• 대한치과보철학회지
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• 제42권6호
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• pp.654-663
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• 2004

Statement of problem. According to the fracture pattern in several reports, fractures most frequently occur in the interface between the ceromer and the substructure. Purpose. The aim of this in vitro study was to compare the macro shear bond strength and microshear bond strength of a ceromer bonded to a fiber reinforced composite (FRC) as well as metal alloys. Material and methods. Ten of the following substructures, type II gold alloy, Co-Cr alloy, Ni-Cr alloy, and FRC (Vectris) substructures with a 12 mm in diameter, were imbedded in acrylic resin and ground with 400, and 1, 000-grit sandpaper. The metal primer and wetting agent were applied to the sandblasted bonding area of the metal specimens and the FRC specimens, respectively. The ceromer was placed onto a 6 mm diameter and 3 mm height mold in the macro-shear test and 1 mm diameter and 2 mm height mold in the micro-shear test, and then polymerized. The macro- and micro-shear bond strength were measured using a universal testing machine and a micro-shear tester, respectively. The macro- and micro-shear strength were analyzed with ANOVA and a post-hoc Scheffe adjustment ($\alpha$ = .05). The fracture surfaces of the crowns were then examined by scanning electron microscopy to determine the mode of failure. Chi-square test was used to identify the differences in the failure mode. Results. The macro-shear strength and the micro-shear strength differed significantly with the types of substructure (P<.001). Although the ceromer/FRC group showed the highest macroand micro-shear strength, the micro-shear strength was not significantly different from that of the base metal alloy groups. The base metal alloy substructure groups showed the lowest mean macro-shear strength. However, the gold alloy substructure group exhibited the least micro-shear strength. The micro-shear strength was higher than the macro-shear strength excluding the gold alloy substructure group. Adhesive failure was most frequent type of fracture in the ceromer specimens bonded to the gold alloys. Cohesive failure at the ceromer layer was more common in the base metals and FRC substructures. Conclusion. The Vectris substructure had higher shear strength than the other substructures. Although the shear strength of the ceromer bonded to the base metals was lower than that of the gold alloy, the micro-shear strength of the base metals were superior to that of the gold alloy.

• 한국표면공학회지
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• 제42권4호
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• pp.161-168
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• 2009

Effects of TiN/Ti multilayer coating on the Ti-30Ta-xZr alloy surface were studied by using various experiments. The Ti-30Ta containing Zr (5, 10 and 15 wt%) were melted 10 times to improve chemical homogeneity by using a vacuum furnace. And then samples were homogenized for 24 hrs at $1000^{\circ}C$. The specimens were prepared for TiN/Ti coating by cutting and polishing. The prepared specimens were coated with TiN/Ti multilayers by using DC magnetron sputtering method. The analyses of coated surface and coated layer were carried out by field emission scanning electron microscope(FE-SEM), EDX, and X-ray diffractometer(XRD). From the microstructure and XRD analysis of Ti-30Ta-xZr alloys, The equiaxed structure was changed to needle-like structure with increasing Zr content. And $\alpha$-peak and elastic modulus increased as Zr content increased. The $\alpha$ and $\beta$ phase predominantly were found in the specimen containing high Zr content. According to the analysis of TiN/Ti coating layer, the surface defects and structures of Ti-30Ta-xZr were covered with TiN/Ti coating layer and surface roughness decreased.

• 조명전기설비학회논문지
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• 제20권6호
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• pp.69-74
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• 2006

[ $Mg_2Ni$ ] 합금 및 $Mg_2Ni$와 카본 혼합물 입자의 수소저장 특성에 대한 기계적 분쇄(MG, Mechanical Grinding) 처리 효과를 고온 가스상의 PCT 측정 및 전기화학적인 마이크로 전극 측정법 등에 의해 검토되었다. PCT 측정은 약 $300[^{\circ}C]$의 고온에서 실시되었으며 전기화학적인 실험은 카본-섬유로 구성된 마이크로 전극을 1M KOH 수용액 속에서 조정자를 사용하여 MG 처리한 합금 단일입자에 접촉시켰다. 그 결과 $Mg_2Ni$ 합금과 카본 혼합물 입자의 경우 가스상에서 수소 해리압이 감소하고 상온에서 전기화학적인 수소화 특성이 크게 개선되었다. 이것은 기계적 분쇄(MG) 작용에 의한 합금의 미세화 및 나노화에 기인한다고 판단된다. 즉 고온 가스상의 PCT 측정 결과 수소 해리압이 MG 처리에 의해 0.55[MPa]에서 0.42[MPa]로 감소하였으며 동일 샘플 입자에 대해 마이크로 전극에 의한 평가에서도 수소화 피크가 보다 분명하게 관찰되었다.

