• Analytical Science and Technology
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• v.8 no.4
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• pp.575-582
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• 1995

A new analytical procedure using a serial dual electrode detector was developed for the analysis of amino acids and proteins. Bromine was generated at the upstream electrode and detected by the downstream electrode. The presence of amino acids and proteins was shown to lower the downstream current but with no apparent effect on the upstream current. This indirect mode of detection can be applied to the determination of amino acids and proteins which are electrochemically inactive or too large to be accessible to the electrode surface for electron exchange. The method is shown capable to determine various amino acids (cystine, tyrosine, lysine, tryptophan, glycine, methionine and arginine) and proteins (cytochrome c, hemoglobin, HAS, a-Amylase, Conalbumin I, Catalase and Myglobin) with linear working range for amino acids between $10^{-6}$ to $10^{-3}M$ and total proteins between $10^{-7}$ to $10^{-3}M$. The method has been applied for the analysis of amino acids and total protein in food using Flow Injection Analysis with results obtained comparable to those using the traditional analytical procedure. Use of pulse generation technique was shown to produce a more stable flow injection analysis peaks for repetitive determination than the use of conventional constant current method which showed increase of the background current after determination over 200 minutes. The pulse method was found to give stable baseline even after 400 minutes. Thus, the method is shown able to provide a suitable analytical procedure for automatic analysis of amino acids and proteins in food by flow injection analysis.

• The Transactions of The Korean Institute of Electrical Engineers
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• v.64 no.4
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• pp.545-551
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• 2015

This paper deals with torque analysis of magnetic spur gear with radial magnetized permanent magnets based on analytical method. The analysis is implemented in three parts: First, on the basis of magnetic vector potential and a two-dimensional (2D) polar-coordinate system, the magnetic field solution due to permanent magnet of source gear are obtained. And by using derived magnetic field solutions, the analytical solutions for external magnetic field distribution which affects load gear are obtained. Second, by using coordinate conversion, external magnetic field which is on the primary coordinate system is converted to the secondary coordinate system. Finally, the load gear is reduced to equivalent current densities, and the torque is computed on these currents in the external field of the source magnet. These analytical results are validated by comparing with the 2-D finite element analysis (FEA).

• Journal of Korean Society of Occupational and Environmental Hygiene
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• v.28 no.1
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• pp.108-116
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• 2018

Objectives: This study investigated to the analytical work environment, analyst's expert and status of analytical instrument in the designated organization's laboratory for measuring work environment, and carried out to ensure reliability of analytical results. Methods: This study was conducted by 114 analysts who work in designated organization's laboratory for measuring work environment. Information on the working environment and personal characteristics of the analysts were collected using a self-reported questionnaire and were analyzed using the SPSS program through analysis of frequency and t-test. Results: The speciality of subjects was occupational health(57.0%), environmental health(38.6%) and environmental engineering(4.4%), and they had a higher level of academic ability than workers in other industries. Analysts had to handle a large number of sample analysis and many tasks other than analytical work. The analysts answered that it was difficult to analyze organic substances than inorganic substances, and the difficult parts were the analytical methods setting of new substances(55.3%), instrument analysis(24.6%) and principle of analysis(23.7%). Analytical instruments mainly have legally required instruments. The difficulty of the analysis is solved from the senior analyst in the laboratory and analytical information is mainly exchanged through seminar organized by the Association of Occupational Health Analysts. The analysts who are planning to move or considering the company were 48.2%, and the reasons for moving the company were difficult to work(14.0%), low salary(9.6%), employment type(8.8%) and job stress(7.0%). Conclusions: The conclusions of our study were that it was possible to secure reliability by solving the problems such as implementing professional education to improve expertise of analysts, strengthening analytical instruments through institutional improvement and improving work environment.

• Analytical Science and Technology
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• v.11 no.6
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• pp.499-504
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• 1998

An analytical method for the simultaneous measurement of trace Cu, Sn, and Bi in sea water has been investigated by Inductively Coupled Plasma-Mass Spectrometry. Amberlite IRC-718 resin was used as a solid phase in solid-liquid extraction technique for the removal of matrix interferences such as Na, S, P, and other polyatomic ion species. Recoveries of 99.8% for Cu, 99.6% for Sn, and 97.9% for Bi were obtained for the standard spiked sample. The developed method was applied to analysis of trace metals in sea water.

