• Title/Summary/Keyword: advanced analysis methods

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Synthesis and spectroscopic characterization of zinc ferrite nanoparticles

  • Arora, Shefali;Nandy, Subhajit;Latwal, Mamta;Pandey, Ganesh;Singh, Jitendra P.;Chae, Keun H.
    • Advances in nano research
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    • v.13 no.5
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    • pp.437-451
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    • 2022
  • Synthesis approaches usually affect the physical and chemical properties of ferrites. This helps ferrite materials to design them for desired applications. Some of these methods are mechanical milling, ultrasonic method, micro-emulsion, co-precipitation, thermal decomposition, hydrothermal, microwave-assisted, sol-gel, etc. These methods are extensively reviewed by taking example of ZnFe2O4. These methods also affect the microstructure and local structure of ferrite which ultimately affect the physical and chemical properties of ferrites. Various spectroscopic techniques such as Raman spectroscopy, Fourier Transform Infrared spectroscopy, Ultra Violet-Visible spectroscopy, Mossbauer spectroscopy, extended x-ray absorption fine structure, and electron paramagnetic resonance are found helpful to reveal this information. Hence, the basic principle and the usefulness of these techniques to find out appropriate information in ZnFe2O4 nanoparticles is elaborated in this review.

Advanced Flow Visualization Technologies and Blue Ocean Strategy (첨단 유동가시화 기법들과 Blue Ocean 전략)

  • Lee, Sang-Joon
    • 유체기계공업학회:학술대회논문집
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    • 2006.08a
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    • pp.145-146
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    • 2006
  • Recently, the next-generation advanced flow visualization techniques such as holographic PIV, dynamic PIV, echo-PIV, micro/nano-PIV, and X-ray PIV have been introduced. These advanced measurement techniques have a big potential as the core technology for analyzing outmost thermo-fluid flows in future. These would be indispensable in solving complicated thermo-fluid flow problems not only in the industrial fields such as automotive, space, electronics, aero- and hydro-dynamics, steel, and information engineering, but also in the research fields of medical science, bio-medical engineering, environmental and energy engineering etc. Especially, NT (Nano Technology) and BT (Bio Technology) strongly demand these advanced measurement techniques, because it is impossible for conventional measurement methods to observe most complicated nano- and bio-fluidic phenomena. In this presentation, the basic principle of these high-tech flow visualization techniques and their practical applications which cannot be resolved by conventional methods, such as blood flows in a micro-tube, in vivo analysis of micro-circulation, and flow around a living body will be introduced as a blue ocean strategy.

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Advanced Flow Visualization Technologies and Blue Ocean Strategy (첨단 유동가시화 기법들과 Blue Ocean 전략)

  • Lee, Sang-Joon
    • Journal of the Korean Society of Visualization
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    • v.4 no.2
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    • pp.3-5
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    • 2006
  • Recently, the next-generation advanced flow visualization techniques such as holographic PIV, aynni.c PIV, echo-PIV, micro/nano-PIV, and X-ray PIV have been introduced. These advanced mea-surement techniques have a big potential as the core technology for analyzing outmost thermo-fluid flows in future. They would be indispensable in solving complicated thermo-fluid flow problems not only in industrial fields such as automotive, space, electronics, aero- and hydro-dynamics. steel, and information engineering, but also in the research fields of medical science, bio-medical engineering, environmental and energy technology etc. Especially, NT (Nano Technology) and BT (Bio Technology) strongly demand these advanced measurement techniques, because it is impossible for conventional measurement methods to observe the nano- and bio-fluidic flow phenomena. In this article, the basic principle of these high-tech flow visualization techniques and their practical applications which cannot be resolved by conventional methods, such as blood flows in a micro-tube, in vivo analysis of micro-circulation, and flow around a living body are introduced as a blue ocean strategy.

