• Title/Summary/Keyword: adhesive energy

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The effect of resin cements and primer on retentive force of zirconia copings bonded to zirconia abutments with insufficient retention

  • Kim, Seung-Mi;Yoon, Ji-Young;Lee, Myung-Hyun;Oh, Nam-Sik
    • The Journal of Advanced Prosthodontics
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    • v.5 no.2
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    • pp.198-203
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    • 2013
  • PURPOSE. The purpose of this study was to investigate the effect of resin cements and primer on the retentive force of zirconia copings bonded to zirconia abutments with insufficient retention. MATERIALS AND METHODS. Zirconia blocks (Lava, 3M ESPE, St. Paul, MN, USA) were obtained and forty sets of zirconia abutments and copings were fabricated using CAD/CAM technology. They were grouped into 4 categories as follows, depending on the types of resin cements used, and whether the primer is applied or not:Panavia F2.0 (P), Panavia F2.0 using Primer (PRIME Plus, Bisco Inc, Schaumburg, IL, USA) (PZ), Superbond C&B (S), and Superbond C&B using Primer (SZ). For each of the groups, the cementation was conducted. The specimens were kept in sterilized water ($37^{\circ}C$) for 24 hours. Retentive forces were tested and measured, and a statistical analysis was carried out. The nature of failure was recorded. RESULTS. The means and standard deviations of retentive force in Newton for each group were $265.15{\pm}35.04$ N (P), $318.21{\pm}22.24$ N (PZ), $445.13{\pm}78.54$ N (S) and $508.21{\pm}79.48$ N (SZ). Superbond C&B groups (S & SZ) showed significantly higher retentive force than Panavia F2.0 groups (P & PZ). In Panavia F2.0 groups, the use of primer was found to contribute to the increase of retentive force. On the other hand, in Superbond C&B groups, the use of primer did not influence the retention forces. Adhesive failure was observed in all groups. CONCLUSION. This study suggests that cementation of the zirconia abutments and zirconia copings with Superbond C&B have a higher retentive force than Panavia F2.0. When using Panavia F2.0, the use of primer increases the retentive force.

A STUDY ON THE SHEAR BOND STRENGTH BY PLASMA ARC CURING SYSTEM FOR BRACKET BONDING (Plasma arc curing system을 이용한 브라켓의 접착에 관한 연구)

  • Kim, Jung-Yoon;Kim, Jong-Soo;Kwon, Soon-Won
    • Journal of the korean academy of Pediatric Dentistry
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    • v.28 no.4
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    • pp.638-642
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    • 2001
  • Recently, plasma arc curing system for curing resin composites has been introduced. This is characterized by a high output of light energy, which has the advantage of reducing the chair time and thereby making the treatment more comportable for the patients as well as for the dentist. The purpose of this study was to compare the shear bond strengths of light-cured orthodontic adhesive polymerized with conventional halogen light and plasma arc light. The 2 curing devices used were the XL3000 (3M, USA) conventional curing light and the Flipo (LOKKI, France) plasma arc light. The results from the present study can be summarized as fellows; 1. The mean shear bond strength for three groups were quite similar for 50 second conventional light group, 2 second plasma arc curing light group, 5 second plasma arc curing light group. 2. There was no statistically significant difference for three groups(p>0.05).

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Quality Characteristics of Mixed Polysaccharide Gels with Various Kiwifruit Contents (키위 첨가량에 따른 다당류 혼합겔의 품질 특성)

  • 윤혜신;오명숙
    • Korean journal of food and cookery science
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    • v.19 no.4
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    • pp.511-520
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    • 2003
  • This study was carried out to determine the effects of various contents of kiwifruit contents on the quality characteristics of mixed polysaccharide gels made from $\kappa$-carrageenan and locust bean gum. The color value, gelling temperature, melting temperature, break down rate, syneresis, rupture properties, TPA properties and sensory properties of mixed polysaccharide gels with various contents of kiwifruit contents were measured. As the kiwifruit contents was increased, the lightness (L), yellowness (b) and greenness (-a) of the mixed polysaccharide gels increased. There were no differences in the color values of gels during storage. As the kiwifruit content was increased, the gelling and melting temperatures of the mixed polysaccharide gels also increased. The mixed polysaccharide gels with high kiwifruit contents were difficult to melt, and it seemed that the addition of kiwifruit to the mixed polysaccharide gels could improve the thennal stability of the gels. The syneresis of the gel increased with increasing storage time, whereas the addition of kiwifruit to the gel resulted in suppression of syneresis. With regard to the rupture properties, stress, energy and strain, they were all decreased with increasing kiwifruit contents. The TPA properties, adhesiveness, hardness and chewiness increased and cohesiveness decreased with increasing kiwifruit contents. The results showed that the gel became tough and adhesive, and could be easily broken under small deformation, with increasing kiwifruit contents. The sensory evaluation showed that the green color, aroma, sweetness and sourness increased with increasing kiwifruit contents. The texture, adhesiveness, springiness and cohesiveness decreased, and brittleness and hardness increased, with increasing kiwifruit contents. The overall acceptability of the gel with 30% kiwifruit content was the highest. Thus, mixed polysaccharide gels made from kiwifruits could be useful, as the addition of kiwifruit to a mixed polysaccharide gel results in a good aroma, taste and stability, despite a lowering of the textural properties.

