• Title/Summary/Keyword: beer analysis

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Analysis of Drugs and Chemicals by Infrared Absorption Spectrophotometry(II) Quantitative Analysis of Sulfamethoxydiazine and Sulfamethoxypyridazine in Pharmaceutical Preparations. (Infrared spectrophotometry에 의한 의약품의 분석연구 (II) 적외선흡수 Spectra에 의한 Sulfamethoxydiazine 및 Sulfamethoxy-pyridazine의 정량분석)

  • 옥치완;권영훈
    • YAKHAK HOEJI
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    • v.13 no.2_3
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    • pp.51-56
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    • 1969
  • In quantitative analysis of sulfonamide drugs by means of infrared Spectrophotometry, the author tried to analyse Sulfamethoxydiazine and Sulfamethoxypyridazine in their Pharmaceutical Preparations. By the survey of infrared absorption spectra of Sulfamethoxydiazine and Sulfamethoxypyridazine. We found quantitative properties at the peaks of wave number 1150 cm$^{-1}$ (Sulfamethoxydiazine) and 1090 cm$^{-1}$ (Sulfamethoxypyridazine) in the spectra. These peaks obey Beer's Law in a range of 50-150 ug for Sulfamethoxydiazine and 70-350 ${\mu}$g for Sulfamethoxypyridazine in 300 mg KBr disc. By this method, Sulfamethoxydiazine and Sulfamethoxypyridazine could be analyzed less than 2% error.

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A Comparison of the Preference and Consumption Status of Non-Alcohol and Alcohol Beverages of Korean and Chinese University Students in the Jeonbuk Area (전북지역 한국대학생과 중국대학생의 일반음료와 알코올음료의 기호도와 섭취실태 비교)

  • Rho, Jeongok;Chang, Eunha
    • Korean Journal of Human Ecology
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    • v.21 no.4
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    • pp.805-817
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    • 2012
  • This study was conducted to investigate the preference and consumption status of non-alcohol and alcohol beverages of Korean and Chinese university students in the Jeonbuk area. Self-administered questionnaires were collected from 241 Korean and 198 Chinese students. Statistical data analysis was completed using SPSS v. 12.0. 'Water' was the most commonly consumed non-alcohol beverages by all Korean and Chinese students. The intake frequency of 'carbonated drink' (p<.001), 'fruits/vegetable juice' (p<.05), and 'vinegar drink' (p<.01) of Chinese male students was significantly higher than the Korean male students. The intake frequency of 'ionic drink' (p<.001; p<.01) of Korean male and female students was significantly higher than the Chinese male and female students. The intake frequency of 'fruits/vegetable juice' (p<.001), 'milk' (p<.01), and 'soymilk' (p<.05) of Chinese female students was higher than the Korean female students. For the choosing the non-alcohol beverages, the Chinese female students were more health-oriented than the Korean female students (p<.01). 'Beer' was the most commonly consumed alcohol beverages by the Korean male and female and Chinese male students whereas 'Wine' was the most commonly consumed alcohol beverages by the Chinese female students. The intake frequency of 'Soju' of Korean male (p<.001) and female (p<.001) students was higher than the Chinese male and female students. The intake frequency of 'Wine' of Chinese male (p<.05) and female (p<.001) students higher than the Korean male and female students. Compared with the Chinese female students, the Korean female students more funds have to spend, in order to buy alcohol beverages (p<.01). More 81% of the Korean male and 80% of the female students reported drinking alcohol in 'beer house' whereas 78% of the Chinese male and 65% of female students drunken the alcohol in the 'beer house' or at 'home' (p<.01; p<.001). In conclusion, a practically and foreigner-friendly alcohol policies of university should be devised to reduce the alcohol consumption of students and related problems.

Relations of Safety Factor and Reliability for Pile Load Capacity (말뚝 기초지지력에 대한 안전율과 신뢰도지수 평가)

  • Kim, Dae-Ho;Kim, Min-Ki;Hwang, Sung-Uk;Park, Young-Hwan;Lee, Jun-Hwan
    • Journal of the Korean Geotechnical Society
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    • v.22 no.11
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    • pp.65-73
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    • 2006
  • Reliability between safety factor and reliability index for driven and bored pile load capacity was analyzed in this study. 0.1B, Chin, De Beer, and Davisson's methods were used for determining pile load capacity by using load-settlement curve from pile load test. Each method defines ultimate yield and allowable pile load capacities. LCPC method using CPT results was performed for comparing results of pile load test. Based on FOSM analysis using load factors, it is obtained that reliability indices for ultimate pile load capacity were higher than those of yield and allowable condition. Present safety factor 2 for yield and allowable load capacities is not enough to satisfy target reliability index $2.0{\sim}2.5$. However, it is sufficient for ultimate pile load capacity using safety factor 3.