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Advanced Flow Visualization Techniques for Diagnosing Microscale Biofluid Flows (미세 생체유동 해석을 위한 첨단 유동가시화기법)

  • Lee, Sang-Joon
    • Transactions of the Korean Society of Mechanical Engineers B
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    • v.33 no.1
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    • pp.1-8
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    • 2009
  • Recently microscale biofluid flows have been receiving large attention in various research areas. However, most conventional imaging techniques are unsatisfactory due to difficulties encountered in the visualization of microscale biological flows. Recent advances in optics and digital image processing techniques have made it possible to develop several advanced micro-PIV/PTV techniques. They can be used to get quantitative velocity field information of various biofluid flows from visualized images of tracer particles. In this paper, as new advanced micro-PIV techniques suitable for biofluid flow analysis, the basic principle and typical applications of the time-resolved micro-PIV and X-ray micro-PIV methods are explained. As a 3D velocity field measurement technique for measuring microscale flows, holographic micro-PTV method is introduced. These advanced PIV/PTV techniques can be used to reveal the basic physics of various microscale biological flows and will play an important role in visualizing veiled biofluid flow phenomena, for which conventional methods have many difficulties to analyze.

A Study on the Application of Analytic Nodal Method to a CANDU-600 Reactor Analysis

  • C.S. Yeom;Ryu, H.;Kim, H.J.;Kim, Y.H.;Kim, Y.B.
    • Proceedings of the Korea Society for Energy Engineering kosee Conference
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    • 2000.11a
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    • pp.115-120
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    • 2000
  • The analysis of flux distribution under stead-state in large power reactors with assymetry reactivity insertions requires the use of three-dimensional diffusion calculations. For the purpose, consistently formulated modern nodal methods based on higher order interface techniques have become popular tools for flux distributions in large commercial nuclear reactors. Among the earlier developments, the nodal Green's function method obtains its nodal interface equation from the transverse-integrated integral diffusion equation using a finite-medium Green's function. In this method, the outgoing current from a node surface is formulated as a response of the incoming currents and the spatially integrated neutron source within the same node. The well-known nodal expansion method is also based on an interface partial current formulation. Nodal methods high-level interface variables, i.e., interface net current and flux, may be more computationally efficient than the nodal Green's function method because they have one fewer unknown per interface. The Analytic Nodal Method(ANM), which can be classified as an interface net current technique and, was faster in solving some standard benchmark problems than the other two methods.(omitted)

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Alternative Sample Preparation Method for Large-Area Cross-Section View Observation of Lithium Ion Battery

  • Kim, Ji-Young;Jeong, Young Woo;Cho, Hye Young;Chang, Hye Jung
    • Applied Microscopy
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    • v.47 no.2
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    • pp.77-83
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    • 2017
  • Drastic development of ubiquitous devices requires more advanced batteries with high specific capacitance and high rate capability. Large-area microstructure characterization across the stacks of cathode, electrolyte and anode might reveal the origin of the instability or degradation of batteries upon cycling charge. In this study, sample preparation methods to observe the cross-section view of the electrodes for battery in SEM and several imaging tips are reviewed. For an accurate evaluation of the microstructure, ion milling which flats the surface uniformly is recommended. Pros and cons of cross-section polishing (CP) with Ar ion and focused ion beam (FIB) with Ga ion were compared. Additionally, a modified but new cross-section milling technique utilizing precision ion polishing system (PIPS) which can be an alternative method of CP is developed. This simple approach will make the researchers have more chances to prepare decent large-area cross-section electrode for batteries.

An Efficient Approach on Reliability Analysis under Multidisciplinary Analysis Systems (다분야 통합해석 시스템의 효율적인 신뢰성 해석기법 연구)

  • Ahn, Joong-Ki;Kwon, Jang-Hyuk
    • Journal of the Korean Society for Aeronautical & Space Sciences
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    • v.33 no.3
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    • pp.18-25
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    • 2005
  • Existing methods have performed the reliability analysis using nonlinear optimization techniques. This is mainly due to the fact that they directly apply Multidisciplinary Design Optimization(MDO) frameworks to the reliability analysis formulation. Accordingly, the reliability analysis and the Multidisciplinary Analysis(MDA) are tightly coupled in a single optimizer, which hampers utilizing the recursive and function-approximation based reliability analysis methods such as the Advanced First Order Reliability Method(AFORM). In order to utilize the efficient reliability analysis method under multidisciplinary analysis systems, we propose a new strategy named Sequential Approach on Reliability Analysis under Multidisciplinary analysis systems(SARAM). In this approach, the reliability analysis and the MDA are decomposed and arranged in a sequential manner, making a recursive loop. The efficiency of the SARAM method was verified using three illustrative examples taken from the literatures. Compared with existing methods, it showed the least number of subsystem analyses over other methods while maintaining accuracy.