• 한국주조공학회지
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• 제42권3호
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• pp.153-160
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• 2022

초내열합금 625 튜브의 제조에 필요한 원심주조품의 두께에 따라 응고조직과 기계적 특성에 미치는 영향을 고찰하였다. 10, 17, 50 mm 두께로 원심주조한 625합금에서 두께의 증가에 따라 주상정 부분의 길이와 2차 수지상 간격이 약간 증가하였으나 상온 인장특성은 큰 차이를 보이지 않았다. 주상정 부분의 응고는 일방향응고의 형태로 응고가 진행되기 때문에 일방향응고 조건을 변화시켜 2차 수지상의 간격을 비교하여 각 두께의 주조품에서 응고속도를 계산하였다. 두꺼운 주조품일수록 내부 다결정 조직의 비율이 증가하였다. 다결정 부분의 인장특성은 주상정 부분의 평균값과 유사한 값을 보였으며 이는 2차 수지상의 간격보다 결정립 형태의 영향인 것으로 사료된다.

• Steel and Composite Structures
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• 제42권6호
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• pp.827-841
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• 2022

The rotation capacities of the plastic hinges located at beam-ends are significantly reduced in traditional steel framed-tube structures (SFTSs) because of the small span-to-depth ratios of the deep beams, leading to the low ductility and energy dissipation capacities of the SFTSs. High-strength steel framed-tube structures with replaceable shear links (HSSFTS-RSLs) are proposed to address this issue. A replaceable shear link is located at the mid-span of a deep spandrel beam to act as a ductile fuse to dissipate the seismic energy in HSSFTS-RSLs. A 2/3-scaled HSSFTS-RSL specimen with a shear link fabricated of high-strength low-alloy Q355 structural steel was created, and a cyclic loading test was performed to study the hysteresis behaviors of this specimen. The test results were compared to the specimens with soft steel shear links in previous studies to investigate the feasibility of using high-strength low-alloy steel for shear links in HSSFTS-RSLs. The effects of link web stiffener spaces on the cyclic performance of the HSSFTS-RSLs with Q355 steel shear links were investigated based on the nonlinear numerical analysis. The test results indicate that the specimen with a Q355 steel shear link exhibited a reliable and stable seismic performance. If the maximum interstory drift of HSSFTS-RSL is designed lower than 2% under earthquakes, the HSSFTS-RSLs with Q355 steel shear links can have similar seismic performance to the structures with soft steel shear links, even though these shear links have similar shear and flexural strength. For the Q355 steel shear links with web height-to-thickness ratios higher than 30.7 in HSSFTS-RSLs, it is suggested that the maximum intermediate web stiffener space is decreased by 15% from the allowable space for the shear link in AISC341-16 due to the analytical results.

• 대한방사선치료학회지
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• 제31권1호
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• pp.57-65
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• 2019

목 적: 전자선 치료에서 저 용융점 납합금과 순수 납을 이용한 차폐 시 두께증가에 따른 블록 가장자리의 산란선 영향을 알아보고자 한다. 대상 및 방법: $10{\times}10cm^2$ 어플리케이터의 Insert Frame 절반을 차폐하도록 블록을 제작하였고, 두께는 각 재질당 3, 5, 10, 15, 20 (mm)로 하였다. 공통 조건을 에너지 6 MeV, 선량률 300 MU/Min, 갠트리 각도 0, 부여선량 100 MU으로 설정하였고, 블록의 위치와 측정점의 위치, 블록재질을 각각 달리하여 블록 두께증가에 따른 상대적인 산란비율을 평행평판형 전리함과 고체팬텀으로 측정하였다. 결 과: (측정 깊이 / 블록 위치 / 블록 재질)이 (표면 / 어플리케이터 / 순수 납)일 때 블록 두께가 3, 5, 10, 15, 20 (mm) 순으로 증가함에 따라 상대선량은 15.33 nC, 15.28 nC, 15.08 nC, 15.05 nC, 15.07 nC로 측정되었다. (표면 / 어플리케이터 / 합금 납)일 때 15.19 nC, 15.25 nC, 15.15 nC, 14.96 nC, 15.15 nC로 측정되었다. (표면 / 팬텀 위 / 순수 납)일 때 15.62 nC, 15.59 nC, 15.53 nC, 15.48 nC, 15.34 nC로 측정되었다. (표면 / 팬텀 위 / 합금 납)일 때 15.56 nC, 15.55 nC, 15.51 nC, 15.42 nC, 15.39 nC로 측정되었다. (심부 / 어플리케이터 / 순수 납)일 때 16.70 nC, 16.84 nC, 16.72 nC, 16.88 nC, 16.90 nC로 측정되었다. (심부 / 어플리케이터 / 합금 납)일 때 16.83 nC, 17.12 nC, 16.89 nC, 16.77 nC, 16.52 nC로 측정되었다. (심부 / 팬텀 위 / 순수 납)일 때 17.41 nC, 17.45 nC, 17.34 nC, 17.42 nC, 17.25 nC로 측정되었다. (심부 / 팬텀 위 / 합금 납)일 때 17.45 nC, 17.44 nC, 17.47 nC, 17.43 nC, 17.35 nC로 측정되었다. 결 론: 차폐블록을 이용하여 전자선 치료를 진행할 때 블록위치는 환자 체표면보다는 어플리케이터에 삽입하고 두께는 각 사용 에너지에 해당되는 최소 적정차폐두께로 제작해야 한다. 또한 블록 가장자리 경계선으로부터 떨어진 거리에 따라 변화하는 산란선의 영향을 충분히 고려하여 치료를 시행하는 것이 바람직하다고 사료된다.

