• Title/Summary/Keyword: autoclave test

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Analysis of Composite Microporosity according to Autoclave Vacuum Bag Processing Conditions (오토클레이브 진공포장법의 공정 조건에 따른 복합재의 미세기공률 분석)

  • Yoon, Hyun-Sung;An, Woo-Jin;Kim, Man-Sung;Hong, Sung-Jin;Song, Min-Hwan;Choi, Jin-Ho
    • Composites Research
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    • v.32 no.5
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    • pp.199-205
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    • 2019
  • The composite material has the advantage that the fibers can be arranged in a desired direction and can be manufactured in one piece. However, micro voids can be formed due to micro air, moisture or improper curing temperature or pressure, which may cause the deterioration in mechanical strength. In this paper, the composite panels with different thicknesses were made by varying the curing pressure in an autoclave vacuum bag process and their microporosities were evaluated. Microporosity was measured by image analysis method, acid digestion method, and combustion method and their correlation with ultrasonic attenuation coefficient was analyzed. From the test results, it was found that the acid digestion method had the highest accuracy and the lower the curing pressure, the higher the microporosity and the ultrasonic attenuation coefficient. In addition, the microporosity and the ultrasonic attenuation coefficient were increased as the thickness of the composite panel was increased at the same curing pressure.

A Study on the Estimation of Corrosion Protection Performance of Concrete Containing Ground Granulated Blast-Furnace Slag for Massive Coastal Structures (매시브한 해양구조물 적용을 위한 고로슬래그 혼입 콘크리트의 방청성능 평가에 관한 연구)

  • Yoo, Jae-Kang;Kim, Dong-Suk;Park, Sang-Joon;Won, Chul;Lee, Sang-Soo
    • Proceedings of the Korean Institute of Building Construction Conference
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    • 2002.11a
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    • pp.87-91
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    • 2002
  • This paper investigates the corrosion inhibition and the reduction of hydration heat properties of Ground Granulated Blast-Furnace Slag (GGBFS) added concrete. Since the massive civil structure is vulnerable to the thermal crack by hydration. adiabatic temperature rising tests were performed for water-binder ratios from 43.2% to 47.3%, while replacing 15% to 50% of cement with GGBFS of equal weight. Then, the corrosion protection performance was evaluated using cylindrical specimens embedded with steel reinforcement according to the combination of 3 W/B ratios and 2 levels of chloride ion quantity. The corrosion area of the embedded steel ban was determined using the high pressure steam curing method specified in KS F 2561. The test results showed that the replacement of GGBFS was effective in reducing the hydration heat. The corrosion area of the embedded steel ban decreased as the replacement of GGBFS increased. However, the corrosion area of the steel bar was proportional to the autoclave cycle and the chloride ion quantity. Among the tested specimens, compressive strength, reduction of hydration heat, and corrosion inhibition performance were excellent when 50% of cement was replaced with GGBFS of equal weight.

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Strength of Composit Single-lap Bonded Joints with Different Saltwater Moisture Contents (서로 다른 수분율을 갖도록 염수환경에 노출된 복합재 접착체결부의 강도)

  • Yang, Hyeon-Jeong;Jeong, Mun-Gyu;Kweon, Jin-Hwe;Choi, Jin-Ho
    • Composites Research
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    • v.24 no.4
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    • pp.48-54
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    • 2011
  • The effect of moisture contents by salt water on the strength of composite single-lap bonded joints is investigated. The specimens were manufactured in an autoclave by secondary bonding and immersed in the 3.5% salt water of $71^{\circ}C$ for different durations to get various moisture contents; 0, 0.2, 0.5, 1.0, and 2.0%(saturation). A total of 80 joint specimens were tested for 5 different moisture contents and 2 temperature environments. Test results show that while the joint strengths after the saturation of moisture decrease compared to those of dry ones, the strengths of the pre-saturated joint up to 1.0% of moisture content increase in both room and elevated temperature conditions. It is also shown that the strengths of joints tested in elevated temperature are slightly higher than the strength in room temperature by 2-5% until the moisture content reaches 1 %. In contrast, the high temperature strength of the saturated joint is about 5% lower than the room temperature strength.

