• Title/Summary/Keyword: autoclave test

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Prediction of Optimum Fertilizer Rate for Flue-Cured Tobacco by Nitrogen Availability in Soils (토양질소(土壤窒素)의 유효도(有效度) 검정방법(檢定方法)에 의한 황색종연초(黃色種煙草)의 적정시비량(適正施肥量) 추정(推定))

  • Jeong, Hun-Chae;Cho, Seong-Jin;Hong, Sun-Dal;Lee, Yun-Hwan
    • Korean Journal of Soil Science and Fertilizer
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    • v.18 no.2
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    • pp.169-176
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    • 1985
  • Six analytial methods for determing the available nitrogen in soils were tested to predict the optimum fertilizer rate for the flue-cured tobacco and to test the fertility level of soils for tobacco. All methods, nitrifiable $NO_3-N$ value for 2 and 4 weeks incubation, UV absorption value at 260nm and N-value in acid digestion of 0.01 M-$NaHCO_3$ extracts, N-value extracted in boiling with $CaCl_2$ solution, and autoclave-extractable $NH_4-N$ value in 0.01 M-$CaCl_2$, were closely correlated with total nitrogen uptake as well as yield. Therefore available nitrogen indices determined from above 6 analysis method could be used for the predicting of tobacco yield without fertilizer, criteria for fertility class, and recommendable range of optimum fertilization.

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Effect of Final Annealing Temperature on Precipitate and Oxidation of Zr- Nb Alloys (Zr-Nb계 합금의 석출물 특성과 산화 특성에 미치는 마지막 열처리 온도의 영향)

  • Yun, Yeong-Gyun;Jeong, Yong-Hwan;Park, Sang-Yun;Wi, Myeong-Yong
    • Korean Journal of Materials Research
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    • v.11 no.8
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    • pp.647-654
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    • 2001
  • Effects of final annealing temperature on the precipitate and oxidation were investigated for the Zr-lNb and Zr-lNb-lSn-0.3Fe alloys. The microstructure and oxidation of both alloys were evaluated for the optimization of final annealing process of these alloys in the annealing temperature regime of 450 to $800^{\circ}C$. The corrosion test was performed under steam at $400^{\circ}C$ for 270 days in a static autoclave. The oxide formed was identified by low angle X-ray diffraction method. The $\beta$-Zr was observed at annealing temperature above $600^{\circ}C$. Above $600^{\circ}C$, the precipitate area volume fraction of Zr-lNb and Zr-1Nb-lSn-0.3Fe alloys appeared to be increased with increasing the final annealing temperature. The corrosion resistance of Zr-lNb was higher than that of Zr- lNb-lSn-0.3Fe alloy. The corrosion rate of both alloys were accelerated due to the formation and growth of $\beta$-Zr with increasing the annealing temperature.

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Decision of Optimized Mix Design for Lightweight Foamed Concrete Using Bottom Ash by Statistical Procedure (통계적 방법에 의한 바텀애쉬를 사용한 경량기포 콘크리트의 최적배합 결정)

  • Kim, Jin-Man;Kwak, Eun-Gu;Cho, Sung-Hyun;Kang, Cheol
    • Journal of the Korea Concrete Institute
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    • v.21 no.1
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    • pp.3-11
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    • 2009
  • The increased demand and consumption of coal has intensified problems associated with disposal of solid waste generated in utilization of coal. Major utilization of coal by-products has been in construction-related applications. Since fly ash accounts for the part of the production of utility waste, the majority of scientific investigations have focused on its utilization in a multitude of use, while little attention has been directed to the use of bottom ash. As a consequence of this neglect, a large amount of bottom ash has been stockpiled. However, the need to obtain safe and economical solution for its proper utilization has been more urgent. The study presented herein is designed to ascertain the performance characteristics of bottom ash, as autoclaved lightweight foamed concrete product. The laboratory test results indicated that tobermorite was generated when bottom ash was used as materials for hydro-thermal reaction. According to the analysis of variance, at the fresh state, water ratio affects on flow and slurry density of autoclaved lightweight foamed concrete, but foam ratio influences on slurry density, while, at the hardened state, foam ratio affects on the density of dry and the compressive strength but doesn't affect on flexural and tensile strength. In the results of response surface analysis, to obtain target performance, the most suitable mix condition for lightweight foamed concrete using bottom ash was water ratio of 70$\sim$80% and foaming ratio of 90$\sim$100%.

