• Journal of Welding and Joining
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• 제20권2호
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• pp.65-70
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• 2002

This study was to evaluate GMA welding characteristics of the A15083-O aluminum alloy according to the shield gas mixing ratio and heat input change. The GMA welding of the base metal was carried out with flour different shield gas mixing ratios(Ar100%+He0%, Ar67%+He33%, Ar50%+He50%, and Ar33%+He67%). Regarding the if1uence on the bead shape of the shield gas mixing ratio and heat input, the bead width was greatest in Ar100%+He0% mixture. But the penetration depth and area were greatest in Ar33%+He67% mixture considering that the lower Ax gas ratio, the higher bead depth and area. Also, dilution was also best in the shield gas mixing ratio. The size and number of deflects were least in Ar33%+He67% mixture. Higher He gas ratio resulted in less deflects detected by the radiographic inspection.

• 대한용접접합학회:학술대회논문집
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• 대한용접접합학회 2006년도 춘계 학술대회 개요집
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• pp.304-306
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• 2006

Positioning the workpiece accurately and preventing the weld distortion, tack welding is often performed before main welding in the construction of welded structures. The weld bead size of the tack weld is determined according to the workpiece thickness, weld length, weld joint type etc. However, this tack weld deteriorates the final weld bead profile, so that the grinding process is usually adopted for the uniform weld bead profile. In this study, an experimental method for the selection of optimal welding condition was proposed in the fillet weld which was done over the tack weld. This method uses the response surface analysis in which the leg length and the reinforcement height of weld bead were chosen as the quality variables of weld bead profile. The overall desirability function, which was combined desirability function for the two quality variables, was used as the objective function for getting the optimal welding condition. From the result, it was revealed that a uniform weld bead can be obtained by adopting the optimal welding condition which was determined according to the method proposed.

• Food Science and Biotechnology
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• 제16권5호
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• pp.715-721
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• 2007

In this study, the sphericity of calcium alginate gel beads was optimized using response surface methodology. The optimum conditions for bead sphericity were a concentration of 2.24% sodium alginate, a flow rate of 0.059 mL/sec for the sodium alginate solution, and a 459 rpm rotation for the calcium chloride solution. The predicted and experimental bead sphericities under the optimum conditions were 94.5 and 96.7%, respectively, showing close agreement. We also investigated the processing condition effects for the physical properties of the optimized calcium alginate gel beads. Immersion in hot water slightly decreased bead size and rupture strength. NaCl treatment increased bead size and decreased rupture strength. While the pH of the calcium chloride solution had little effect on bead sphericity, the bead sizes and gel strengths decreased with longer times in each pH solution. The beads coated with pectin and glucomannan showed no significant changes in sphericity, but their sizes decreased with time. The coated beads showed higher rupture strengths than the uncoated beads.

• Journal of Welding and Joining
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• 제19권3호
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• pp.317-324
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• 2001

This study deals with high power Nd:YAG laser welding of thin steels for small pressure vessels. Full penetration welding at the overlap joint was performed so as to assure sufficient weld strength. Results showed that mid-depth weld size reduced drastically with increasing the travel speed. Position of focus had little effect on the bead formation even though short focal system was used. However, the shape factor and the bead width had closely related with the position of focus. Based on the microstructural inspection, acceptable weld was obtained when the overlap clearance was controlled up to 20% of the base metal thickness. In the case that the joint contained more clearance than the critical value, both the tensile shear strength and the tear strength were reduced. Results also demonstrated that shielding gases were proved to play a key role as far as the bead formation characteristics was taken into consideration. Blowing dry air through 5mm in diameter nozzle produced narrower bead cross-section than that of argon or nitrogen shielding.

• Journal of Welding and Joining
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• 제22권6호
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• pp.19-24
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• 2004

The laser welding and its analysis of thin-sheet carbon steels were carried out with high power $CO_{2}$ laser. The main factor of weld quality of laser welding is gap and edge quality. This work was preformed to focus on the gap tolerance problem during laser welding. First, bead on plate welding of thin sheet was examined to investigate the effect of laser welding variables, and to obtain optimum welding condition. Butt welding was also carried out to show the effect of gap on the laser weldability of thin sheet. In order to investigate the effect of gap on formability of welded thin sheet, LDH test was caried out. At high welding speed, the partial penetration was obtained by low heat input. Otherwise, porosity was formed in the bead at low weld speed because of too much heat input. The optimum welding condition of welding was derived from bead width, penetration and hardness property. The maximum gap tolerance on laser welding was observed to be about 0.2mm. This gap size has good relationship with beam size of laser spot(about 0.3mm). The formability of welded sheet was about $80{\%}$ value of base metal and the gap size has not affected on the formability, although weld quality is dependent on the gap size.

• Composites Research
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• 제30권4호
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• pp.254-260
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• 2017

본 논문에서는 알루미늄과 복합재료에 대한 이종소재 접합면의 성형안전성을 위해 일정한 두께를 확보할 수 있는 0.1 mm, 0.2 mm, 0.3 mm bead의 적용 방법과 물성변화에 대해 연구하였고, 이를 검증하기 위해 더블랩 시험과 FEM 시뮬레이션으로 접착제의 두께에 따라 미치는 영향을 평가하였다. 그 결과, 접착제에 bead의 양을 1% 이상 함량이 증가함에 따라 접착 소재의 강도가 높아지고 신율이 감소함을 확인하였고, bead의 크기가 커질수록, 강성은 낮아지고, 신율은 증가함을 확인하였다.