Penetration Characteristic of CFRP laminate shell by the curvature -A focus of fracture mode by the penetration- (곡률을 고려한 CFRP 복합재 적층쉘의 관통특성 -관통에 의한 파괴모드를 중심으로-)

  • 조영재;김영남;심재기;양인영
    • Proceedings of the Korean Society of Precision Engineering Conference
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    • 2004.10a
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    • pp.1434-1439
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    • 2004
  • CFRP composite materials have wide application in structure materials of airplane, ships, and aero space vehicles because of their high strength and stiffness. This paper is to study the effects of curvature and orientation angle on the penetration characteristics of CFRP laminate shell. They are staked with 8 Ply specimens [0$_2$/90$_2$]$_{s}$, [0/90$_2$/0]$_{s}$ and the stacked of outer plates degree with 12 Ply specimens [0$_3$/90$_3$]$_{s}$, [0$_2$/90$_2$/0]$_{s}$ and [90$_3$/0$_3$], [90$_2$/0$_2$/90]S. They are manufactured to varied curvature radius (R=100,150,200mm and $\infty$). They are cured by heating to the appropriate harding temperature(13$0^{\circ}C$) by mean of a heater at the vaccum bag of the autoclave. Test specimens were prepared with dimensions 100mm$\times$140mm. When the specimen is subjected to transverse impact by a steel ball, the velocity of the steel ball was measured both before and after impact by determining the time for it to pass two ballistic-screen sensor located a known distance apart. In general, kinetic energy after impact-kinetic energy before impact rised in all specimens. This study observed a fracture mode inside the specimen after a penetration test using a digital camera and it examined a fracture mode and a penetration mode to stack of outer orientation angle and curvature.rvature.

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Stress Analysis for Bendable Electronic Module Under Thermal-Hygroscopic Complex Loads (열·습도 복합하중에서의 유연성 전자모듈에 대한 구조해석)

  • Han, Changwoon;Oh, Chulmin;Hong, Wonsik
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.37 no.5
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    • pp.619-624
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    • 2013
  • A bendable electronic module is developed. In this module, thin silicon electronic chips are embedded in a polymer-based encapsulating adhesive between flexible copper-clad polyimide layers. During the qualification test of a harshly thermal-hygroscopic complex loading condition, delaminations occur inside the module layers. A finite element model is developed for the module. To investigate the effect of hygroscopic stress on delamination, the results of the thermal and thermal-hygroscopic loads are compared. The analysis results reveal that the hygroscopic effect more strongly affects delamination than does the thermal effect. The potential failure mechanisms of the module are investigated based on the stress analysis.

The Optimal Mixing Design of the PHC Piles Utilizing the Air Cooled Blast Furnace Slag as Coarse Aggregate (서냉 고로슬래그 굵은골재를 활용한 PHC 파일의 최적배합 및 물리적 특성)

  • Park, Yong-Kyu;Kim, Hyun-Woo;Kim, Seung-Il;Hur, Kab-Soo;Yoon, Ki-Won
    • Journal of the Korean Recycled Construction Resources Institute
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    • v.2 no.2
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    • pp.137-144
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    • 2014
  • The PHC pile utilizing the air-cooled blast-furnace slag as coarse aggregate was studied. This research was progressed with the range from the indoor mixing design evaluation into the actual goods production. The physical properties of the PHC pile are determined to satisfy through the appropriate mixing design adjustments. However, it should eliminate the aggregates including CaO and MgO in SG when it utilize in an AC (autoclave) type manufacturing process. It satisfied the bending moment, shear strength, and compressive strength of KS F 4306 except the surface states of the pile.

Design Analysis/Manufacturing /Performance Evaluation of Curved Unsymmetrical Piezoelectric Composite Actuator LIPCA (곡면형 비대칭 압전복합재료 작동기 LIPCA의 설계해석/제작/성능평가)

  • Gu, Nam-Seo;Sin, Seok-Jun;Park, Hun-Cheol;Yun, Gwang-Jun
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.25 no.10
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    • pp.1514-1519
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    • 2001
  • This paper is concerned with design, manufacturing and performance test of LIPCA ( Lightweight Piezo- composite Curved Actuator) using a top carbon fiber composite layer with near -zero CTE(coefficient of thermal expansion), a middle PZT ceramic wafer and a bottom glass/epoxy layer with high CTE. The main point of this design is to replace the heavy metal layers of THUNDER by thigh tweight fiber reinforced plastic layers without losing capabilities to generate high force and large displacement. It is possible to save weight up to about 30% if we replace the metallic backing material by the light fiber composite layer. We can also have design flexibility by selecting the fiber direction and the size of prepreg layers. In addition to the lightweight advantage and design flexibility, the proposed device can be manufactured without adhesive layers when we use epoxy resin prepreg system. Glass/epoxy prepregs, a ceramic wafer with electrode surfaces, and a graphite/epoxy prepreg were simply stacked and cured at an elevated temperature (177 $^{circ}C$ after following an autoclave bagging process. It was found that the manufactured composite laminate device had a sufficient curvature after detached from a flat mold. The analysis method of the cure curvature of LIPCA using the classical lamination theory is presented. The predicted curvatures are fairly in agreement with the experimental ones. In order to investigate the merits of LIPCA, a performance test of both LIPCA and THUNDE$^{TM}$ were conducted under the same boundary conditions. From the experimental actuation tests, it was observed that the developed actuator could generate larger actuation displacement than THUNDERT$^{TM}$.

