• Korean Journal of Materials Research
• /
• v.11 no.10
• /
• pp.813-819
• /
• 2001

The microstructure and the distribution of hardness of Co and A1 alloy powder cladding layer in high carbon 9CrSi alloy steel for roll materials cladded by laser surface cladding were investigated. And, for the evaluation of soundness as the roll materials, we examined the wear resistance of the cladding materials with the wear appratus of pin on disc type. The experimental results showed that the microstructure of laser cladding layer was constituted with the clad surface layer, the alloy layer, the heat treatment layer with base metal. The wear resistance of Ni alloy Powder cladding material was superior to that of Co alloy powder cladding material both at the low speed (0.46m/s) and the high speed(0.92m/s). It seemed that the behavior of wear showed the abrasive wear at the early stage and the adhesive wear at the late stage.

• International Journal of Precision Engineering and Manufacturing
• /
• v.2 no.4
• /
• pp.69-74
• /
• 2001

Powder forging technology has been introduced to manufacture the parts for vehicles. This paper describes the process conditions for the powder forging of aluminium also piston for vehicles including the determination of composition of aluminum alloy by experiment, preform design by FEM simulation, coed compaction of aluminum alloy powder, sintering of preform, and the experiment of powder forging. The mechanical properties such as hardness, tensile strength, and elongation of the farmed piston were invested and compared with casted piston and forged piston. The tensile strength and hardness of the piston formed by powder forging technology were much more excellent than other pistons.

• Proceedings of the Korean Powder Metallurgy Institute Conference
• /
• 2006.09b
• /
• pp.1264-1265
• /
• 2006

Study about the feasibility and effect of high-energy ball milling on a specific Mg alloy under protection medium of alcohol was presented via comparing with conventional vacuum milling. More fine particles with wider powder size distribution but more irregular shape were shown of the powder milled under alcohol. No obvious oxide was revealed from the two kinds of Mg alloy powders with limited milling time. And since slip induced in a preferential direction, the (002) texture was formed in the Mg alloy powders at the initial stage of alcohol milling. More O and Fe contaminants were introduced into the powders milled under alcohol according to the EDS analysis.

• Advances in materials Research
• /
• v.6 no.4
• /
• pp.343-348
• /
• 2017

High-pressure gas atomization was employed to prepare the Fe-based $Fe_{50}Cr_{24}Mo_{21}Si_2B_3$ alloy powder. The effect of flow rate of atomizing gas on the median powder diameter was studied. The results show that the powder size decreased with increasing the flow rate of atomizing gas. Fe-based alloy coatings with amorphous phase fraction was then prepared by high velocity oxygen fuel spraying (HVOF) of gas atomized $Fe_{50}Cr_{24}Mo_{21}Si_2B_3$ powder. Microstructural studies show that the coatings present dense layered structure and low porosity of 0.17% in about $200{\mu}m$ thickness. The Fe-based alloy coating exhibits an average hardness of about 1230 HV. Our results show that the HVOF process results in dense and well-bonded coatings, making it attractive for protective coatings applications.

• Transactions of the Korean Society of Mechanical Engineers A
• /
• v.24 no.12
• /
• pp.3061-3071
• /
• 2000

Densification behavior of titanium alloy powder was investigated under hot pressing at various pressures and temperatures. Experimental date were obtained for densification of titanium alloy powder under an instantaneous loading and subsequent creep deformation during hot pressing. The constitutive models of Fleck et al. and the modified Gurson were employed for thermo-phastic deformation under the instantaneous loading and that f Abouaf and co-workers for creep deformation of titanium alloy powder during hot pressing. By implementing these constitutive equations into a finite element program(ABAQUS), finite element results were compared with experimental data during hot pressing. To investigate the effect of friction between the power and die wall, density distributions of power compacts were measured and compared with finite element calculations. Finite element results from the models of Fleck et al. and the modified Gurson agreed reasonably good with experimental data for densification and density distribution of titanium alloy powder under the instantaneous loading during hot pressing. Finite element results from the model of Abouaf and co-workers, however, somewhat overestimate experimental data for creep deformation of power compacts during hot pressing.

