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Effects of Film Formation Conditions on the Chemical Composition and the Semiconducting Properties of the Passive Film on Alloy 690

  • Jang, HeeJin;Kwon, HyukSang
    • Corrosion Science and Technology
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    • v.5 no.4
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    • pp.141-148
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    • 2006
  • The chemical composition and the semiconducting properties of the passive films formed on Alloy 690 in various film formation conditions were investigated by XPS, photocurrent measurement, and Mott-Schottky analysis. The XPS and photocurrent spectra showed that the passive films formed on Alloy 690 in pH 8.5 buffer solution at ambient temperature, in air at $400^{\circ}C$, and in PWR condition comprise $Cr_2O_3$, $Cr(OH)_3$, ${\gamma}-Fe_2O_3$, NiO, and $Ni(OH)_2$. The thermally grown oxide in air and the passive film formed at high potential (0.3 $V_{SCE}$) in pH 8.5 buffer solution were highly Cr-enriched, whereas the films formed in PWR condition and that formed at low potential (-0.3 $V_{SCE}$) in pH 8.5 buffer solution showed relatively high Ni content and low Cr content. The Mott-Schottky plots exhibited n-type semiconductivity, inferring that the semiconducting properties of the passive films formed on Alloy 690 in various film formation conditions are dominated by Cr-substituted ${\gamma}-Fe_2O_3$. The donor density, i.e., concentration of oxygen vacancy, was measured to be $1.2{\times}10^{21}{\sim}4.6{\times}10^{21}cm^{-3}$ and lowered with increase in the Cr content in the passive film.

PWHT Cracking Susceptibility in the Weld Heat-Affected Zone of Reduced Activation Ferritic/Martensitic Steels (핵융합로 구조용 저방사화강의 용접열영향부 후열처리 균열 감수성)

  • Lee, Jinjong;Moon, Joonoh;Lee, Chang-Hoon;Park, Jun-Young;LEE, Tae-Ho;Hong, Hyun-Uk;Cho, Kyung-Mox
    • Journal of Welding and Joining
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    • v.34 no.6
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    • pp.47-54
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    • 2016
  • Post-Weld Heat Treatment (PWHT) cracking susceptibility in the weld heat-affected zone (HAZ) of reduced activation ferritic-martensitic (RAFM) steels was evaluated through stress-rupture tests. 9Cr-1W based alloys including different C, Ta and Ti content were prepared. The coarse grained heat-affected zone (CGHAZ) samples were simulated with welding condition of 30 kJ/cm heat input. CGHAZ samples consisted of martensite matrix. Stress rupture experiments were carried out using a Gleeble simulator at temperatures of $650-750^{\circ}C$ and at stress levels of 125-550 MPa, corresponding to PWHT condition. The results revealed that PWHT cracking resistance was improved by Ti addition, i.e., Ti contributed to the formation of fine and stable MX precipitates and suppression of coarse M23C6 carbides, resulting in improvement of stress rupture ductility. Meanwhile, rupture strength increased with increasing solute C content.

Stabilization of Rice Bran by Microwave Energy (마이크로파 에너지에 의한 쌀겨의 안정화)

  • Rhee, Joon-S.;Yoon, Heeny H.N.
    • Korean Journal of Food Science and Technology
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    • v.16 no.1
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    • pp.113-119
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    • 1984
  • Initial moisture content and weight of the rice bran and treatment time were identified as important variables for the inactivation of lipase and peroxidase present in rice bran. Multiple regression analysis was used to obtain a prediction equation to measure the effects of moisture content and weight of the sample and microwave treatment time on the residual lipase activity and loss in weight. It was found that the microwave treatment did not affect acid value and extractability of the rice bran oil.

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Corrosion Fatigue Cracking of Low Alloy Steel in High Temperature Water

  • Lee, S.G.;Kim, I.S.;Jang, C.H.;Jeong, I.S.
    • Corrosion Science and Technology
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    • v.2 no.2
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    • pp.93-97
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    • 2003
  • Fatigue crack growth test or low alloy steel was performed in high temperature water. Test parameters were dissolved oxygen content. loading frequency and R-ratio ($P_{min}/P_{max}$). Since the sulfur content or the steel was low, there were no environmentally assisted cracks (EAC) in low dissolved oxygen(DO) water. At high DO, the crack growth rate at R = 0.5 tests was much increased due to environmental effects and the crack growth rate depended on loading frequency and maximized at a critical frequency. On the other hand, R = 0.7 test results showed an anomalous decrease of the crack growth rate as much different behavior from the R = 0.5. The main reason of the decrease may be related to the crack tip closure effect. All the data could be qualitatively understood by effects of oxide rupture and anion activity at crack tip.

