• Title/Summary/Keyword: analytical testing

Search Result 442, Processing Time 0.022 seconds

A Study on the Characteristics of VOC Removal by Cordierite Filter Loaded with Catalyst (촉매를 담지한 코디어라이트 필터의 VOC 제거 특성에 관한 연구)

  • Chung, Kyung-Won;Kim, Yong-Nam;Park, Jeong-Hyun;Choi, Beom-Jin;Cho, Eul-Hoon;Lee, Hee-Soo
    • Analytical Science and Technology
    • /
    • v.15 no.3
    • /
    • pp.263-269
    • /
    • 2002
  • After porous filters were manufactured using cordierite powder whose mean particle size was 200 ${\mu}m$, they were loaded with catalysts such as Pt, Pd, Cu, Co, La, $V_2O_5$ by vacuum impregnation method. And we investigated the activity of catalysts used for catalytic oxidation of VOC by passing toluene through catalyst-loaded filters. The porous filters had the apparent porosity of 62%, the compressive strength of about 10 MPa and the pressure drop of 15 mmHg at the face velocity of 5 cm/sec. The loading of catalyst decreased the porosity of the filters and increased the pressure drop and the compressive strength of them. Among the catalysts, Pt had the highest activity for catalytic oxidation and could remove more than 90% of toluene at 250 $^{\circ}C$. Below 250 $^{\circ}C$, the content of Pt catalyst had an influence on the conversion of toluene but didn't show any influence above 250 $^{\circ}C$.

Study on the unification between KS I ISO standard and official test method enacted by Korean Ministry of Environment - drinking water and indoor air quality - (환경오염공정시험기준과 KS ISO규격의 일원화에 관한 연구 - 먹는 물 및 실내공기질 -)

  • Lee, Jeong-Il;Lee, Ju-Hee;Lee, Jeong-Hee;Lee, Jun-Hee;Lee, Won-Seok;Kim, Ji-In;Kim, Bo-Kyung;Choi, Sung-Hun
    • Analytical Science and Technology
    • /
    • v.25 no.2
    • /
    • pp.102-113
    • /
    • 2012
  • Our study researched on unification of KS I ISO standard harmonized with ISO and Official Test Method enacted by Korean Ministry of Environment-drinking water and indoor air quality. We reviewed KS methods related to drinking water and indoor air quality for about 23,000 KS methods. KS methods related environmental field are classified as KS I, total 635 methods and 583 KS I methods were harmonized with ISO. For Environmental Standard methods for drinking water, 100 methods were reviewed according to 232 KS methods related to ISO/ TC 147 "Water Quality". Environmental Standard methods for indoor air quality were reviewed according to 95 KS standard methods related to ISO/TC 146 "Air Quality". By reviews and comparison tests for unifiable ES for drinking water and indoor air quality with KS methods harmonized with ISO, it was evaluated that for 100 ES methods for drinking water, 23 ES methods were unification complete, 29 ES methods were unification possible, 12 ES methods were unification impossible, no corresponding methods were found in KS I ISO for 36 ES methods and for 17 ES methods for indoor air quality,1 ES methods were unification complete, 3 ES methods were unification possible, 3 ES methods were impossible, no corresponding methods were found in KS I ISO for 10 ES methods.

Proficiency testing of cadmium and lead in polypropylene resin (폴리프로필렌 수지 중 카드뮴과 납 측정 숙련도시험)

  • Cho, K.H.;Lim, M.C.;Min, H.S.;Han, M.S.;Song, H.J.;Park, C.J.
    • Analytical Science and Technology
    • /
    • v.20 no.3
    • /
    • pp.183-192
    • /
    • 2007
  • The various environmental regulation directives such as RoHS (restriction of hazardous substances in electrical and electronic products) and WEEE (waste from electrical and electronic equipments) are practically used as the technical barrier in international trade (TBT) of vehicles and electrical and electronic products recently. Regarding such an environmental regulation, Korea Research Institute of Standards Science (KRISS) organized a proficiency testing scheme to establish the reliability of measurement results produced by the relevant research institutes and test laboratories in Korea. Participants were 31 laboratories related to production of the electrical and electronic equipments and mobile vehicles. Two polypropylene samples of pellet type were employed as the proficiency testing materials (PTMs). Cadmium and lead were the analytes chosen among six components regulated in European Union (EU) RoHS directive. The PTMs were sent to the participants by post on September $1^{st}$ 2006, and deadline for results submission were October $10^{th}$ 2006. The results of each laboratory were evaluated in comparison with KRISS reference values using Robustic Z-score and Youden plot methods. The results of the various sample digestion methods were also compared. Most of participants reported good agreement within 10 % range of reference values. However, results from several laboratories showed significant biases from reference values. These laboratories should establish the quality assurance system for improvement of the measurement reliability.

