• Title/Summary/Keyword: autoclave method

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AN EXPERIMENTAL STUDY ON THE PRODUCTION OF HIGH-STRENGTH CONCRETE PILE IN SITE (현장생산용 고강도 콘크리트 파일에 관한 실험적 연구)

  • 박칠림;권영호;백명종;이상수;정도순
    • Proceedings of the Korea Concrete Institute Conference
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    • 1995.04a
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    • pp.183-188
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    • 1995
  • Up to date, high-strength concrete pile which is producing in factory sells in the market. But according to the site and the construction conditions, the system to produce high-strength concrete pile directly in site is utilized in advanced country. Such the production system is the technique phenomenon very disirable in the side of quality control in site and the construction schedule, the time and the cost saving. This study is a fundamental experiment including concrete mixing design, non-autoclave curing method and the optimum condition to produce high-strengh concrete pile in site. As results of this study, High-strength concrete pile in site which target strength is 400kg/ $\textrm{cm}^2$ is able to produce it with optimum curing ciondition(75$^{\circ}C$, 9hr)and mixing design.

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Influence of Bonding Strength on Surface Pattern in Bonding of Carbon Fiber Reinforced Plastic and Metal (탄소 섬유 강화 플라스틱과 금속의 접합에서 표면 패턴에 따른 접합 강도 영향)

  • Kim, Ji-Hun;Cheong, Seong-Kyun;Kim, Joohan
    • Journal of the Korean Society of Manufacturing Technology Engineers
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    • v.26 no.4
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    • pp.430-435
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    • 2017
  • The effect of the surface profile on CFRP and aluminum metal bonding was studied. A small number of steps were made on the aluminum surface, and the shear stress and elongation were measured using a shear test after bonding with an autoclave method. As the number of surface steps increased, the shear stress and elongation increased. The surface bonding strength increased because of the effect of the mechanical and chemical bonding. When the number of effective stages was exceeded, the shear strength decreased again due to the aspect ratio of the step and the reduction of the penetration effect of the resin into the groove.

Synthesis of Carbon Nanotubes by Chemical Method at Warm Temperatures (탄소나노튜브의 중저온에서의 화학적 합성)

  • Ahn, Jung-Ho;Lee, Sang-Hyun;Kim, Yong-Jin;Chung, Byung-Sik
    • Journal of Powder Materials
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    • v.13 no.5 s.58
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    • pp.305-312
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    • 2006
  • Amorphous carbon nanotubes were synthesized by a reaction of benzene, ferrocene and Na mixture in a small autoclave at temperatures as low as $400^{\circ}C$. The resulting carbon nanotubes were short and straight, but their inner hole was filled with residual products. The addition of quartz to the reacting mixture considerably promoted the formation of carbon nanotubes. A careful examination of powder structure suggested that the nanotubes in this process were mainly formed by surface diffusion of carbon atoms at the surface of solid catalytic particles, not by VLS(vapor-liquid-solid) mechanism.

Synthesis of Yttrium Oxide Nanowire by Hydrothermal Method (수열합성법을 이용한 이트륨 산화물 나노와이어의 합성)

  • Kim, Kyung-Ki;Kim, Yong-Jin;Ahn, Jung-Ho
    • Journal of Powder Materials
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    • v.18 no.1
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    • pp.73-77
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    • 2011
  • $Y(OH)_3$ nanowires were synthesized by a hydrothermal reaction of metallic Y with aqueous solution of LiOH. The morphology and the size of the nanowires changed with varying the volume of the LiOH solution inside the autoclave. $Y(OH)_3$ nanowires transformed to $Y_2O_3$ by a subsequent heat-treatment without morphological change. By a proper control of hydrothermal reaction parameter and heat-treatment, the yield of pure $Y_2O_3$ nanowires up to 97% was attained.

Synthesis and Industrial Application of Dimer Acid(1);Synthesis of Dimer Acid with Clay Catalyst (다이머산 합성 및 공업적 응용성(제1보);점토촉매하에서 다이머산의 합성)

  • Yoon, Young-Kyoon;Jeong, Noh-Hee;Nam, Ki-Dae
    • Journal of the Korean Applied Science and Technology
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    • v.16 no.2
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    • pp.135-141
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    • 1999
  • A synthesis of Dimer acid was studied from a tall oil fatty acid. Catalytic activity measured as reactant conversion in a autoclave reactor increase in accordance with the acidity. The optimization of process conditions were tested by an experimental design method. Optimization synthetic conditions of dimer acid and were reaction of tall oil fatty acid during 2 hour at $250^{\circ}C$, used of 7.3 wt% active clay and $1.2{\sim}1.4wt%$ water, and found reation pressure $8{\sim}9Kg/cm^2$. The maximum conversion rate was researched $74{\sim}76%$.