Studies on analysis of the Korean lager beers. (I) "On the estimation of total carbohydrates, amino acids and peptides" (한국산 맥주성분에 관한 연구 (제 1 ) "Total carbohydrates, amino acids 및 peptides 의 정 에 관하여")

  • 한홍의;김종협
    • Korean Journal of Microbiology
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    • v.6 no.2
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    • pp.63-67
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    • 1968
  • Total carbohydrates, amino acids and peptide-like substances in two kinds of Korean lager beers have been analyzed by the calorimetric method of Dreywood's anthrone reagent and Fowden's ninhydrin reagent. The samples were fractionated with column of ion-exchange resin. The experimental results are as follows; 1. Amounts of non-hydrolyzed carbohydrates in the part of column processed is 1. 82% and 1. 96 % (the value was measured by Bertrand's method). But the amounts of those measured by Dreywood's anthrone method are 5.57% and 4.25%, this values are much more than those of Bertrand's method. 2. It can be estimated the amounts of gum and dextrin are 3.75% and 3.30% in both two beers, by comparison of samples with the above mentioned two method. 3. The amounts of carbohydrates by anthrone reagent in acid-hydrolyzed beers are much increased than those of non-hydrolyzed, so it is suggested the presence of polymer carbohydrates which couldn't be detected by Bertrand's method. 4. Total amounts of amino acids are 0.015% and 0.025% (as glycine) in non-hydrolyzed beers measured by ninhydrine color reaction method, on the other hand the amount of amino acids in acid hydrolyzed beers are 0.06% and 0.056%, this is much more than those of nonhydrolysis. The different amounts means that of peptide-like substances. 5. It is necessary to determine the constituent of amino acid for the better taste of beer, and also it is desirable to check the role of carbohydrates in the course of fermentation, mashing and on lager beer for effective utilization of carbohydrate materials to eliminate the losses.

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Characterization of Cholesterol Lowering Lactic Acid Bacteria Isolated from Palm Wine and Maize Beer and Assessment of Their Use in the Production of Probiotic Papaya Juice

  • Bertrand Tatsinkou Fossi;Dickson Ebwelle Ekabe;Liliane Laure Toukam Tatsinkou;Rene Bilingwe Ayiseh;Frederic Tavea;Pierre Michel Jazet
    • Microbiology and Biotechnology Letters
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    • v.51 no.2
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    • pp.191-202
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    • 2023
  • Elevated serum cholesterol is a main risk factor for heart disorders. Most probiotic products administered to lower cholesterol are dairy products which are not suitable for lactose-intolerant individuals. In this study, we assessed the cholesterol-lowering efficacy of LAB isolated from traditionally fermented drinks in diet-induced rats and determine their efficacy in the production of non-dairy, probiotic formulations using papaya juice. LAB were isolated from palm wine and corn beer on MRS agar using a pour-plate technique. Identification was carried out using 16S rRNA gene sequencing. A hypercholesterolemia model in which diet-induced Wistar albino rats were assigned into four groups was established. Oral gavage was carried out for 30 days. On the 31st day, the rats were dissected and the serum lipid profile was analyzed using biochemical kits. A 106 cfu/ml of a 24-h-old culture of selected lactobacilli was used to inoculate papaya juice and incubated at 37℃. Microbial and chemical changes were assessed during papaya fermentation and after four weeks of cold storage. Two selected isolates (Pw1 and Cb4) had in vitro cholesterol reduction of > 80%. These two isolates lowered lipid profile (triglyceride, total cholesterol, LDL-c) significantly, and increased HDL-c levels (p < 0.5) in the rat sera. Phylogenetic analysis showed that Pw1 was 98.86% similar to Limosilactobacillus fermentum, while Cb4 was 99.54% similar to Enteroccocus faecium. Both strains fermented papaya juice with cell viability reaching 8.92 × 108 cfu/ml and 25.3 × 108 cfu/ml respectively, and were still viable after 4 weeks of cold storage.

Isolative Determination of Ethinyl Estradiol and Norethindrone Acetate in the Mixed Preparations (혼합성분중(混合成分中) Ethinyl Estradiol과 Norethindrone Acetate의 분리정량(分離定量))

  • Lee, Jung-Hyun;Young, Jae-Ick
    • Journal of Pharmaceutical Investigation
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    • v.1 no.1
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    • pp.47-52
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    • 1971
  • Application of the spectrophotometer to the analysis of 17 ${\alpha}-ethinyl$ estradiol and $17{\alpha}-ethinyl-19-nortestosterone$ acetate mixture in oral contraceptive has been accomplished. It is used Beckman Du Spectrophotometer as a apparatus. The petroleum ether extract of ethinyl estradiol is determined at $535\;m{\mu}$ and the chloroform extract of norethindrone acetate is determined at $380\;m{\mu}$ respectively. This analytical method is formed Lambert Beer's law. This method can be used to the analysis of ethinyl estradiol aid norethindrone acetate mixture in commercial dosage form of routine assay.