• Analytical Science and Technology
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• v.15 no.5
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• pp.433-438
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• 2002

Trace elements in two air filters (V-50, P-50) artificially loaded with urban dust provided from IAEA were determined non-destructively using instrumental neutron activation analysis. Standard reference material (Urban Particulate Matter, SRM 1648) of National Institute of Standard and Technology was used for analytical quality control. About 20 elements in both of loaded filter samples were determined. To evaluate inter-laboratory comparison and proficiency test, analytical data were statistically treated with the results which collected from 49 laboratories, 40 countries participated in this study using neutron activation analysis, particle induced X-ray emission, inductively coupled plasma mass spectroscopy, etc,. From the results of statistical treatment, Z-scores are within ${\pm}2$. Furthermore, accuracy and precision of obtained analytical values are passed according to the criteria of the proficiency test. Consequently, it was proved that analytical quality for air dust samples being performed has been controlled properly.

• KCI Concrete Journal
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• v.13 no.2
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• pp.19-25
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• 2001

A simple expression to predict bond strength of reinforcing bars with rib deformation to the surrounding is derived for the case of splitting bond failure. Finite element analysis is used to model the confining behavior of concrete cover. The roles of the interfacial properties, specifically, the friction coefficient, cohesion, the relative rib area and the rib face angle are examined. Values of bond strength obtained using the analytical model are in good agreement with the bond test results from the previous studies. The analytical model provides insight into interfacial bond mechanisms and the effects of the key variables on the bond strength of deformed bars to concrete. Based on the comparison between the analytical results and the test results, the values of cohesion, coefficient of friction, and the effective rib face angle are proposed.

• Transactions of the Korean Society of Mechanical Engineers A
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• v.31 no.7 s.262
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• pp.800-807
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• 2007

Autofrettage process is used for internal forming and sizing of cylinder designed to withstand high internal pressures. Once the tube is autofrettaged, it needs to be machined to its final dimensions both at the bore and its outer surface. This paper presents an analytical analysis and numerical analysis of machined compound cylinder using finite element code, ANSYS10.0. An analytical model for predicting the level of autofrettage following either inner, outer, or combined machining of the compound cylinder is developed for the autofrettage residual stress field is simulated by an autofrettaged pressure. The autofrettaged pressures are obtained by using trying-error method. As autofrettage percentage is 20 % and 40 %, the numerical results are found to be in almost agreement with the analytical ones. However, as autofrettage percentage is 60 %, the numerical results have a little difference with the analytical ones.

• Proceedings of the Computational Structural Engineering Institute Conference
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• 2004.10a
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• pp.503-510
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• 2004

One of the methods improving the seismic behavior of a structure is the frame with reduced beam section (RBS) which cuts a segment of flanges of the beam near the beam-to-column connection so that the section with reduced flanges has smaller flexural strength than the beam end. It is difficult to analyze the RBS frame because RBS portion has circular-cut type flange. And inelastic response of the steel frame with the RBS is very sensitive to the RBS model. In this paper, the analytical models of RBS portion are investigated and the results of the inelastic analysis for RBS analytical models are compared and then the analytical model for RBS is determined based on the results of inelastic analysis. Inelastic behavior of the RBS frame and its dynamic characteristics are investigated for selected analytical model of RBS.

• Steel and Composite Structures
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• v.20 no.6
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• pp.1237-1257
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• 2016

The paper concerns analysis of effects of shrinkage of slab concrete in a steel-concrete composite deck of a through truss bridge span. Attention is paid to the shrinkage alongside the span, i.e., transverse to steel-concrete composite cross-beams. So far this aspect has not been given much attention in spite of the fact that it affects not only steel-concrete decks of bridges but also steel-concrete floors of steel frame building structures. For the problem analysis a two-dimensional model is created. An analytical method is presented in detail. A set of linear equations is built to compute axial forces in members of truss girder flange and transverse shear forces in steel-concrete composite beams. Finally a case study is shown: test loading of twin railway truss bridge spans is described, verified FEM model of the spans is presented and computational results of FEM and the analytical method are compared. Conclusions concerning applicability of the presented analytical method to practical design are drawn. The presented analytical method provides satisfactory accuracy of results in comparison with the verified FEM model.

• Journal of the Korea institute for structural maintenance and inspection
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• v.3 no.1
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• pp.137-146
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• 1999

Analysis of R/C columns requires modeling of the plastic hinge region, as well as nonlinear material characteristics. This becomes a challenging task in view of the nonlinearity of both steel and concrete. Furthermore, formation and progression of plasticity in the hinge is a difficult phenomenan to simulate, especially under reversed cyclic loading and decaying strength conditions. This research provide one analytical model employed in column analysis, including the analysis procedure for establishing inelastic force-deformation relationships. The analytical results show good correlation with experimental data. The employed procedure with the adopted analytical models can be used to compute inelastic displacements of concrete columns with welded reinforcement grids. The inelastic deformability beyond the peak was similar to those indicated by columns with conventional ties. The superior performance of columns with welded grids may be attributed to the improved confinement characteristics of grids associated with increased rigidity of welded ties.