• 대한기계학회논문집A
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• 제23권11호
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• pp.1904-1911
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• 1999

The most effective material in the shape memory alloy(SMA) is the TiNi alloy, because its shape recovery characteristics are very excellent. We molded the composite material with shape memory function. The fiber of it is $Ti_{50}-Ni_{50}$ shape memory alloy and matrix of it is epoxy resin(Araldite B41, Hardner HT903. Ciba Geigy), its adhesive and optical sensitivity are very excellent. It was assured that the composite material could be used as model material of photoelastic experiment for intelligent materials or structures. In this research, the composite material with shape memory function is used as model material of photoelastic experiment. Photoelastic experimental hybrid method is developed in this research, it is assured that it is useful on the obtaining stress intensity factor and the separation of stress components from only isochromatic data. The measuring method of stress intensity factor of intelligent material by photoelastic experiment is introduced. In the mode I state, we can know that stress intensity factors are decreased more than 50% of stress intensity factor of room temperature when temperature of fiber is greater than 4$0^{\circ}C$, prestrain greater than 5% and fiber volume ratio greater than 0.42% and that stress intensity factors are decreased by 100% when fiber volume ratio is greater than 0.84%, prestrain greater than 5% and temperature greater than 60 $^{\circ}C$.

• 한국재료학회지
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• 제32권9호
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• pp.391-395
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• 2022

Research is being actively conducted on the continuous thin plate casting method, which is used to manufacture magnesium alloy plate for plastic processing. This study applied a heat transfer solidification analysis method to the melt drag process. The heat transfer coefficient between the molten magnesium alloy metal and the roll in the thin plate manufacturing process using the melt drag method has not been clearly established until now, and the results were used to determine the temperature change. The estimated heat transfer coefficient for a roll speed of 30 m/min was 1.33 × 10⁵ W/m²·K, which was very large compared to the heat transfer coefficient used in the solidification analysis of general aluminum castings. The heat transfer coefficient between the molten metal and the roll estimated in the range of the roll speed of 5 to 90 m/min was 1.42 × 10⁵ to 8.95 × 10⁴ W/m²·K. The cooling rate was calculated using a method based on the results of deriving the temperature change of the molten metal and the roll, using the estimated heat transfer coefficient. The DAS was estimated from the relationship between the cooling rate and DAS, and compared with the experimental value. When the magnesium alloy is manufactured by the melt drag method, the cooling rate of the thin plate is in the range of about 1.4 × 10³ to 1.0 × 10⁴ K/s.

• Composites Research
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• 제20권3호
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• pp.37-42
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• 2007

금속복합재료에서는 강화재와 기지재 사이의 열팽창계수 차이에 의해 복합재료 내부에 잔류응력이 남아있어 복합재료 전체의 강도저하를 가져온다. 본 연구에서는 TiNi 형상기억합금을 강화재료로써 이러한 잔류응력 문제를 해결하기 위하여 이용하였다. TiNi 형상기억합금은 형상기억효과를 이용하여 복합재료의 잔류응력문제를 해결할 뿐만 아니라 복합재료의 인장강도를 증가시키는 역할을 한다. 핫프레스 방법에 의해 제작된 형상기억복합재료의 강도증가를 위하여 냉간압연을 실시하여 실험을 실시하였다. 이와 같이 제작된 형상기억복합재료의 저온에서의 미시적 손상거동을 평가하기 위하여 음향방출기법을 이용하였다. 또한 열충격을 받은 시험편의 손상에 대한 연구도 이루어졌다.

• 한국안전학회지
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• 제24권1호
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• pp.26-30
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• 2009

Shape memory recoverable stress and strain of Ti-42.5at%Ni-10at%Cu alloys were measured by means of constant temperature tensile tests. The alloys' transformation behavior is B2 - B19 by DSC result. The strain by tensile stress were perfectly recovered by heating at any testing conditions but shape memory recoverable stress increased to 66MPa and then slightly decreased. Transformation temperatures from thermal cycling under constant uniaxial applied tensile loads linearly increased by increasing tensile load and their thermal hysteresis are about 110K and their maximum recoverable strain is 6.5% at 100MPa condition.