• 제목/요약/키워드: analytical testing

검색결과 442건 처리시간 0.029초

Overview of the Leading Environmental Specimen Banks in the World and Future Challenges of the National Environmental Specimen Bank in Korea (선진국 환경시료은행의 특성 분석을 통한 국가환경시료은행의 발전방안)

  • Lee, Jong-Chun;Kim, Myung-Jin
    • Economic and Environmental Geology
    • /
    • 제45권2호
    • /
    • pp.169-180
    • /
    • 2012
  • The ESBs (Environmental Specimen Banks) have monitoring functions for the contemporary environmental qualities and also offer the future generation tangible information on the past environment by preserving the specimens. This entails the sampling of the representative specimen for each distinctive ecosystem, which is performed under a strict and stipulated procedure and a condition that does not allow any change in the component so that a retrospective analysis can be readily done even in the distant future. It has been more than 30 years that some developing countries started collecting a broad spectrum of specimens to vindicate the effectiveness of an environmental policy and to monitor the long-term variations of background concentrations of environmental pollutants. Though being late, the National Institute of Environmental Research (NIER), Korea, has successfully launched the National Environmental Specimen Bank (NESB) in 2009 equipped with its state-of-the-art automated cryogenic tanks. Since then, the researchers at the NESB have been doing their best to excel the existing ESBs around the world by learning and improving the expertise. To do so, they conducted a pilot study for developing and testing their own Standard Operating Procedure (SOP) based on the analysis of the examples of the other ESBs. The problems from the pilot study had been reviewed to improve the SOP to meet the requirements for an ESB, that is to say, preserving representative environmental specimens in cryogenic condition and enhancing the analytical method. Furthermore, they also need to prepare themselves to address the future challenges by providing some additional functions, which makes it distinguishable from the other ESBs. If successful, this will be a step further to be recognized as a full-fledged member of the ESB society of the world.

The importance of NIR spectroscopy in the estimation of nutritional quality of grains for ruminants

  • Flinn, Peter C.
    • Proceedings of the Korean Society of Near Infrared Spectroscopy Conference
    • /
    • 한국근적외분광분석학회 2001년도 NIR-2001
    • /
    • pp.1612-1612
    • /
    • 2001
  • The production of grain for export and domestic use is one of Australia's most important agricultural industries, and the NIR technique has been used extensively over many years for the routine monitoring of grain quality, particularly moisture and protein content. Because most Australian grain is intended for human food production, the determinants of grain quality for livestock feed, apart from protein, have been largely ignored. However the increasing use of grain for feeding to pigs, poultry, beef cattle and dairy cows has led to an important national research project entitled “Premium Grains for Livestock”. Two of the objectives of this project are to determine the compositional and functional characteristics of grains which influence their nutritional quality for the various classes of livestock, and to adopt rapid and objective analytical tests for these quality criteria. NIR has been used in this project firstly to identify a set of grain samples from a large population of breeders' lines which showed a wide spectral variation, and hence a potentially wide variation in nutritional value. The selected samples were not only subjected to an extensive array of chemical, physical and in vitro analyses, but also were grown out to produce sufficient quantities of grain to feed to animals in vivo studies. Additional grains were also strategically selected from farms in order to include the effect of weather damage, such as rain, drought and frost. In this study to date, NIR calibrations have been derived or attempted, on both ground and whole grains, for in vivo dry matter digestibility (DMD), pepsin-cellulase dry matter disappearance, protein, fat, acid detergent fibre, neutral detergent fibre, starch, in sacco DMD and in vitro assays to simulate starch digestion in the lumen and small intestine. Results so far indicate high calibration accuracy for chemical components (SECV 0.3 to 2.6%) and very promising statistics for in vivo DMD (SECV 1.8, $R^2$ 0.93, SD 7.0, range 61.9 to 92.3, n=60). There appears to be some potential for NIR to estimate some in vitro properties, depending upon the accuracy of reference methods and appropriate sample populations. Current work is in progress to extend the range of grains with in vivo DMD values (a very laborious and expensive process) and to increase the robustness of the various NIR calibrations, with the aim of implementing uniform testing procedures for nutritional value of grains throughout Australia.