The Use of Advanced Optical Measurement Methods for the Mechanical Analysis of Shear Deficient Prestressed Concrete Members

  • Wilder, K. De;Roeck, G. De;Vandewalle, L.
    • International Journal of Concrete Structures and Materials
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    • v.10 no.2
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    • pp.189-203
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    • 2016
  • This paper investigates on the use of advanced optical measurement methods, i.e. 3D coordinate measurement machines (3D CMM) and stereo-vision digital image correlation (3D DIC), for the mechanical analysis of shear deficient prestressed concrete members. Firstly, the experimental program is elaborated. Secondly, the working principle, experimental setup and corresponding accuracy and precision of the considered optical measurement techniques are reported. A novel way to apply synthesised strain sensor patterns for DIC is introduced. Thirdly, the experimental results are reported and an analysis is made of the structural behaviour based on the gathered experimental data. Both techniques yielded useful and complete data in comparison to traditional mechanical measurement techniques and allowed for the assessment of the mechanical behaviour of the reported test specimens. The identified structural behaviour presented in this paper can be used to optimize design procedure for shear-critical structural concrete members.

Effect of Sintering Condition on Tensile Strength of Fe-based Non-equiatomic High Entropy Alloy (철계 비동일분율 고엔트로피 합금의 인장 강도에 미치는 소결 조건 영향)

  • Seo, Namhyuk;Jeon, Junhyub;Kim, Gwanghun;Park, Jungbin;Son, Seung Bae;Lee, Seok-Jae
    • Journal of Powder Materials
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    • v.28 no.3
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    • pp.221-226
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    • 2021
  • We fabricate the non-equiatomic high-entropy alloy (NE-HEA) Fe49.5Mn30Co10Cr10C0.5 (at.%) using spark plasma sintering under various sintering conditions. Each elemental pure powder is milled by high-energy ball milling to prepare NE-HEA powder. The microstructure and mechanical properties of the sintered samples are investigated using various methods. We use the X-ray diffraction (XRD) method to investigate the microstructural characteristics. Quantitative phase analysis is performed by direct comparison of the XRD results. A tensile test is used to compare the mechanical properties of small samples. Next, electron backscatter diffraction analysis is performed to analyze the phase fraction, and the results are compared to those of XRD analysis. By combining different sintering durations and temperature conditions, we attempt to identify suitable spark plasma sintering conditions that yield mechanical properties comparable with previously reported values. The samples sintered at 900 and 1000℃ with no holding time have a tensile strength of over 1000 MPa.

Preliminary study on the ground behavior at shore connection of submerged floating tunnel using numerical analysis

  • Kang, Seok-Jun;Kim, Jung-Tae;Cho, Gye-Chun
    • Geomechanics and Engineering
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    • v.21 no.2
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    • pp.133-142
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    • 2020
  • Submerged floating tunnel (SFT) is a type of tunnel which causes the tunnel segments to float in the water. When the SFTs are connected to the ground, the connection between the SFT and the subsea bored tunnel is fragile due to the difference in behavioral characteristics between the two types of tunnels. Therefore, special design and construction methods are needed to ensure the stability of the area around the connection. However, since previous research on the stability of the connection site has not been undertaken enough, the basic step necessitates the evaluation of ground behavior at the shore connection. In this study, the numerical analysis targeting the shore connection between the subsea bored tunnel and the SFT was simulated. The strain concentration at the shore connection was analyzed by numerical simulation and the effects of several factors were examined. The results showed the instability in the ground close to the shore connection due to the imbalance in the behavior of the two types of tunnels; the location of the strain concentration varies with different environmental and structural conditions. It is expected that the results from this study can be utilized in future studies to determine weak points in the shore connection between the submerged floating tunnel and the subsea bored tunnel, and devise methods to mitigate the risks.