A Study on Manufacturing Method of Standard Void Specimens for Non-destructive Testing in RFI Process and Effect of Void on Mechanical Properties (RFI 공정 부품 비파괴검사용 표준 기공률 시편 제조 방법 및 기공률에 따른 기계적 물성 영향에 대한 연구)

  • Han, Seong-Hyeon;Lee, Jung-Wan;Kim, Jung-Soo;Kim, Young-Min;Kim, Wee-Dae;Um, Moon-Kwang
    • Composites Research
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    • v.32 no.6
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    • pp.395-402
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    • 2019
  • The RFI process is an OoA process that fiber mats and resin films are laminated and cured in a vacuum bag. In case that resin film is insufficient to fill empty space in fibers, it makes void defect in composites and this void decrease mechanical properties of the composites. For this reason, non-destructive testing is usually used to evaluate void of manufactured composites. So, in this study, a manufacturing method of standard void specimens, which are able to be used as references in non-destructive testing, was proposed by controlling resin film thickness in the RFI process. Also, a fiber compaction test was proposed as a method to set the resin film thicknesses depending on target voids of manufacturing panels. The target void panels of 0%, 2%, and 4% were made by the proposed methods, and signal attenuation depending on void was measured by non-destructive testing and image analysis. In addition, voids of specimens for tensile, in-plane, short beam and compressive tests were estimated by signal attenuation, and mechanical properties were evaluated depending on the voids.

Study on Corrosion Characteristic of New Nb-containing Zr based Alloys for Fuel cladding (Nb 첨가 핵연료피복관용 Zr 신합금의 부식특성 연구)

  • Choe, Byeong-Gwon;Ha, Seung-Won;Jeong, Yong-Hwan
    • Korean Journal of Materials Research
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    • v.11 no.5
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    • pp.405-412
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    • 2001
  • Corrosion tests were carried out in $360^{\circ}C$ water and $360^{\circ}C$ 70ppm LiOH solution to investigate the corrosion behavior of new zirconium alloys (Zr-0.4Nb-0.8Sn-xFeCrMn, Zr-0.2Nb-1.1Sn-xFeCrMn, Zr-1.0Nb-xFeCu). Microstructures of tested alloys were analyzed by optical microscope and TEM. The cross-sectional surface and crystalline structure of the oxide layer were analyzed by SEM and XRD. From the results of corrosion test, all the alloys showed higher corrosion rates in $360^{\circ}C$ 70ppm LiOH aqueous solution thats in $360^{\circ}C$ water. Especially, high Nb-containing alloy exhibited the acceleration of corrosion rate in LiOH solution. The low Nb- and Sn-added alloys showed better corrosion resistance than the Sn- free high Nb alloy. from the effect of final annealing on the corrosion, it was observed that the partially recrystallized alloys showed better corrosion resistance than fully recrystallized alloys. This would be related to the size and distribution of the second phase particles.

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Optimum Mix of Extrusion panel Using Low Energy Curing Admixture (LA) based on Ground Granulated Blast-Furnace Slag and Ladle Furnace Slag (고로슬래그와 환원슬래그를 기반으로 한 저에너지양생용 결합재를 사용한 압출성형패널의 최적배합)

  • Kim, Ha-Seog;Baek, Dae-Hyun;Lee, Sea-Hyun
    • Resources Recycling
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    • v.24 no.2
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    • pp.13-22
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    • 2015
  • $CO_2$ emitted from building materials and construction materials industry reaches about 67 million tons, which occupy about 30 % of $CO_2$ emitted from the construction field. Controls on the use of consumed fossil fuels and reduction of emission gases are essential for the reduction of $CO_2$ in the construction area as we reduce the second and third curing to emit $CO_2$ in the construction materials industry. Accordingly, this study applied the low energy curing admixture (hereinafter "LA") to the extruded panels to observe the physical properties, depending on the mixing amount of fiber, type of fiber and mixing ratio of fiber. The type of fiber did not appear to be a main factor to affect strength, while the LA mixing ratio and mixing amount of fiber appeared to be major factors to affect strength. Especially, the highest strength was developed when the LA mixing ratio was 40%, whereas the test object with the mixing ratio of 50% resulted in the decrease of strength. In addition, it appeared that the mixing ratio of fiber greatly affected flexural strength and strength increased as the mixing ratio increased.

Properties of Soil Suppressiveness to Cucumber Wilt, caused by Fusarium oxysporum f. sp. cucumerinum Owen (오이 덩굴쪼김병의 발병(發病)을 억제(抑制)하는 토양(土壤)의 특성(特性)에 관(關)하여)

  • Park, Chang-Seuk;Cho, Yong-Sup
    • Korean journal of applied entomology
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    • v.24 no.2 s.63
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    • pp.85-95
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    • 1985
  • It has been tried to find effective biological control measures involved in nature of soil suppressiveness to fusarium wilt of cncumber caused by Fusarium oxysporum f. sp. cucumerinum Owen. Total 28 soil samples were obtained from Jinju, Haman, Namji, Milyang and Suncheon vinyl house area. The disease response of test soil was quantified in terms of DI50 value which caculated from log-probit transformation of diseases response curves. Soils designated 5 from Jinju, 7 from Suncheon, 22 from Namji were recognized as suppressive to fusarium wilt of cucumber. This suppressiveness was completely nullified after autoclave. The disease suppressiveness of tested soil did not indicate any consistency according to either chemical property or texture of soil. Conidial germination, induction and germination of chlamydospore were markedly inhibited in supprerssive soil compared to those in intermediate or conducive soils, however, mycelial lysis did not appear to have direct relationship with disease suppressiveness of given soil. Population density of fluorescent Pseudomonads and Bacillus spp. in the soil originated from different degree of suppressiveness were not different significantly but the number of lytic bacterial plaques measured by triple layer agar method was remarkably higher in suppressive soil than that in intermediate or conducive soil.