  • PDF

A Study of the Vibration Characteristics of a Haptic Vibrator for Horizontal and Vertical Magnetization (수평 및 수직 착자에 대한 햅틱 진동자의 진동특성에 관한 연구)

  • Ko, Dong Shin;Hur, Deog Jae;Park, Tae Won;Lee, Jai Hyuk;Lee, Sung Su
    • Transactions of the Korean Society of Mechanical Engineers A
    • /
    • 제39권4호
    • /
    • pp.415-421
    • /
    • 2015
  • This paper describes the study of the design procedure for the step-by-step setup parameters and of the magnetizing method for performance and size reduction in the development of a haptic vibrator. The study of magnetization was accomplished by comparing the electromagnetic force in accordance with the horizontal and the vertical magnetization. The theoretical results indicated that the horizontal magnetization resulted in a better performance. The systematic design of a step-by-step procedure for establishing the design parameters was verified by testing the characteristics of the fabricated prototype product. The vibration response function analysis and electric field analysis were processed by decoupling of the analytical method, and these were determined to be in good agreement with the test results. The design parameters to contributing to the product reliability included the spring height, the welding position, and the coil position. The sensitivity of the electromagnetic field and the performance change were analyzed based on the design parameters. As a result, we proposed a design method to implement a reliability-based, high performance haptic vibrator.

Isolation and Chemical Structure Identification of Allelopathic Substances from the Ginkgo(Ginkgo biloba L.) Leaf Waste Produced by Phamaceutical Process (제약폐기 은행잎중에 함유된 식물생육억제물질 분리동정)

  • Seong, Ki-Seog;Kim, Bok-Jin;Kwon, Oh-Kyung;Choi, Du-Hoi
    • Korean Journal of Soil Science and Fertilizer
    • /
    • 제30권4호
    • /
    • pp.377-383
    • /
    • 1997
  • Studies were conducted on the nature of allelopathic effect of the substances in the waste of ginkgo leaves from pharmaceutic factory. In the first step, to find out whether there was any allelophatic effect, young seedlings of radish and rice were grown in the water (crude) extract of ginkgo leaf waste and in different liquid/lquid partitioned fractions of EtOAc at pH 9, EtOAc at pH 3, and BuOH. As second step, attempts were made to isolate and identify the allelophatic substance in different liquid/liquid partitioned fractions using GC/MS and NMR techniques. The water (crude) extract of ginkgo leaf waste retarded the growth of radish seedlings under 10% concentration. In case of rice seedlings, the water extract of ginkgo leaf extract showed adverse effect on the growth when combined with $3.3{\times}10^{-6}M$ gibberellin A3. All of the liquid/liquid fractions of crude extract showed strong retardation of seedling growth of radish and rice at the concentration of 1%. Allelophatic substance was isolated from the crude extract using liquid/liquid partition, column chromatography and HPLC techniques. The analytical results of isolated componet using GC/MS and NMR proved that the allelophatic substance in the ginkgo leaf wastes is catechol; one of phenol compounds. Based on the experiences current study, a practical method for the testing of allelophatic effect of crude extract of some materials was proposed. In this method, rice seeds were allowed to sprout until the length of coleoptile to reach 0.5 mm. Such seedlings were submerged in the solution containing supposedly allelophatic substance and the length of shoot and root was measured 3 days after treatment.

  • PDF

Experimental Study on Dynamic Behavior of a Titanium Specimen Using the Thermal-Acoustic Fatigue Apparatus (열음향 피로 시험 장치를 이용한 티타늄 시편의 동적 거동에 관한 실험적 연구)

  • Go, Eun-Su;Kim, Mun-Guk;Moon, Young-Sun;Kim, In-Gul;Park, Jae-Sang;Kim, Min-Sung
    • Journal of the Korean Society for Aeronautical & Space Sciences
    • /
    • 제48권2호
    • /
    • pp.127-134
    • /
    • 2020
  • High supersonic aircraft are exposed to high temperature environments by aerodynamic heating during supersonic flight. Thermal protection system structures such as double-panel structures are used on the skin of the fuselage and wings to prevent the transfer of high heat into the interior of an aircraft. The thin-walled double-panel skin can be exposed to acoustic loads by supersonic aircraft's high power engine noise and jet flow noise, which can cause sonic fatigue damage. Therefore, it is necessary to examine the behavior of supersonic aircraft skin structure under thermal-acoustic load and to predict fatigue life. In this paper, we designed and fabricated thermal-acoustic test equipment to simulate thermal-acoustic load. Thermal-acoustic testing of the titanium specimen under thermal-acoustic load was performed. The analytical model was verified by comparing the thermal-acoustic test results with the finite element analysis results.

