• 제목/요약/키워드: bonding glass

검색결과 429건 처리시간 0.021초

In-Ceram 코아의 표면처리 방법에 따른 레진 시멘트와의 결함강도 및 표면상태에 관한 연구 (STDUY ON THE SURFACE MORPHOLOGE AND SHEAR BOND STRENGTH OF IN-CERAM CORE TO RESIN CEMENT AFTER VARING MODES OF SURFACE CONDITIONING)

  • 김영숙;우이형;임호남;최부병
    • 대한치과보철학회지
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    • 제33권4호
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    • pp.693-704
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    • 1995
  • This study was performed to evaluate effective surface conditioning method of In-Ceram core to improve bonding with resin cement. The surface of each sample was avraded with glass bead for 20 seconds and then subjected to one of the following conditions : no modification, sandblasting with $50{\mu}m$ slumimum oxide powders for 20 seconds, etching with 20% hydrofluoric acid for 5, 10, and 15 minutes(half of the etched samples were coated with silane), and sandblasting with $250{\mu}m$ aluminum oxide powders and silica coating whith Silicoater MD system(Kulzer, Germany). The surface morphology changes were examined with scanning electronic microscope(SEM. and the shear bond strength of In-Ceram core samples to resin cement(Panavis 21, Kurayay, Japan) were measured. It was concluded that : 1. By SEM observation, 20% HF acid etching did not create clear microretentive structure and surface roughness diminished with increace in etching time. Sandblasting was more effective than 20% hydrofluoric acid etching in producing microretentive structure. 2. The bond strengths of all In-Ceram core samples surface conditioned were increased that that of control group. 3. Silica coating showed higher bond strength than etching with 20% hydrofluoric acid. 4. The use of silane coating was more effective in improving bond strength than lengthening etching time.

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복합재료 동력전달축의 접착조인트에 관한 연구 (A Study on Adhesive Joints for Composite Driveshafts)

  • 김진국;이대길;최진경;김일영
    • Composites Research
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    • 제14권2호
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    • pp.13-21
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    • 2001
  • 비강성, 비강도가 우수한 복합재료의 특성상, 기존의 금속 구조물을 복합재료 구조물로 대체 하는 것은 많은 이득을 가져온다. 이 논문에서는 탄소섬유/에폭시 복합재료와 유리섬유/에폭시 복합재료를 이용하여 정적 토크전달 능력, 비틀림 좌굴 하중. 굽힘 1차 고유진동수의 설계 기준을 만족하는 후륜구동 자동차용 일체형 동력전달축이 설계 및 제조되었다. 복합재료 중공축과 알루미늄 요크와의 결합을 위하여 단일 겹치기 접착조인트가 사용되었으며, 접착조인트의 정적 토크전달 능력은 접착길이와 요크두게에 따라 유한요소 해석을 이용하여 계산되었고, 실제 실험결과와 비교되었다. 복합재료 중공축의 정적 토크전달 능력은 Tasi-Wu 파괴지수와 아루미늄 요크와 에폭시 접착제의 비선형 물성을 적용하여 계산되었다. 실험과 해석결과로부터 복합재료 동력전달축의 정적 토크전달 능력은 임계 요크 두께에서 가장 높았으며, 임계 접착길이 이상에서는 포화되었다. 또한 일체형 복합재료 동력전달축은 기존의 2단 분리형 강철 동력전달축과 비교하여 40%의 무게 감소효과를 가져왔다.

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PVOH와 polyDADMAC 첨가에 의한 산화전분의 표면사이징 효과 변화 (Effect of PVOH or polyDADMAC Addition on Surface Sizing with Oxidized Starch)

  • 서동일;정영빈;정광호;이학래;윤혜정
    • 펄프종이기술
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    • 제45권4호
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    • pp.1-8
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    • 2013
  • High loading of printing and writing grades with fillers has many advantageous aspects in papermaking because it allows decreasing fiber use and reducing manufacturing cost. High loading technology, however, has some disadvantageous aspects as well. It decreases physical properties of papers, especially strength properties. The problem associated with high loading can be reduced by applying surface sizing starch solution onto paper surface. It is important to control the penetration of the surface sizing starch solution into paper web to obtain the desired property improvement. In this study, the effect of the addition of two polymers into starch solution on paper properties has been examined. PVOH and polyDADMAC were used as polymeric additives for surface sizing with oxidized starch. Viscosity of starch solutions and surface roughness of dried starch films on glass slides showed that some interactions between polymeric additives and oxidized starch have been occurred and the most extensive interaction with starch solution was obtained with high molecular weight polyDADMAC. Low molecular weight PVOH was most effective in improving folding endurance and internal bond strength. On the other hand, polymer addition showed no effect on surface strength of paper. This indicates that not the level of starch holdout but the bonding strength of starch itself has predominant influence on surface strength of paper.

