• 제목/요약/키워드: adhesive layer

검색결과 543건 처리시간 0.027초

Effect of adhesive application method on repair bond strength of composite

  • Hee Kyeong Oh;Dong Hoon Shin
    • Restorative Dentistry and Endodontics
    • /
    • 제46권3호
    • /
    • pp.32.1-32.10
    • /
    • 2021
  • Objectives: This study aimed to evaluate the effect of the application method of universal adhesives on the shear bond strength (SBS) of repaired composites, applied with different thicknesses. Materials and Methods: The 84 specimens (Filtek Z350 XT) were prepared, stored in distilled water for a week and thermocycled (5,000 cycles, 5℃ to 55℃). They were roughened using 400-grit sandpapers and etched with phosphoric acid. Then, specimens were equally divided into 2 groups; Single Bond Universal (SU) and Prime&Bond Universal (PB). Each group was subdivided into 3 subgroups according to application methods (n = 14); UC: 1 coat + uncuring, 1C: 1 coat + curing, 3C: 3 coats + curing. After storage of the repaired composite for 24 hours, specimens were subjected to the SBS test and the data were statistically analyzed by 2-way analysis of variance and independent t-tests. Specimens were examined with a stereomicroscope to analyze fracture mode and a scanning electron microscope to observe the interface. Results: Adhesive material was a significant factor (p = 0.001). Bond strengths with SU were higher than PB. The highest strength was obtained from the 1C group with SU. Bonding in multiple layers increased adhesive thicknesses, but there was no significant difference in SBS values (p = 0.255). Failure mode was predominantly cohesive in old composites. Conclusions: The application of an adequate bonding system plays an important role in repairing composite resin. SU showed higher SBS than PB and the additional layers increased the adhesive thickness without affecting SBS.

Warm spray를 이용한 알루미늄-알루미나 복합 코팅층의 제조 및 특성 (Manufacturing and Properties of Al-Al2O3 Composite Coating Layer Using Warm Spray Process)

  • 권의표;이종권
    • 한국재료학회지
    • /
    • 제27권7호
    • /
    • pp.374-380
    • /
    • 2017
  • Properties of coatings produced by warm spray were investigated in order to utilize this technique as a repair method for Al tire molds. $Al-(0-10%)Al_2O_3$ composite powder was sprayed on Al substrate by warm spraying, and the microstructure and mechanical properties of the composite coating layer were investigated. For comparative study, the properties of the coating produced by plasma spray, which is a relatively high-temperature spraying process, were also investigated. The composite coating layers produced by the two spray techniques exhibited significantly different morphology, perhaps due to their different process temperatures and velocities of particles. Whereas the $Al_2O_3$ particles in the warm sprayed coating layer maintained their initial shape before the spray, flattened and irregular shape $Al_2O_3$ particles were distributed in the plasma sprayed coating layer. The coating layer produced by warm spray showed significantly higher adhesive strength compared to that produced by plasma spray. Hardness was also higher in the warm sprayed coating layer compared to the plasma sprayed one. Moreover, with increasing the fraction of $Al_2O_3$, hardness gradually increased in both spray coating processes. In conclusion, an $Al-Al_2O_3$ composite coating layer with good mechanical properties was successfully produced by warm spray.

Enhanced Adhesion of Cu Film on the Aluminum Oxide by Applying an Ion-beam-mixd Al Seed Layar

  • 김형진;박재원
    • 한국진공학회:학술대회논문집
    • /
    • 한국진공학회 2012년도 제43회 하계 정기 학술대회 초록집
    • /
    • pp.229-229
    • /
    • 2012
  • Adhesion of Copper film on the aluminum oxide layer formed by anodizing an aluminum plate was enhanced by applying ion beam mixing method. Forming an conductive metal layer on the insulating oxide surface without using adhesive epoxy bonds provide metal-PCB(Printed Circuit Board) better thermal conductivities, which are crucial for high power electric device working condition. IBM (Ion beam mixing) process consists of 3 steps; a preliminary deposition of an film, ion beam bombardment, and additional deposition of film with a proper thickness for the application. For the deposition of the films, e-beam evaporation method was used and 70 KeV N-ions were applied for the ion beam bombardment in this work. Adhesions of the interfaces measured by the adhesive tape test and the pull-off test showed an enhancement with the aid of IBM and the adhesion of the ion-beam-mixed films were commercially acceptable. The mixing feature of the atoms near the interface was studied by scanning electron microscopy, Auger electron spectroscopy, and X-ray photoelectron spectroscopy.

  • PDF

전단하중하의 반도체 칩 접착계면의 특이응력 해석 (Analysis of Singular Stresses at the Bonding Interface of Semiconductor Chip Subjected to Shear Loading)

  • 이상순
    • 마이크로전자및패키징학회지
    • /
    • 제7권4호
    • /
    • pp.31-35
    • /
    • 2000
  • 반도체 칩과 리드프레임을 접착하고 있는 얇은 접착제층에 전단하중이 가해질 때 발생하는 응력상태를 조사하고 있다. 계면 응력상태를 해석하기 위해서 경계요소법이 사용되고 있다. 선형 탄성이론을 적용하여 해석하면, 강체와 접착제의 계면이 자유 경 계면과 만나는 부분에서 $\gamma^{\lambda=1}$(0<1<1) 형태의 응력 특이성이 존재한다. 이러한 특이성으로 인해, 모서리 균열이나 계면 박리가 발생할 수 있다.