Southern Analysis after Long-range PCR: Clinical Application in Korean Patients with Myotonic Dystrophy 1

  • Yum, Mi-Sun;Lee, Beom Hee;Kim, Gu-Hwan;Lee, Jin-Joo;Choi, Seung Hoon;Lee, Joo Yeon;Kim, Jae-Min;Kim, Yoo-Mi;Ko, Tae-Sung;Yoo, Han-Wook
    • Journal of Genetic Medicine
    • /
    • 제10권1호
    • /
    • pp.33-37
    • /
    • 2013
  • Purpose: Myotonic dystrophy 1 (DM1, OMIM 160900) is an autosomal-dominant muscular disorder caused by an expansion of CTG repeats in the 3' UTR of the DMPK gene. Variable expansions of CTG repeats preclude the accurate determination of repeat size. We tried to show the clinical and analytical validity of the application of Southern blotting after long-range PCR was demonstrated in Korean DM1 patients. Materials and Methods: The Southern blotting of long-range PCR was applied to 1,231 cases with clinical suspicion of DM1, between 2000 and 2011. PCR was performed using genomic DNA with forward 5'-CAGTTCACAACCGCTCCGAGC-3' and reverse 5'-CGTGGAGGATGGAACACGGAC-3' primers. Subsequently, the PCR fragments were subjected to gel electrophoresis, capillary transfer to a nylon membrane, hybridization with a labeled (CAG)10 probe. The correlation between clinical manifestations and the CTG repeat expansions were analyzed. Results: Among a total of 1,231 tested cases, 642 individuals were diagnosed with DM1 and the range of the detected expansion was 50 to 2,500 repeats; fourteen cases with mild DM1 ($75{\pm}14$ repeats), 602 cases with classical DM1 ($314{\pm}143$ repeats), and 26 cases with congenital DM1 ($1,219{\pm}402$ repeats). The positive and negative predictive values were 100%. The age at test requested and the CTG repeat numbers were inversely correlated (R=-0.444, P<0.01). Conclusion: This study indicates that Southern blotting after long-range PCR is a reliable diagnostic method DM1.

Directions towards sustainable agricultural systems in Korea

  • Kim, Chang-Gil
    • Proceedings of the Korean Society of Crop Science Conference
    • /
    • 한국작물학회 2017년도 9th Asian Crop Science Association conference
    • /
    • pp.3-3
    • /
    • 2017
  • The question of how to establish sustainable agricultural systems has become as prominent as questions related to water, energy and climate change. High input/high output agriculture has brought with it many adverse effects; the massive deterioration of soil and water in both quantity and quality, increased greenhouse gas emissions and an increased prevalence of unsafe foods. Additionally, urbanization and climate change has worsened the shortage of farmland and reduced the supply of agricultural water. Given these challenges, maintaining, conserving and efficiently using agri-environmental resources, through fostering of sustainable agriculture, have emerged as key tasks in solving these problems. What is needed therefore is research, based on systematic and comprehensive empirical analyses, that can propose plans and methods for establishing an appropriate sustainable agricultural system. The empirical analysis of sustainable agricultural system is approached separately from economic, environmental and social aspects. An analysis of environment effect reveals that the available phosphate level is 1.3~2.1 times greater than the optimal amount in rice paddies, upland fields and orchards. Further examination has revealed that the excess nutrient is polluting both ground water and surface water. Analytical results for economic feasibility show that factors of production have been invested heavily in the rice crop. Under these conditions, sustainable agriculture, including low-input agriculture, appears to be a possible alternative that will facilitate simultaneous improvements in both economic feasibility and environment effects. Analysis results for sociality reveal that social factors include the value of producer, association and interior networks. Social conditions are comprised of leadership, consumers' awareness, education and conflict solutions. In addition, analysis as to the degree investments contribute to improving agricultural value added has revealed that the direct payment program is the most effective instrument. Experts confirm that economic feasibility can be improved by scientific and well-reasoned nutrient management on the basis of soil testing. Farmers pointed to 'economic factors' as being the largest obstacle to switching to the practice of sustainable agriculture. They also indicate 'uncertainty with regards to sustainable agriculture technology' as an impediment to practicing sustainable agriculture. Even so, farmers who believe environmental and regional issues to be the most pressing problems have expanded their practice of sustainable agriculture. The keys to establishing sustainable agriculture system are classified into the following four aspects. Firstly, from an economic aspect, the research indicates that agricultural policy needs to be integrated with environmental policy and that the function of market making based on the value chain needs to be revitalized. Secondly, from an environmental aspect, there is a need for an optimal resource management system to be established in the agricultural sector. In addition, sustainable agriculture practice will need to be extended with attendant environmentally-friendly and sustainable intensive technology also requiring further development. Thirdly, from a social aspect, green agriculture management needs to be fostered, technology and education extended, and social conflict mediated. Lastly, from a governance aspect, it will be necessary to strengthen good governance, assign and share suitable roles and responsibilities, build a cooperation system and utilize community supported agriculture.