Dynamic Properties of a Lowrise Masonry-infilled RC Frame Building Before and After Seismic Retrofit (저층 조적채움벽 철근콘크리트 골조의 내진보강 전후 동특성 변화)

  • Yu, Eunjong;Kim, Min-Jae;Kim, Seung-Nam;Kim, Ji-Young;Choi, Ki-Sun
    • Journal of the Computational Structural Engineering Institute of Korea
    • /
    • v.28 no.3
    • /
    • pp.293-300
    • /
    • 2015
  • In this study, a series of forced vibration testing and ambient vibration measurement were performed at a lowrise masonry-infilled reinforced concrete frame structure before and after seismic retrofit and its dynamic properties were extracted using system identification techniques. Also, analytical models which show similar dynamic properties to the measures ones were constructed. The system identification results showed that damping ratios in x direction along which the dampers were installed has been increased. From the comparison between the analytical models, the effective stiffness of post-installed member and post-reinforced members(shear walls and damper frames) were only 50% of gross sectional stiffness of the members, which indicates that the these members were not fully integrated with the existing structure or members. In addition, support condition of post-installed footing has to be pinned in y direction to match the dynamic properties, which is seemingly caused by the change of fixity of the soil due to the installation of new footing.

Propagation characteristics of ultrasonic guided waves in tram rails

  • Sun, Kui;Chen, Hua-peng;Feng, Qingsong;Lei, Xiaoyan
    • Structural Engineering and Mechanics
    • /
    • v.75 no.4
    • /
    • pp.435-444
    • /
    • 2020
  • Ultrasonic guided wave testing is a very promising non-destructive testing method for rails, which is of great significance for ensuring the safe operation of railways. On the basis of the semi-analytical finite element (SAFE) method, a analytical model of 59R2 grooved rail was proposed, which is commonly used in the ballastless track of modern tram. The dispersion curves of ultrasonic guided waves in free rail and supported rail were obtained. Sensitivity analysis was then undertaken to evaluate the effect of rail elastic modulus on the phase velocity and group velocity dispersion curves of ultrasonic guided waves. The optimal guided wave mode, optimal excitation point and excitation direction suitable for detecting rail integrity were identified by analyzing the frequency, number of modes, and mode shapes. A sinusoidal signal modulated by a Hanning window with a center frequency of 25 kHz was used as the excitation source, and the propagation characteristics of high-frequency ultrasonic guided waves in the rail were obtained. The results show that the rail pad has a relatively little influence on the dispersion curves of ultrasonic guided waves in the high frequency band, and has a relatively large influence on the dispersion curves of ultrasonic guided waves in the low frequency band below 4 kHz. The rail elastic modulus has significant influence on the phase velocity in the high frequency band, while the group velocity is greatly affected by the rail elastic modulus in the low frequency band.

The End-to-end Performance Evaluation Method on Next Generation Network (NGN 환경에 적합한 단대단 성능평가 방법)

  • Nam, Chang-Sup;Kim, Hyung-Soo;Kim, Nam;Jeon, Hong-Beom
    • The Journal of Korean Institute of Communications and Information Sciences
    • /
    • v.31 no.10B
    • /
    • pp.857-865
    • /
    • 2006
  • In order to test and evaluate the various functions and services of NGN would be promised, a specified methodology is needed and a development for the identification of testing object, configuration and test traffic are required. Simulation and analytical modeling methodshave used for IP performance testing, but further study issue still remains. This paper proposes new evaluation methodology to achieve an objective approach rather than a subjective and isolated, based on the real-field environment, for NGN network. For this purpose, background traffic pattern to interfere test traffic was specified and it was tested in actual NGN testbed with systems having NGN technology, such as per bandwidth and packet size. The results shows the suggested methodology is appropriate, comparing with parameters which are Delay, Jitter and Loss the current approach for the end-to-end performance evaluation on NGN.

Analytical and Field Investigation of Bridge Stress Distribution under Proof Load (기지하중을 받는 교량구조물의 현장 계측 및 해석에 따른 응력분포 연구)

  • Eom, Jun-Sik;Lho, Byeong-Cheol
    • Journal of the Korea institute for structural maintenance and inspection
    • /
    • v.7 no.3
    • /
    • pp.139-146
    • /
    • 2003
  • The objective of the presented study is to develop an efficient procedure of proof load testing for existing bridges. By analytical methods, some of these bridges are not adequate to carry normal highway traffic. However, the actual load carrying capacity is often much higher than what can be determined by conventional analysis. Proof load testing can reveal the hidden strength reserve and thus verify the adequacy of the tested bridge. Proof load level required for meaningful tests should be sufficiently higher than legal load. In the state of Michigan, the legal 11-axle truck can weigh up to 685 kN. In this study, a combination of two military tanks and two Michigan 11-axle trucks was used. The proof loads were gradually increased to ensure the safety of the test. After each move, measurements were taken. For the considered bridge, stress levels were rather low compared to pre-test analysis results. This is due to incorrect material strength, structural contribution of nonstructural components such as parapets and railings, and partially fixed supports.