  • PDF

상아질과 접착제 간의 계면양상 (INTERFACIAL MORPHOLOGY BETWEEN DENTIN AND ADHESIVES)

  • 강지영;허복
    • Restorative Dentistry and Endodontics
    • /
    • 제20권1호
    • /
    • pp.183-192
    • /
    • 1995
  • The purpose of this study was to evaluate the effect of smear layer management on the interfacial morphology between dentin bonding system and dentin. Clearfil New Bond, Scotchbond Multipurpose, Prisma Universal Bond 3 and X-R Bond were used on the cervical dentinal surfaces of bovine incisor teeth. All of the dentin bonding systems were labeled with fluorescene in primer and rhodamine B in adhesive. Specimens of 2~3mm thichness were prepared by longitudinal and labiolingual sectioning. The interface between dentin bonding system and dentin was observed by flouresence imaging with a confocal laser scanning microscope. Following results were obtained. 1. In the specimen of Clearfil New Bond, dentinal tubules were widened by destruction of peritubular dentin in the course of treatment with phosphoric acid of high concentration. 2. Hybrid layer was observed in the specimen of Scotchbond Multipurpose and X-R Bond. 3. In the specimen of Prisma Universal Bond 3, the penetraton of adhesive was not observed clearly.

  • PDF

Predictions of the maximum plate end stresses of imperfect FRP strengthened RC beams: study and analysis

  • Rabia, Benferhat;Daouadji, Tahar Hassaine;Abderezak, Rabahi
    • Advances in materials Research
    • /
    • 제9권4호
    • /
    • pp.265-287
    • /
    • 2020
  • A theoretical method to predict the interfacial stresses in the adhesive layer of reinforced concrete beams strengthened with porous FRP plate is presented in this paper. The effect due to porosity is incorporated utilizing a new modified rule of mixture covering the porosity phases. The adherend shear deformations have been included in the present theoretical analyses by assuming a linear shear stress through the thickness of the adherends. Remarkable effect of the porosity has been noted in the results. Indeed, the resulting interfacial stresses concentrations are considerably smaller than those obtained by other models which neglect the porosity effect. It was found that the interfacial stresses are highly concentrated at the end of the FRP plate, the minimization of the latter can be achieved by using porous FRP plate in particular at the end. It is also shown that the interfacial stresses of the RC beam increase with volume fraction of fibers, but decrease with the thickness of the adhesive layer.

지하 구조물용 비노출형 방수재의 외부환경에 따른 방수재의 성능 변화 요구 (Waterproofing Materials According to the External Environment of Non-exposed Waterproofing Materials for Underground Structures Performance Change Requirement)

  • 정석주;송제영;원승재;오상근
    • 한국건축시공학회:학술대회논문집
    • /
    • 한국건축시공학회 2020년도 봄 학술논문 발표대회
    • /
    • pp.85-86
    • /
    • 2020
  • In securing durability of underground structure non-exposed waterproof materials, the company aims to improve durability of waterproof materials by studying more realistic weather conditions than KS standards and developers' durability standards. Analyzing the actual climate data in Korea and the temperature of the basement layer, it is a waterproofing sheet method, a self-adhesive sheet method in which a film and a compound, which are currently widely used as underground water-proofing, and a self-adhesive waterproofing sheet method, etc. We would like to present the guidelines necessary to prevent the temperature situation and waterproof defects that are ideal for setting the endurance conditions later.

  • PDF

카라신과 어류 3종의 수정란 난막 미세구조에 대한 비교 연구 (A Comparative Study on the Ultrastructures of the Egg Envelope in Fertilized Eggs of Fishes, Characidae, Three Species)

  • 김동희;류동석;등영건
    • Applied Microscopy
    • /
    • 제26권3호
    • /
    • pp.277-291
    • /
    • 1996
  • The structures of the egg envelope in fertilized eggs of three species of characidae, head and tail light fish (Hemigrammus ocellifer), black tetra (Gymnocorymbus ternetzi), and buenos aires tetra (Hemigrammus caudovittatus) were studied using light and electron microscopes. The fertilized eggs in all species were colorless, transparent, spherical and non-floted type. The egg envelopes have a single micropyle resembling the pathway of sperm in the area of the animal pole. The micropyle was surrounded by protruded lines of the egg envelope in a radiated form. Egg envelopes of fertilized eggs in both head and tail light fish and buenos aires tetra consisted of three distinct layers; an outer layer, a middle layer and an inner layer. And that of blacktetra consisted of two layers; an outer layer and an inner layer. Also, an outer layers of both head and tail light fish and black tetra were adhesive types but, in that of buenous aires tetra was non-adhesive type. An outer surface of egg envelope in black tetra was arranged by pores regularly. In that of head and tail light fish and buenos aires tetra have a rough side. An inner layer of egg envelope in fertilized eggs consisted of lamellae alternating with interlamellae of lower electron density; an inner layer of fertilized eggs in head and tail light fish consisted of three layers, that of black tetra was four layers, and that of buenos aires tetra was five layers.

  • PDF