  • PDF

Piezocone Neural Network Model for Estimation of Preconsolidation Pressure of Korean Soft Soils (국내 연약지반의 선행압밀하중 추정을 위한 피에조콘 인공신경망 모델)

  • 김영상
    • Journal of the Korean Geotechnical Society
    • /
    • 제20권8호
    • /
    • pp.77-87
    • /
    • 2004
  • In this paper a back-propagation neural network model is developed to estimate the preconsolidation pressure of Korean soft soils based on 176 oedometer tests and 63 piezocone test results, which were compiled from 11 sites - western and southern parts of Korea. Only 147 data were used for the training of the neural network and 29 data, which were not used during the training phase, were used for the verification of trained network. Empirical and theoretical models were compared with the developed neural network model. A simple 4-4-9-1 multi-layered neural network has been developed. The cone tip resistance $q_T$ penetration pore pressure $u_2$, total overburden pressure $\sigma_{vo}$ and effective overburden pressure $\sigma'_{vo}$ were selected as input variables. The developed neural network model was validated by comparing the prediction results of the proposed neural network model for the new data which were not used for the training of the model with the measured preconsolidation pressures. It can also predict more precise and reliable preconsolidation pressures than the analytical and empirical model. Furthermore, it can be carefully concluded that neural network model can be used as a generalized model for prediction of preconsolidation pressure throughout Korea since developed model shows good performance for the new data which were not used in both training and testing data.

Characterization of the Kaolinite Synthesized According to the pH. (pH에 따른 캐올리나이트 합성과 특성 분석)

  • Ryu, Gyoung-Won;Jang, Young-Nam;Bae, In-Kook;Suh, Yong-Jae
    • Economic and Environmental Geology
    • /
    • 제41권2호
    • /
    • pp.165-172
    • /
    • 2008
  • Kaolinite [$Al_2Si_2O_5(OH)_4$] used in these experiments was synthesized at 250$^{\circ}C$ for 36 hrs by a hydrothermal process from amorphous $Al(OH)_3$ and $SiO_2$. The change of the mineralogical properties of the phase synthesized were observed in the pH range 2 to 9. The synthetic kaolinite were characterized by the analytical methods of XRD, IR, DIA, and FE-SEM. Kaolinite was obtained in a wide range of pH. The phases with high- to midium- defect kaolinite with high thermal stability were obtained from the acidic conditions and high-defect kaolinite with low thermal stability from the basic conditions. These variations of kaolinite properties appears to be related to the pH dependence of kaolinite surface speciation. The peaks intensity and resolution of the kaolinite decrease according to the alkalinity of the solution by the results of the IR testing. And the peak intensity increases in the 60 to 70$^{\circ}C$ range due to dehydration reaction observed by TG-DTA. Such phenomena was the result of increase of unreacted amorphous materials in the high pH condition, which could be identified by FE-SEM.

A Study on the Economic Feasibility Analysis of Cosmetics Beauty Industrialization Center

  • Kim, Ji-In;Park, Jeong-Min
    • Journal of the Korea Society of Computer and Information
    • /
    • 제25권2호
    • /
    • pp.221-229
    • /
    • 2020
  • As the cosmetics beauty industry grows into a key next-generation industry, the establishment of an industrialization center is needed, but failure to verify the adequacy and feasibility of the investment could lead to financial burdens. In this study, the project costs and facilities of an industrial center are reviewed to analyze its economic feasibility based on the cost estimates, revenue estimates, estimated profit or loss calculations, and estimated operating cash flows. The profit estimation criteria were analyzed by applying 90 per cent of expected orders for research projects (24 billion won) and 12 per cent of rental rates for testing equipment (4.5 billion won for construction), and the benefit/cost ratio is higher than 1.02 per cent and the net present value is higher than '0' won, and the internal rate of return is also more than 5.06 per cent for all three analytical methods. Therefore, in order for the construction of a cosmetics beauty industrialization center to be economically feasible, it is necessary to maintain research project orders of more than 90 percent and return on equipment rent of more than 12 percent, and a strategic approach is needed to diversify business profits.