심미보철 치료의 경향과 이해 : part 1. IPS e.max (Understanding and trends of esthetic treatment in prosthodontics : IPS e.max)

  • 강정인;허유리;이명선;손미경
    • 한국치위생학회지
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    • 제14권4호
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    • pp.447-452
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    • 2014
  • With the increase of esthetic demands, most patients want to have restorations which are not only functional but also esthetic. For the esthetic restoration, many ceramic systems have been introduced and applied in dentistry. Among those ceramic restorations, IPS e.max system composed of lithium disilicate glass ceramic is one of the most commonly used systems because it has strength and esthetic characteristics. IPS e.max system is divided into IPS e.max Press and IPS e.max CAD according to the manufacturing methods. IPS e.max Press is fabricated through heat-pressed technique with ceramic ingot, which is very simple. The restorations which are made using IPS e.max system can apply to 3 units restoration for the anterior teeth and premolar, and single posterior tooth restoration. Cementation is one of the most important clinic procedure for the longevity of the restorations. All ceramics are bonded by resin cements, it is classified into three groups including adhesive, self-adhesive, and conventional. Variolink N, which is an adhesive resin cement and manufactured by same company with IPS e.max, is recommended for the bonding of IPS e.max restoration. Conventional and self-adhesive resin cement is also available. The aim of this review article is to provide the understanding of material properties, production procedure and clinical application of IPS e.max system.

Bond behavior between steel and Glass Fiber Reinforced Polymer (GFRP) bars and ultra high performance concrete reinforced by Multi-Walled Carbon Nanotube (MWCNT)

  • Ahangarnazhad, Bita Hosseinian;Pourbaba, Masoud;Afkar, Amir
    • Steel and Composite Structures
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    • 제35권4호
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    • pp.463-474
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    • 2020
  • In this paper, the influence of adding multi-walled carbon nanotube (MWCNT) on the pull behavior of steel and GFRP bars in ultra-high-performance concrete (UHPC) was examined experimentally and numerically. For numerical analysis, 3D nonlinear finite element modeling (FEM) with the help of ABAQUS software was used. Mechanical properties of the specimens, including Young's modulus, tensile strength and compressive strength, were extracted from the experimental results of the tests performed on standard cube specimens and for different values of weight percent of MWCNTs. In order to consider more realistic assumptions, the bond between concrete and bar was simulated using adhesive surfaces and Cohesive Zone Model (CZM), whose parameters were obtained by calibrating the results of the finite element model with the experimental results of pullout tests. The accuracy of the results of the finite element model was proved with conducting the pullout experimental test which showed high accuracy of the proposed model. Then, the effect of different parameters such as the material of bar, the diameter of the bar, as well as the weight percent of MWCNT on the bond behavior of bar and UHPC were studied. The results suggest that modifying UHPC with MWCNT improves bond strength between concrete and bar. In MWCNT per 0.01 and 0.3 wt% of MWCNT, the maximum pullout strength of steel bar with a diameter of 16 mm increased by 52.5% and 58.7% compared to the control specimen (UHPC without nanoparticle). Also, this increase in GFRP bars with a diameter of 16 mm was 34.3% and 45%.

진공 저온 분사 공정을 통해 형성된 Fe계 비정질 재료의 적층거동 및 미세구조 변화 관찰 (Deposition Behavior and Microstructure of Fe-based Amorphous Alloy Fabricated by Vacuum Kinetic Spraying Process)

  • 권주혁;박형권;이일주;이창희
    • 한국재료학회지
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    • 제24권1호
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    • pp.60-65
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    • 2014
  • Fe-based amorphous coatings were fabricated on a soda-lime glass substrate by the vacuum kinetic spray method. The effect of the gas flow rate, which determines particle velocity, on the deposition behavior of the particle and microstructure of the resultant films was investigated. The as-fabricated microstructure of the film was studied by field emission scanning electron microscopy (FE-SEM) and high resolution transmission electron microscopy (HR-TEM). Although the activation energy for transformation from the amorphous phase to crystalline phase was lowered by severe plastic deformation and particle fracturing under a high strain rate, the crystalline phases could not be found in the coating layer. Incompletely fractured and small fragments 100~300 nm in size, which are smaller than initial feedstock material, were found on the coating surface and inside of the coating. Also, some pores and voids occurred between particle-particle interfaces. In the case of brittle Fe-based amorphous alloy, particles fail in fragmentation fracture mode through initiation and propagation of the numerous small cracks rather than shear fracture mode under compressive stress. It could be deduced that amorphous alloy underwent particle fracturing in a vacuum kinetic spray process. Also, it is considered that surface energy caused by the formation of new surfaces and friction energy contributed to the bonding of fragments.