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Experimental validations of fire-resistant materials for protecting LPG small storage tank from building fires (건물 화재 시 LPG소형저장탱크 보호용 화재 저항 재료 성능 실증)

  • Kim, Seung-Hwan;Kim, Kyung-Sik;Heo, Seung-Geon;Lee, Jae-Hun
    • Journal of the Korean Institute of Gas
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    • v.24 no.4
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    • pp.18-24
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    • 2020
  • The purpose of this study is to validate thermal hinderance effects, i.e., feasibilities, of fire-proof structure for LPG tank exposed to fire from adjacent burning building. The panel materials suggested for the fire-proof structure are (1) 10 mm-thick wood, (2) wood with fireproof coating, (3) 75 mm-thick Expanded Polystyrene, (4) 75 mm-thick glass wool filled sandwich panel, and (5) 75 mm-thick autoclaved lightweight concrete. The square planar fire source of 1 ㎡, a matrix of nozzles releasing 120-140 g/s of LPG, is used to heat up the wall and the tank beyond, mimicking heat transfer from burning exterior wall finishes. The feasibility is tested by inspecting structural integrity after test, and then by examining temperatures at both sides of panels and tank's front surface as well as heat fluxes. As a result, it can be concluded that, among the suggested sample materials, fire-proof wall with ALC panel only showed the feasibility for explosion prevention with the proven evidences of structural integrity and least increase in temperature of tank.

Therapeutic Effect of Hovenia dulcis Thunberg Extracts and 6 Types Herbal Extracts on $CCl_4-induced$ Chronic Organ Damages in the Rats-Liver and Kidney (Carbon Tetrachlorid으로 유발된 Rat의 만성 장기(간, 신장) 손상시 헛개나무열매 추출물등 6종 생약의 투여시 조직병리학적변화)

  • Lim, Mee-Kyoung;Kim, Joo-Wan;Kim, Hong-Tae;Lee, Byoung-Je;Ku, Sae-Kwang;Kang, Mi-Young;Lee, Keun-Woo
    • Journal of Veterinary Clinics
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    • v.24 no.3
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    • pp.384-391
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    • 2007
  • This study was conducted to clarify the effects of the Korean raisin (Hovenia dulcis Thunb) extracts and polyherbal extracts consisted of 6 types herbal extracts including HDT (HDTmix) on $CCl_4$ induced organ damages. Extracts were prepared by autoclave ($121^{\circ}C$, 15 psi, 3 hours) and filtered with nylon cloth and filter paper then freezing dried. Male Sprague-Dawley rats $(200^{\circ}{\ae}20g)$ were used as experimental groups, which were divided into 5 groups; intact control group (100 mg/kg), $CCl_4$ dosing group (100 mg/kg), $CCl_4$ dosing after HDT extract dosing group (100 mg/kg), $CCl_4$ dosing after HDTmix dosing group (100 mg/kg), Silymarin dosing group (5 mg/kg) after all test articles were orally dosed once a day for 28 days. They were sacrifiled under ether anesthesia. HDT extracts and HDTmix dramatically inhibits the $CCl_4$ intoxicated hepato/nephropathies with immuno-suppress changes on the spleen. They showed more dramatical protective effects on most of specific organs compared to that of Silymarin 5 mg/kg except for hepatoprotective effects in which, quite similar effects were detected. In addition, HDT extracts showed synergic effects with other types of herbal extracts because HDTmix showed more favorable protective effects on the all specific organs showing $CCl_4-related$ histopathological changes compared to HDT extracts.

Effect of limestone addition on mechanical properties of ceramic tiles with fly ash (플라이애시가 첨가된 도자타일 성능에 석회석 함량이 미치는 효과)

  • Lee, Jin-Wook;Han, Kyu-Sung;Hwang, Kwang-Taek;Kim, Jin-Ho
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.28 no.6
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    • pp.256-262
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    • 2018
  • A great amount of fly ash, which is a waste from a thermal power plant, has not been appropriately recycled until now. Landfill of flay ash causes environmental pollution and enormous economic costs. In this study, manufacturing of architectural ceramic tile was investigated replacing fly ash with clay raw material. The properties of porcelain tile was analyzed after manufacturing porcelain tile with mineral based glaze and fast firing process. In particular, the effect of the fly ash addition on the properties of ceramic tile was investigated by increasing the amount of limestone addition. Porcelain tile with fly ash showed excellent bending strength, water absorption, warping and abrasion resistance. However, a significant decrease in durability was observed through the autoclave test. Addition of limestone increased the water absorption, twisting and hydration expansion of the ceramic tile, but it was confirmed that the durability of the ceramic tile with fly ash was greatly improved. In conclusion, recycled architectural ceramic tiles, which can meet domestic construction standards, could be manufactured with the addition of fly ash and limestone.