• 환경영향평가
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• 제30권4호
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• pp.247-257
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• 2021

본 연구에서는 기존 바이오차의 제한점인 비소 오염 토양 안정화에 대한 낮은 효율과 비산에 의한 유실 가능성을 개선할 수 있는 철 나노입자가 담지된 바이오차 기반 비드 형태 안정화제인 INPBC/bead (Iron Nano-Particles Impregnated BioChar/bead)를 제조하였다. 폐목재 바이오매스를 Fe(III) 용액과 함께 수열 반응을 진행하고 이후 소성을 거쳐 INPBC를 제조하였다. INPBC/bead는 알지네이트의 cross-linking 반응을 통해 제조 하였다. 제조한 INPBC/bead의 특성을 평가하기 위해 FT-IR, XRD, BET 비표 면적, SEM-EDS 분석을 실시하였다. 특성 평가 결과 입자 크기가 1-4 mm인 INPBC/bead는 여러 산소 함유 관능기를 보유하며 표면의 철 결정성은 Fe3O4인 것으로 확인되었다. INPBC/bead의 성능을 평가하기 위해 폐광산 주변 지역에서 채취한 비소 및 중금속 오염 토양을 이용하여 배양 실험을 실시하였다. 4주 동안의 배양이 종료된 후 처리된 토양을 대상으로 TCLP, SPLP 시험을 실시한 결과 안정화제 적용 비율이 증가함에 따라 안정화 효율은 높아지는 것으로 확인되었다. SPLP 시험 결과, INPBC/bead 5%의 비소 안정화 효율은 81.56%이며 납의 경우에는 농도가 검출한계 미만으로 저감되었다. 상기의 결과를 종합하였을 때 INPBC/bead는 토양 중 비소와 납에 대한 안정화 효과를 동시에 보유하고 토양의 pH 변화를 일으키지 않으며 비드 형태로써 적용 과정에서 비산되는 것이 방지할 수 있는 안정화제이기 때문에 비소 및 중금속 복합 오염 토양 안정화에 적용 가능성이 높은 안정화제 인 것으로 판단된다.

• 한국전기전자재료학회:학술대회논문집
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• 한국전기전자재료학회 2005년도 추계학술대회 논문집 Vol.18
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• pp.151-152
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• 2005

Both $Al_2O_3$ and AlN nanopowders with diameters from ${\mu}m$ to mm were bead-milled and surface-modified by stabilizing agent. The size of bead-milled nanoparticles compared with the primary powder was effectively decreased and was dependent on milling time and bead size. The results of dispersion stability analysis indicated that chemical bonding between nanoparticles and surfactant is more effective than chemical adsorption to prepare the stable transformer oils containing nanoparticles. In this study, the thermal conductivity of the transformer oils containing nanoparticles was measured by transient hot-wire and laser flash methods.

• Korean Chemical Engineering Research
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• 제53권6호
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• pp.792-797
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• 2015

그래핀은 다양하고 뛰어난 물성으로 그 적용 분야가 넓다. 그러나 반델반스 상호 작용으로 유기용매 내에서 쉽게 분산되지 않고 뭉쳐 있거나 포개진 상태로 존재한다. 게다가 그래핀은 화학적으로 비활성이며 크기나 모양이 넓은 분포도를 가지므로 균일한 상태 유지가 어렵다. 본 연구에서는 덩어리로 구성된 그래핀을 용매에 분산시키고 개질시키는 방법에 대해서 고찰하였다. 분산방법으로서 i) 유리비드를 이용한 물리적 분쇄. ii) 유리비드와 초음파를 이용한 처리 iii)유기용매에서의 분산 iv)드라이아이스를 이용한 개질법이 포함된다. 2.5 mm 크기의 유리비드처리는 대조구와 비교하여 36.4%의 감소율을 나타내었다. 유리비드(2.5 mm)와 초음파(225W, 10분) 병용 처리구가 76%로 입자 크기 감소효과를 나타내었다. 그래핀 입자 크기감소는 유리비드의 크기와 초음파 처리강도와 처리시간에 의존되었다. Ethyl acetate(EA)와 Isoprophyl alcohol(IPA)의 용매로 그래핀 표면을 개질시켰다. IPA용매에서 FT-IR 분석결과 CO 작용기가 높게 나타남으로 확인할 수 있었다. 한편, 드라이아이스로 그래핀 표면을 개질시킨 결과 처리 전 산소함량이 0.80%에서 처리 후 4.90%로 산소 함량 크게 증가되었다. 본 연구 결과로부터 IPA용매에 그래핀을 분산시킬 때 CO 작용기가 증가하여 장시간 분산상태 유지에 도움이 되는 것으로 판단된다.

• 한국재료학회지
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• 제27권2호
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• pp.100-106
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• 2017

Nanosized and aggregated $Y_2O_3:Eu$ Red phosphors were prepared by template method from metal salt impregnated into crystalline cellulose. The particle size and photoluminescent property of $Y_2O_3:Eu$ red phosphors were controlled by variation of the calcination temperature and time. Dispersed nanosol was also obtained from the aggregated $Y_2O_3:Eu$ Red phosphor under bead mill wet process. The dispersion property of the $Y_2O_3:Eu$ nanosol was optimized by controlling the bead size, bead content ratio and milling time. The median particle size ($D_{50}$) of $Y_2O_3:Eu$ nanosol was found to be around 100 nm, and to be below 90 nm after centrifuging. In spite of the low photoluminescent properties of $Y_2O_3:Eu$ nanosol, it was observed that the photoluminescent property recovered after re-calcination. The dispersion and photoluminescent properties of $Y_2O_3:Eu$ nanosol were investigated using a particle size analyzer, FE-SEM, and a fluorescence spectrometer.