defined. Therefore, the minimum amount of reinforcement in KCI(2012) and KCI(2017) was examined, and a rational review method was studied by parametric analysis.

• Journal of the Korea institute for structural maintenance and inspection
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• v.27 no.1
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• pp.78-85
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• 2023

This study evaluates the performance of reinforced concrete columns using hybrid fiber sheets for structural behavior. The purpose of this method is to improve the load-bearing capacity of the reinforced structure by impregnating a hybrid fiber sheet, which is woven by arranging aramid and glass fibers uniaxially and attached to an aged concrete structure requiring reinforcement with epoxy. In particular, not only the weight reduction of the material obtained by using a fiber lighter than the steel material, but also the low-strength, high-toughness fiber element among the fibers used delays the brittle fracture of the high-strength, low-toughness fiber element. The low-strength, high-toughness fiber element among the fibers used delays the brittle fracture of the high-strength, low-toughness fiber element, resulting in weight reduction compared to steel. The study conducted structural tests on four specimens, with the hybrid reinforcement method and failure mode as main variables. Specimen size and loading conditions were chosen to be comparable with previous studies. The structural performance of the specimen was evaluated using energy dissipation capacity and ductility. Analysis shows that excellent results can be obtained with the hybrid fiber sheet reinforcement.

• KIEAE Journal
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• v.15 no.1
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• pp.139-146
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• 2015

This is an experimental study on the engineering characteristics of perforated reinforced concrete beams with shells. In the material matter of this study, the water cement ratio put 60%, the ratio of substitution of oyster shells to fine aggregate 30%. And in the structural matter, the form of opening put circle and square, the size of opening as the radius and the length of it changed from one to three times of the beam depth with a change presence and absence of reinforced steel around opening. All thirteen reinforced concrete beam tests composed one standard beam and twelve six beams with the circle and square opening were tested in shear strength under two points loading and compared and analyzed the characteristics of test beams under the same conditions one another. The results of the study showed as followed. 1) The initial crack load value of the opening test beams is similar the standard beam but the maximum load value decreased with increase in proportion of the opening size, in the square opening than the circle opening and in the absence than the presence of reinforced steel. 2) As the difference between the circle opening and the square opening beams is represented 2.17~9.8% in the maximum load value and the load capacity of the square opening suddenly decrease than it of the circle opening, it is judged because of the shortage of concrete section, the concentration of the stress in the corner of the square opening and material influence of shell substitution. 3) The failure figure such as the pattern of the crack and so on is represented brittle failure as the opening size is the bigger and the ratio of substitution is higher because of the lack material properties.

• International Journal of Highway Engineering
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• v.17 no.4
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• pp.53-61
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• 2015

PURPOSES : The objective of this study is to evaluate the SDAR (solvent deasphaltene residue), which is obtained from the solvent deasphalting (SDA) process, as a pavement material. METHODS : The physical properties of the SDAR were evaluated based on its chemical composition, and asphalt mixtures with the SDAR were fabricated and used for the evaluation of mechanical properties. Firstly, the chemical composition of SARA (saturate, aromatic, resin and asphaltene) was analyzed using the TLC-FID (thin-layer chromatography-flame ionization detector). Moreover, the basic material properties of the asphalt binder with the SDAR were evaluated by the penetration test, softening point test, ductility test, and PG (performance grade) grade test. The rheological properties of the asphalt binder with the SDAR were evaluated by the dynamic shear modulus ($G^*$) obtained using the time-temperature superposition (TTS) principle. Secondly, the mechanical properties of the asphalt mixtures with the SDAR were evaluated. The compactibility was evaluated using the gyratory compacter. Moreover, the tensile strength ratio (TSR) was used for evaluating the moisture susceptibility of the asphalt mixtures (i.e., susceptibility to pothole damage). The dynamic modulus $E^*$, which is a fundamental property of the asphalt mixture, obtained at different temperatures and loading cycles, was used to evaluate the mechanical properties of the asphalt mixtures. RESULTS AND CONCLUSION : The SDAR shows stiffer and more brittle behavior than the conventional asphalt binder. As the application of the SDAR directly in the field may cause early failures, such as cracks on pavements, it should be applied with modifiers that can favorably modify the brittleness property of the SDAR. Therefore, if appropriate additives are applied on the SDAR, it can be used as a pavement material because of its low cost and strong resistance to rutting.