• Journal of Powder Materials
• /
• v.10 no.5
• /
• pp.333-336
• /
• 2003

The purpose of this study is the fabrication of nano-sized Fe-Co alloy powders with soft magnetic properties by the slurry mixing and hydrogen reduction (SMHR) process. $FeCl_2$0 and $CoCl_2$ powders with 99.9% purities were used for synthesizing nanostructured Fe-Co alloy powder. Nano-sized Fe-Co alloy powders were successfully fabricated using SMHR, which was performed at 50$0^{\circ}C$ for 1 h in H$_2$ atmosphere. The fabricated Fe-Co alloy powders showed $\alpha$' phase (ordered body centered cubic) with the average particle size of 45 nm. The SMHR powder exhibited low coercivity force of 32.5 Oe and saturation magnetization of 214 emu/g.

• Journal of Powder Materials
• /
• v.8 no.3
• /
• pp.157-162
• /
• 2001

An optimum route to fabricate the ferrous alloy dispersed $Al_2O_3$ nanocomposites such as $Al_2O_3$/Fe-Ni and $Al_2O_3$/Fe-Co with sound microstructure and desired properties was investigated. The composites were fabricated by the sintering of powder mixtures of $Al_2O_3$ and nano-sized ferrous alloy, in which the alloy was prepared by solution-chemistry routes using metal nitrates powders and a subsequent hydorgen reduction process. Microstructural observation of reduced powder mixture revealed that the Fe-Ni or Fe-Co alloy particles of about 20 nm in size homogeneously surrounded $Al_2O_3$, forming nanocomposite powder. The sintered $Al_2O_3$/Fe-Ni composite showed the formation of Fe$Al_2O_4$ phase, while the reaction phases were not observed in $Al_2O_3$/Fe-Co composite. Hot-pressed $Al_2O_3$/Fe-Ni composite showed improved mechanical properties and magnetic response. The properties are discussed in terms of microstructural characteristics such as the distribution and size of alloy particles.

• Applied Chemistry for Engineering
• /
• v.34 no.4
• /
• pp.450-454
• /
• 2023

Chloride ions in the alloy powder used as flux in Flux Cored Arc Welding (FCAW) can cause pores on the bead surface of the welding metal to cause defects, or chloride remaining in the alloy powder can cause corrosion of the metal. Combustion-ion chromatography is mainly used to quantify the chloride ions in alloy powder, but there is a limitation in that the equipment is expensive and requires a high degree of expertise. Therefore, this study aims to find an easy and accurate quantification method in the field by comparing combustion-ion chromatography (C-IC), which is mainly used for chloride ion quantification of alloy powder, X-ray fluorescence analysis (XRF), and potentiometric titration. In this article, magnesium-aluminum alloy powder is applied to the quantification of chloride ions because it is most commonly used as flux. This study confirmed that potentiometric titration can be applied to the quantification of chloride ions in the alloy powder in the industry field.

• Journal of Powder Materials
• /
• v.30 no.4
• /
• pp.339-345
• /
• 2023

This study investigates the melting point and brazing properties of the aluminum (Al)-copper (Cu)-silicon (Si)-tin (Sn) alloy fabricated for low-temperature brazing based on the alloy design. Specifically, the Al-20Cu-10Si-Sn alloy is examined and confirmed to possess a melting point of approximately 520℃. Analysis of the melting point of the alloy based on composition reveals that the melting temperature tends to decrease with increasing Cu and Si content, along with a corresponding decrease as the Sn content rises. This study verifies that the Al-20Cu-10Si-5Sn alloy exhibits high liquidity and favorable mechanical properties for brazing through the joint gap filling test and Vickers hardness measurements. Additionally, a powder fabricated using the Al-20Cu-10Si-5Sn alloy demonstrates a melting point of around 515℃ following melting point analysis. Consequently, it is deemed highly suitable for use as a low-temperature Al brazing material.

• Journal of Powder Materials
• /
• v.29 no.2
• /
• pp.123-131
• /
• 2022

The purpose of this study is to improve the mechanical properties and develop manufacturing technology through self-soluble alloy powder flame spray coating on the surface of a run-out table roller for hot rolling. The roller surface of the run-out table should maintain high hardness at high temperatures and possess high wear, corrosion, and heat resistances. In addition, sufficient bonding strength between the thermal spray coating layer and base material, which would prevent the peel-off of the coating layer, is also an important factor. In this study, the most suitable powder and process for roll manufacturing technology are determined through the initial selection of commercial alloy powder for roll manufacturing, hardness, component analysis, and bond strength analysis of the powder and thermal spray coating layer according to the powder.