Residual Stresses in Thick Fabric Composite Rings with Respect to Compaction (압착에 따른 원환체 형상의 두꺼운 직물 복합재 내부의 잔류응력)

  • Kim Jong Woon;Kim Hyoung Geun;Lee Dai Gil
    • Proceedings of the Korean Society For Composite Materials Conference
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    • 2004.10a
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    • pp.139-142
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    • 2004
  • The fabric composite rings for nozzle parts of solid rocket motors should be thick to endure high temperature and pressure of combustion gas. Since the thermal residual stresses developed during manufacturing of the axi-symmetric composite structures increase as the thickness increases and eventually induce failures during storage and operation, the estimation of the residual stresses is indispensable for design and manufacture of the thick composite nozzle parts. In this paper, thick fabric rings made of carbon fabric phenolic composites were fabricated in a hydroclave and in an autoclave using a multi-step pre-compaction process to minimize draping. The residual stresses distributed in the rings were measured by the radial-cut method and it was found that the compaction reduces the residual stresses in the composite ring.

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A Study on Property of Thermoset Composite in FPS Process (FPS 공정에 의한 열경화성 복합재 유효성 검증 연구)

  • Kim J-H;Um M-K;Byun J-H;Lee S-K;Jeon Y-J
    • Proceedings of the Korean Society For Composite Materials Conference
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    • 2004.10a
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    • pp.241-245
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    • 2004
  • Among the various manufacturing processes of composites, the tape lay-up process of thermoset prepreg has many advantages compared to autoclave or hot press forming. It has a high potential to process automation and continuous fabrication .. Fiber placement developed as a logical combination of filament winding and automated tape placement to overcome some of the limitations of each manufacturing method. Fiber placement uses a compaction device to apply direct contact between the incoming materials in the fiber placement head and Heat is added to the materials at the nip point of the compaction roller. This paper will discuss property of thermoset composite as compaction and heat effect in Automated fiber placement

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A Study on the Evaluation of the properties change of Aircraft Composites Parts During Repair by Thermal Analysis Test (열분석시험을 통한 항공기 복합재료 부품의 수리 시 반복경화에 따른 물성변화 측정에 관한 연구)

  • 엄수현;이상언;한중원;김국진;김영식;김윤해
    • Proceedings of the Korean Society For Composite Materials Conference
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    • 2002.10a
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    • pp.33-37
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    • 2002
  • Recently, composites have been widely applied in the sporting goods, automobile, aerospace industry. As the use of advanced composites increase, specific techniques have been developed to repair damaged composite structures. In order to repair the damaged part, it is required that the material in the damaged area be removed first by utilizing the proper method, and prepreg be laid up in the area and cured under vacuum using the vacuum bagging materials. In curing process, either in an oven or autoclave is to be delamination can be occurred in the sound areas during and/or after the exposure to the elevated curing temperature in case that the repair process is repeated. Therefore, this study was conducted to evaluate the degree of degradation of properties of the cured parts and how it affects to the delamination phenomenon between laminated skin and honeycomb core.

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Slippage Effects on the Curvature Shape of Unsymmetric Laminates (비대칭 적층판의 곡률형상에 대한 미끄러짐 효과)

  • Roh, Hee-Yuel;Cho, Maeng-Hyo
    • Proceedings of the KSME Conference
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    • 2000.11a
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    • pp.420-425
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    • 2000
  • The room-temperature shapes of cured unsymmetric composite laminates have out-of-plane warping after autoclave processing. In addition, they exhibit two stable room-temperature configurations due to snap-through phenomena when the side length of laminates exceeds a critical value. The cured shapes of unsymmetric laminates are influenced by many environmental factors. Experiments show that the effect of too-plate cannot be ignored and has significant influence on the cured shape of unsymmetric laminates. In this present study, approximations to the strain fields are used in the expression for the total potential energy and the Rayleigh-Ritz method is applied. The slippage effects resulting from the interaction between the laminates and the tool-plate are considered. By introducing a dimensionless slippage coefficient and correlating the corresponding value with experimental results, the influence of processing parameters is investigated. Modeling is extended to predict curvatures of plate configurations with various aspect ratio.

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Hydrocarbon Synthesis of Waste Lignocellulosics by Liquefaction Reaction of Thermochemical Deoxyhydrogenolysis Method(I) (목질폐재(木質廢材)의 열(熱)-화학적(化學的) 탈(脫)산소-수소첨가반응(환원반응)에 의한 액화(液化)탄화수소의 합성(I))

  • Lee, Byung-Guen
    • Journal of the Korean Wood Science and Technology
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    • v.18 no.4
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    • pp.79-85
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    • 1990
  • Many kinds of acetosolv lignin including ricestraw and spruce lignin were pyrolyzed. and liquefied in the autoclave reactor using 50% tetralin and m-cresol solution respectively as soluble solvent and Co-Mo as catalyst. In order to promote deoxyhydrogenolysis reaction $H_2$ gas was supplied into the reactor. The ratio between lignin and the soluble solvent are lg and 10cc. The reaction conditions are $200^{\circ}-700^{\circ}C$ of reaction temperature, 10-50 atms of reaction pressure and 100-500rpm of the reactor stirrer. By the deoxyhydrogenolysis liquefaction reaction, the main chemical structures of lignin which are aryl-alkyl-${\beta}$-0-4 ether, phenylcoumaran and biphenyl etc. are easily destroyed into liqufied aromatic compounds and aliphatic compunds linked with aromatic compounds. The percent yield of monomeric phenols on the weight bvase of lignin reacted reached to 12-14% by the chemical analytic GC-MS etc.

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