A study on the variation of in-plane and out-of-plane properties of T800 carbon/epoxy composites according to the forming pressure (성형 압력에 따른 T800 탄소섬유/에폭시 복합재료의 평면 내.외 물성 변화에 대한 연구)

  • Park, Myong-Gil;Cho, Sung-Kyum;Chang, Seung-Hwan
    • Composites Research
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    • v.23 no.6
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    • pp.61-66
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    • 2010
  • In this paper, the variation of mechanical properties of T800 carbon/epoxy composites according to the forming pressure, which was referred to previous studies on a filament winding process, were investigated. The specimens of all the tests were fabricated by an autoclave de-gassing molding process controlling forming pressure (absolute pressures of 0.1MPa, 0.3MPa, 0.7MPa including vacuum) and water jet cutting after fabricating composite laminates. Various tensile tests were performed for in-plane properties and interlaminar properties were also measured by using Iosipescu test jig. Fiber volume fraction was measured to correlate the property variation and the forming pressure. This properties are expected to be utilized in the design of Type III pressure vessel for hydrogen vehicles which uses the same carbon fiber (T800 carbon fiber) for the filament winding process.

Test Evaluation of a Linerless Composite Propellant Tank Using the Composite Collapsible Mandrel (복합재 분리형 맨드릴을 이용한 라이너 없는 복합재 추진제 탱크에 대한 시험 평가)

  • Seung Yun Rhee;Kwangsoo Kim;Young-Ha Yoon;Moo-Keun Yi;Hee Chul Kim
    • Composites Research
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    • v.36 no.2
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    • pp.132-139
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    • 2023
  • A linerless composite propellant tank was designed and manufactured by using the carbon fiber-reinforced composite materials which have superior strength-to-weight ratio in order to reduce weight of the tank. In this research, we designed a sub-scale composite propellant tank with a diameter of 800 mm to withstand an MEOP of 1.7 MPa. We manufactured the boss of the tank by using the same composite materials to reduce the thermal expansion difference between the boss and the secondary-bonded composite layers of the barrel in the cryogenic environment. We used the collapsible mandrel to manufacture the tank without any liner. The mandrel was made from epoxy-based composite tooling prepregs to reduce weight of the mandrel. We manufactured the test tanks by laying up the carbon fiber fabric prepregs manually on the mandrel and then applying the autoclave cure process. We performed a proof test, a helium tightness test, a repeated pressurization test, and a burst test in room temperature. The test results demonstrate that the proposed design and manufacture process satisfies all strength requirements as well as an anti-leakage requirement.

High Temperature Application of Iron Removal Chemical Cleaning Solvent in the Secondary Side of Nuclear Steam Generators (증기발생기 2차측 제철화학세정액의 고온적용)

  • Hur, D.H.;Lee, E.H.;Chung, H.S.;Kim, U.C.
    • Nuclear Engineering and Technology
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    • v.26 no.1
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    • pp.140-148
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    • 1994
  • A qualification test was performed for the iron removal chemical cleaning of the secondary side of nuclear steam generators at the selected temperature, 1$25^{\circ}C$, higher than the standard application temperature, 93$^{\circ}C$. The field cleaning condition for a nuclear unit was tested in a bench scale test loop including a SUS 316 stainless steel autoclave with one gallon capacity as a test vessel. The kinetics of sludge dissolution, corrosion of the secondary side materials and change of solvent chemistry were monitored. Test results indicated that more thorough cleaning was accomplished in less than half of the cleaning time required at 93$^{\circ}C$. And the total corrosions of the secondary side materials were found to be less than the values at 93$^{\circ}C$. While the solvent is recirculated and heated by an external chemical cleaning equipment for the conventional 93$^{\circ}C$ process, the secondary side is heated by the lateral heat of the primary coolant without the recirculation of the cleaning solution, and the solvent is mixed by vigorous boiling induced by periodic ventilation for the high temperature process. The requirement that the reactor coolant pumps should be running during the cleaning operation is the major disadvantage of the high temperature process which also should be considered when chemical cleaning is planned for steam generators under operation.

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