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Relations of Safety Factor and Reliability Index for Pile Load Capacity (말뚝 기초지지력에 대한 안전율과 신뢰도지수 평가)

  • Kim, Dae-Ho;Lee, Jun-Hwan
    • Proceedings of the Korean Geotechical Society Conference
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    • 2006.03a
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    • pp.466-475
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    • 2006
  • Reliability analysis between safety factor and reliability index for driven and bored pile load capacity was analyzed in this study. 0.1B, Chin, De Beer, and Davisson's methods were used for determining pile load capacity by using load-settlement curve from pile load test. Each method define ultimate, yield and allowable pile load capacities. LCPC method using CPT results was performed for comparing with results of pile load test. Based on FOSM analysis using load factors, it is obtained that reliability indices for ultimate pile load capacity were higher than those of yield and allowable condition. Present safety factor 2 for yield and allowable load capacities are not enough to satisfy target reliability index $2.0\sim2.5$. However, it is sufficient for ultimate pile load capacity using safety factor 3.

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Analysis of $Cr_2O_7^{-2}/MnO_4^{-}$ Mixtures by an Absorption Spectrometry Coupled with Flow Injection Analysis(FIA) (흐름주입분석기법에 접목된 흡수분광분석법에 의한 $Cr_2O_7^{-2}/MnO_4^{-}$혼합물의 분석)

  • Hwang, Hoon
    • Journal of the Korean Chemical Society
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    • v.44 no.3
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    • pp.212-219
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    • 2000
  • An absorption spectrometry coupled with flow injection analysis has been developed and tested for the analysis of the Cr$_2O_7^{2-}$/Nn$O_4^-$ mixtures. Even though one has to inject the sample twice into the FIA system and the process of the sample treatment is required to completely destroy the Mn$O_4^-$ ion for the analysis of the Cr$_2O_7^{2-}$ ion, the new method has definite advantages over the current method. It utilizes only a single analytical wavelength (570 nm) and enables one to construct calibration curves which accurately follow the Beer's law over wide ranges of analytical concentrations of both ions ($2.0{\times}10^{-6}$M∼$8.0{\times}10^{-3}$M for Cr$_2O_7^{2-}$ ion, $2.0{\times}10^{-6}$M∼$4.0{\times}10^{-3}$M for MnO4- ion).

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Dietary patterns associated with hypertension among Korean males

  • Kim, Young-Ok
    • Nutrition Research and Practice
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    • v.3 no.2
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    • pp.162-166
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    • 2009
  • The objectives of this study were to identify the dietary patterns associated with hypertension among Korean males. Data from the 2001 Korean National Health and Nutrition Survey of 1,869 men aged 20-65 years were used for the analysis. As an initial analysis, a factor analysis was applied to identify major dietary patterns among the subjects. Then logistic regression analysis was conducted to identify the pattern related with hypertension. As a result of the initial analysis, three major dietary patterns were identified. Dietary pattern 1 (traditional) was heavily loaded with vegetables, fish and cereal. Dietary pattern 2 (Western) was loaded with fast foods, bread, meats and dairy products. Dietary pattern 3 (Drinker) was loaded with mostly pork, beer and soju (Korean liquor). From the second stage of the analysis, there was a tendency of positive association between traditional patterns and hypertension risks. However, the tendency did not meet statistical significance level (p<0.05). In summary, unlikely findings from European and American studies, vegetables rich traditional dietary patterns did not show any protective effect on hypertension in Korean males. The Korean dietary practice, which is consuming salted vegetables instead of fresh vegetables, might have played a role in these findings. However, the full explanation of the findings remained to be answered with further investigation since none of the dietary patterns identified showed any statistical significance.

Simultaneous Spectrophotometric Determination of Cr(Ⅲ) and Cr(Ⅳ) in Chromium Plating Solution via Flow-Through Analysis (흐름계를 이용한 크롬도금 용액의 Cr(Ⅲ)와 Cr(Ⅵ)의 분광학적 동시 분석 방법)

  • Kim, Sun Kwan;Nam, Hakhyun;So, Jae Chun;Lee, Won;Cha, Geun Sig;Han, Sang Hyun
    • Journal of the Korean Chemical Society
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    • v.39 no.2
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    • pp.87-93
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    • 1995
  • The amount of Cr(Ⅲ) and Cr(Ⅵ) in a chromium plating solution could be determined simultaneously within five minutes using UV/VIS spectrophotometer coupled with a flow-through analysis(FTA) setup. The λmax's at 580 nm and 440 nm which correspond to Cr(Ⅲ) and Cr(Ⅵ), respectively, well obey the Beer-Lambert law in the range over 0.05 g/L for Cr(Ⅲ) and 0.005 g/L for Cr(Ⅵ). when the pH of the sample is less than 4.0, the absorption extinction coefficients of those peaks are not much dependent on the proton concentration. The amount of Cr(Ⅲ) and Cr(Ⅵ), and the total chromium in post treatment chromium plating solution, which normally has few g/L of Cr concentration, could be easily measured using UV/VIS spectrophotometry after the sample had been diluted with sulfuric acid of pH=1.0 in the flow-through analysis setup; this method is far more convenient and faster than the common redox titration (which requires at least 40 min/sample) method, while the accuracy of the method is highly comparable to conventional titrimetric method. Since the implementation of an PTA-UV/VIS setup in any plating industry is cost effective and easy to operate, the analytic method described in this paper may be applied directly for in situ analysis of plating solutions.

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