섬유시트로 보강된 RC 보의 해석기법 연구 (Analysis of RC Beams Strengthened with Fiber Sheets)

  • 김성도
    • 한국구조물진단유지관리공학회 논문집
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    • 제10권6호
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    • pp.154-163
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    • 2006
  • 본 논문에서는 철근 콘크리트보의 인장면에 고강도이며 경량인 섬유시트를 외부 부착한 보강보의 휨 실험결과를 바탕으로 섬유시트로 보강된 RC 휨부재의 비선형 해석 기법을 제시한다. 섬유시트의 인장성능을 측정하기 위하여 총 120개의 섬유시트 인장시험편을 제작하여 시험하였으며, 섬유시트 보강 RC보의 여러 가지 보강특성 및 섬유시트의 적절한 파단변형률을 평가하기 위한 실험적 연구를 위해 75개의 비교적 큰 규모의 보를 시험하였다. 콘크리트의 비선형 압축 분포 및 인장성능을 고려한 비선형 단면 해석과정을 전개하였으며, 이러한 비선형 해석기법이 섬유시트 보강 RC보의 하중-변위 응답 및 휨거동 특성을 정확하게 예측함을 확인하였다.

저 압력 측정을 위한 실리콘 용량형 압력센서 (Silicon Capacitive Pressure Sensor for Low Pressure Measurements)

  • 서희돈;이윤희;박종대;최세곤
    • 센서학회지
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    • 제2권1호
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    • pp.19-27
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    • 1993
  • 본 논문은 $n^{+}$ 에피택셜층을 이용한 전기화학 에칭스톱과 글라스-실리콘의 양극 접합기술을 이용하여 저 압력측정을 위한 용량형 압력센서를 제작한 것이다. 제작된 센서는 하이브리드형으로 센서 커패시터와 기준 커패시터를 갖는 센서 칩과 두가지 출력검출회로 칩으로 구성되어 있다. 이 제작된 센서는 다이아프램 크기가 $1.0{\times}1.0 mm^{2}$이고, 두께가 $10{\mu}m$로 제작된 센서는 압력이 인가되지 않을 때 용량의 크기가 7.1 pF이고, 10 KPa 압력에서 감도가 5.2 %F.S.이다. 또 용량을 전압으로 검출하는 컨버터회로를 이용할 경우, $5{\sim}45^{\circ}C$ 온도범위에서 영점 온도특성과 감도 온도특성은 각각 0.051 %F.S./$^{\circ}C$와 0.12 %F.S./$^{\circ}C$ 이다.

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콘크리트에 표면매입 보강된 탄소섬유 판의 온도에 따른 부착성능 (Bond Capacity of Near-Surface-Mounted CFRP Plate to Concrete Under Various Temperatures)

  • 서수연;김정훈
    • 한국구조물진단유지관리공학회 논문집
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    • 제17권4호
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    • pp.75-83
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    • 2013
  • 본 연구에서는 탄소섬유판을 이용하여 표면매입 보강된 철근콘크리트 부재의 내화성능에 관한 연구로서 온도변화에 따른 탄소섬유 판의 인장시험, 에폭시의 상태변화 실험, 그리고 온도변화에 따른 부착성능에 관한 일련의 실험연구를 실시하였다. 실험연구로부터, 부착강도의 측면에서 콘크리트를 보강하기 위한 효율적인 보강방법은 표면매입 보강이며, 이 보강법은 상온에서는 그 효과가 매우 높지만, 비록 낮은 온도일지라도 주변온도가 높아질 경우에는 보강효과가 현저히 저하될 수 있음을 확인하였다. 특히, 주변 온도가 에폭시의 화학적 성질이 변화하기 시작하는 유리전이 온도에 근접할 경우, 부착기능이 상실되기 시작하므로 구조물의 안전한 내화설계를 위해서는 부착용으로 사용되는 에폭시의 성능을 개선시키고 또한 섬유보강재의 성능개선이 시급한 것으로 사료된다.

진공 압력차이법에 의한 나노 정밀도를 가지는 폴리디메틸실록산 형상복제 (Fabrication Process of a Nano-precision Polydimethylsiloxane Replica using Vacuum Pressure-Difference Technique)

  • 박상후;임태우;양동열;공홍진;이광섭
    • 폴리머
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    • 제28권4호
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    • pp.305-313
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    • 2004
  • 본 연구는 나노 복화공정을 이용하여 마이크로 혹은 나노공정에 응용이 가능한 형상모형 제작공정 개발과 폴리디메틸실록산 (polydimethylsiloxane)를 이용하여 만들어진 형상모형의 몰드로 나노급 정밀도의 폴리디메틸실록산 형상을 복제하는 공정에 관한 것이다. 본 연구에서 제안한 나노 복화공정은 복잡한 형상모형 (pattern)이나 2차원 형상을 CAD 파일 없이 비트맵 그림파일을 이용하여 직접적으로 200nm 정밀도를 가지는 형상으로 만들 수 있다. 형상모형은 펨토초 레이저를 이용하여 이광자 흡수 중합법으로 제작하기 때문에 형상의 정밀도는 레이저 범의 회절한계 이하로 얻을 수 있다. 이렇게 제작된 마스터 형상모형은 본 연구에서 제안한 진공압력차이법으로 폴리디메틸실록산 몰드를 제작하여 기존의 제작방법에 비하여 정밀한 제작이 가능함을 보였으며 또한 제작된 몰드를 이용하여 양각의 플리디메틸실록산 스탬프를 제작하였다.