COSMIC : Design and Implementation of a Content-Based Multimedia Retrieval System using Domain Knowledge and Visual Information (COSMIC : 영역지식과 시각정보를 이용한 내용기반 멀티미디어 검색 시스템의 설계 및 구현)

  • Kim, Deok-Hwan;Kim, Si-U;Park, Gwang-Sun;Lee, Byeong-Gu;Cha, Gwang-Ho;Jeong, Jin-Wan
    • Journal of KIISE:Computing Practices and Letters
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    • v.5 no.1
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    • pp.14-28
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    • 1999
  • 최근 멀티미디어 데이터로부터 내용에 대한 정보를 추출하여 데이터베이스에 저장하고 내용에 기반한 질의를 수행하도록 하는 내용 기반 검색 시스템이 중요한 핵심 기술로 대두되고 있다. 본 논문에서는 내용 기반 멀티미디어 검색 시스템인 COSMIC(Content Based Multimedia Information Processor)의 설계 및 구현에 관하여 기술한다. COSMIC은 대용량 이미지 데이터로부터 자동으로 추출된 시각적 특징 데이터들을 다차원 점접근 방법(Point Access Method)인 HG-트리를 이용하여 색인하고 예제 이미지와 사용자가 그린 스케치에 의한 시각적 질의를 제공한다. 또한 COSMIC은 비디오 데이터로부터 추출된 다양한 의미 정보를 이용하여 의미 질의를 제공한다. COSMIC의 유효성을 입증하기 위해서 다양한 시각적 질의와 이미 질의를 이용한 실험을 수행하였다.

Study for the Development of Fe-NbC Composites by Advanced PM Techniques

  • Gordo, E.;Gomez, B.;Gonzalez, R.;Ruiz-Navas, E.M.
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2006.09a
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    • pp.118-119
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    • 2006
  • The development of Fe-based metal matrix composites (MMCs) with high content of hard phase has been approached by combining the use of advanced powder metallurgy techniques like high-energy milling (HEM), cold isostatic pressing (CIP) and vacuum sinterings. A 30% vol. of NbC particles was mixed with Fe powder by HEM in a planetary mill during 10h, characteristing the powder by the observation of morphology and microstructure by scanning electron microscopy (SEM). After of sintering process the variation of density, hardness,carbon content and the microstructural changes observed, permits to find the optimal conditions of processing. Afterwards, a heat treatment study was performed to study the hardenability of the composite.

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Comparisons of Pericarp Thickness And Sugar Content on New Waxy Corn Hybrids

  • Lee, Moon-Sub;Na, Wong-Hyeun;Ha, Ji-hyung;Yang, Jae-Hyeon;Lee, Hee-Bong
    • KOREAN JOURNAL OF CROP SCIENCE
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    • v.60 no.2
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    • pp.180-184
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    • 2015
  • For waxy corn hybrid development, 23 waxy corn hybrids were planted and surveyed in both pericarp thickness and sugar content. Pericarp thickness showed average 50 to $49{\mu}m$ in field and greenhouse. Results like these advanced than previous other hybrids. Also, sugar content in developed waxy corn evaluated as 13.6 to 15.3 brix. Here, we concluded that edible quality of waxy corn depended on combing of two factors. Especially, CNU11H8 hybrid at field and CNU11H-38 at greenhouse were good in both factors. Accordingly, these hybrids will be planted in next time for productivity and area adaptation.

Corrosion behavior of Mg-(0~6)%Zn Casting Alloys in 1M NaCl Solution (1M NaCl 용액에서 Mg-(0~6)%Zn 주조 합금의 부식 거동)

  • Hwang, In-Je;Kim, Young-Jig;Jun, Joong-Hwan
    • Journal of Korea Foundry Society
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    • v.36 no.4
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    • pp.117-125
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    • 2016
  • The effects of the Zn content on the microstructure and corrosion behavior in 1M NaCl solution were investigated in Mg-(0~6)%Zn casting alloys. The MgZn phase was scarcely observed in the Mg-1%Zn alloy, while the Mg-(2~6)%Zn alloy consisted of ${\alpha}$-(Mg) and MgZn phases. With an increase in the Zn content, the amount of the MgZn phase was gradually increased. Immersion and electrochemical corrosion tests indicated that the Mg-1%Zn alloy had the lowest corrosion rate among the alloys, and a further increase in the Zn content resulted in the deterioration of the corrosion resistance. Microstructural examinations of the corroded surfaces and EIS analyses of surface corrosion films revealed that the best corrosion resistance at 1%Zn was associated with the absence of MgZn phase particles in the microstructure and the contribution of Zn element to the formation of a protective film on the surface. A micro-galvanic effect by the MgZn particles led to the increased rate of corrosion at a higher Zn content.

Content Validity of a Korean-Translated Version of a Fullerton Advanced Balance Scale: A Pilot Study

  • Kim, Gyoung-mo
    • Physical Therapy Korea
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    • v.22 no.4
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    • pp.51-61
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    • 2015
  • The purpose of this study were to translate the Fullerton Advanced Balance (FAB) scale into Korean and to verify the content validity by utilizing a back-translation method with a view to assessing balance function and the risk of falling in a clinical research setting. This research was conducted in six steps. First, three Korean physical therapists translated the FAB scale into Korean. Second, two bilingual professors of physical therapy and a physical therapist evaluated translation conformity of Korean-translated FAB scale. In the third and fourth steps, twelve physical therapists evaluated the degree of translation comprehension, and a translator back-translated the Korean FAB scale into the original language. Fifth, a bilingual professor of physical therapy and two native speakers evaluated the technical and conceptual equivalence between the original and translation versions. In this process, inappropriate translated items were revised using recommended substitute words or sentences, and all items were evaluated on the basis of three points or more on a rating scale in terms of translation comprehension, and the technical and conceptual equivalence of the back-translation. In the sixth and last step, the translation verification committee completed the final Korean version. The above process indicated that the content validity of the Korean-translated FAB scale was established by means of systematic translation methods, and it can therefore be used to assess balance function and the risk of falls in a clinical research setting.