Real-time Hybrid Testing a Building Structure Equipped with Full-scale MR dampers and Application of Semi-active Control Algorithms (대형 MR감쇠기가 설치된 건축구조물의 실시간 하이브리드 실험 및 준능동 알고리즘 적용)

  • Park, Eun-Churn;Lee, Sung-Kyung;Lee, Heon-Jae;Moon, Suk-Jun;Jung, Hyung-Jo;Min, Kyung-Won
    • Journal of the Computational Structural Engineering Institute of Korea
    • /
    • v.21 no.5
    • /
    • pp.465-474
    • /
    • 2008
  • The real-time hybrid testing method(RT-HYTEM) is a structural testing technique in which the numerical integration of the equation of motion for a numerical substructure and the physical testing for an experimental substructure are performed simultaneously in real-time. This study presents the quantitative evaluation of the seismic performance of a building structure installed with an passive and semi-active MR damper by using RT-HYTEM. The building model that was identified from the force-vibration testing results of a real-scaled 5-story building is used as the numerical substructure, and an MR damper corresponding to an experimental substructure is physically tested by using the universal testing machine(UTM). The RT-HYTEM implemented in this study is validated because the real-time hybrid testing results obtained by application of sinusoidal and earthquake excitations and the corresponding analytical results obtained by using the Bouc-Wen model as the control force of the MR damper respect to input currents were in good agreement. Also for preliminary study, some semi-active control algorithms were applied to the MR damper in order to control the structural responses optimally. Comparing between the test results of semi-active control using RT-HYTEM and numerical analysis results show that the RT-HYTEM is more resonable than numerical analysis to evaluate the performance of semi-active control algorithms.

Determination of Excitation and Response Measurement Points for an Efficient Modal Testing (효율적 모우드시험을 위한 가진점과 응답측정점의 결정)

  • 박종필;김광준;박영진
    • Transactions of the Korean Society of Mechanical Engineers
    • /
    • v.16 no.9
    • /
    • pp.1643-1653
    • /
    • 1992
  • A method, which uses analytical or numerical modal analysis results, e.g. from finite element analysis, to select desirable response measurement and excitation points for an efficient modal testing is introduced. First, points of master degree of freedom(DOP) are determined so as to statistically minimize errors between responses of a full order model and those estimated from the reduced order model. Such master DOF's are selected as the response measurement points. Then a criterion named 'driving point model constant(DPMC)' related to the magnitudes of resonance peaks of the driving point freqency response functions used to select the point of excitation out of the master DOF's. In this work, the method is demonstrated through applications to modal testing on a one dimensional cantilever beam and an aluminum plate and the results are compared with those by another technique. also, the method is applied to a two dimensional structural component of a passenger car.

Evaluation of confidence for measurement of VOCs in indoor air (실내공기질 VOCs 측정의 신뢰도 평가를 위한 연구)

  • Kim, Myoung Ock;Kim, Young Lan;Hong, Suk Young;Heo, Gwi Suk;Lim, Hyun Woo;Choe, Seoung Hun;Lee, Won Suk;Han, Jin Seok;Kim, Kum Hee
    • Analytical Science and Technology
    • /
    • v.26 no.3
    • /
    • pp.165-173
    • /
    • 2013
  • To establishment of PT Program for Indoor air quality field that manufacture of confidential development PTMs (proficiency testing materials) and examined of proficiency testing evaluation included sampling process whether or not that is valid. Confirmation of homogeneity and stability of PTMs prepared. PTMs were confirmed to be homogeneous enough to be used as proficiency testing materials since withinbottle homogeneities of the RMs were lower than 0.3 times of targeted standard deviation of proficiency testing. The result of this study showed that the Robust RSD of proficiency testing for VOCs (volatile organic compounds) appeared 23~43% in concentration of 50~320 ${\mu}g/m^3$ for Method A(Distribution by adsorption in Tenax-tube of VOCs), but less 13~42% in concentration of 200~1200 ${\mu}g/m^3$, 16~31% in concentration of 100~450 ${\mu}g/m^3$ for Method B (distribution by VOCs of gas phase in 10L Tedalr bag), C (directly sampling of cylinder with high pressure) respectively. The result of this study showed that method C with sampling is most adequate to the proficiency testing for VOCs in indoor air.