A Method to Determine Amount of Adsorbed Oil in Hair Washing Using Absorption Spectroscopy (흡수 분광법을 이용한 세정 과정에서 흡착된 오일의 평가)

  • Song, Sang-Hun;Kim, Hyun young;Son, Seong Gil
    • Journal of the Society of Cosmetic Scientists of Korea
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    • v.45 no.2
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    • pp.105-116
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    • 2019
  • Oil adsorption during hair or body washing is responsible for the hair conditioning. In this study, we established a method to extract oil from a substrate, and to determine amount of adsorbed oil upon substrate using a conventional absorption spectroscopy. We controlled the mole fraction of a surfactant in a mixture of anionic and amphoteric surfactants because that it induces the coacervate that regulates amount of adsorbed oil through the alteration of oil viscosity. Based on this, we established the optimized condition for adsorption and extraction for oil. UV absorbance were employed to estimate the amount of adsorbed oil using optical absorbance after extraction via adsorption. The estimation was confirmed by comparing with a mass analysis in HPLC and an adhesive energy in AFM. It has been proved that this method can be applied to all cases of oil adsorption from the results with various cationic polymers and a complex system of the polymers which regulate the oil adsorption.

Flexural behavior of reinforced concrete beams strengthened with an ultra-high performance concrete panel of various thicknesses

  • Seonhyeok Kim;Taegeon Kil;Sangmin Shin;Daeik Jang;H.N. Yoon;Jin-Ho Bae;Joonho Seo;Beomjoo Yang
    • Computers and Concrete
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    • v.32 no.5
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    • pp.487-498
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    • 2023
  • The present study investigated the flexural behavior of reinforced concrete (RC) beams strengthened with an ultrahigh performance concrete (UHPC) panel having various thicknesses. Two fabrication methods were introduced in this study; one was the direct casting of UHPC onto the bottom surface of the RC beams (I-series), and the other was the attachment of a prefabricated UHPC panel using an adhesive (E-series). UHPC panels having thicknesses of 10, 30, 50, and 70 mm were applied to RC beams, and these specimens were subjected to four-point loading to assess the effect of the UHPC thickness on the flexural strengthening of RC beams. The test results indicated that the peak strength and initial stiffness were vastly enhanced with an increase in the thickness of the UHPC panel, showing an improved energy dissipation capacity. In particular, the peak strength of the E-series specimens was higher than that of I-series specimens, showing high compatibility between the RC beam and the UHPC panel. The experimental test results were comparatively explored with a discussion of numerical analysis. Numerical analysis results showed that the predictions are in fair agreement with experimental results.

Method for the Assembly of a High-density Multi-channel Deformable Mirror for High Energy Lasers (고에너지 레이저용 고밀집 다채널 실리콘-카바이드 변형거울의 정밀 조립 방법)

  • Hyug-Gyo Rhee;Sunho Cho;Sihyun Kim;Jaehyun Lee;Pilseong Kang
    • Korean Journal of Optics and Photonics
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    • v.35 no.4
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    • pp.170-174
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    • 2024
  • A laser beam propagating in free space can be negatively affected by atmospheric turbulence. To overcome this and correct the wavefront error of the laser beam itself, a deformable mirror (DM), which is a key component of adaptive optics, is widely used. In this paper, a novel precision assembling method is suggested for a multi-channel high-density DM. The material of the mirror sheet of the DM is silicon carbide (SiC), and the actuator is a stacked-type lead-magnesium-niobate (Pb(Mg1/3Nb2/3)O3; PMN). To connect the mirror sheet and each actuator, a flexure is inserted. The flexure can make the DM operate with full strokes without the failure of adhesive. A series of jigs were designed and applied in order to assemble these three parts (the mirror sheet, actuators, and flexures) precisely. After assembly, the performance of the DM was also checked.

A Study on Micro-insect Screens Using Coffee Grounds (커피찌꺼기를 활용한 미세방충망 연구)

  • Yu Kyung Lee;Gyuri Kim;Min Ji Woo;Ga In Cho;Donghyeon Lee;Mantae Kim;Dong-Jun Kwon
    • Composites Research
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    • v.37 no.4
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    • pp.363-368
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    • 2024
  • Due to the increase in coffee consumption, the amount of coffee grounds is also increasing, which leads to environmental problems. In order to solve these problems, this study proposes the utilisation of coffee grounds. In particular, the porous structure of coffee grounds was utilised to optimise a micro insect screen for filtering fine dust. To realize the porous structure of coffee grounds, a polar/non-polar separation method using KOH and n-hexane was applied to obtain coffee grounds with increased porosity. In addition, the composition of an eco-friendly adhesive was identified to fix the coffee grounds to the screen, and the conditions for homogeneous adhesion of the coffee grounds to the screen were optimised. As a result, we confirmed the effect of the number of coatings of coffee grounds on the filtering effect of fine dust, and found that two coatings of coffee grounds increased the filtering.

Mixed Mode Analysis using Two-step Extension Based VCCT in an Inclined Center Crack Repaired by Composite Patching (복합재료 팻칭에 의한 중앙경사균열에서 2단계 확장 가상균열닫힘법을 사용한 혼합모우드해석)

  • Ahn, Jae-Seok;Woo, Kwang-Sung
    • KSCE Journal of Civil and Environmental Engineering Research
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    • v.32 no.1A
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    • pp.11-18
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    • 2012
  • This paper deals with the numerical determination of the stress intensity factors of cracked aluminum plates under the mixed mode of $K_I$ and $K_{II}$ in glass-epoxy fiber reinforced composites. For the stress intensity factors, two different models are reviewed such as VCCT and two-step extension method. The p-convergent partial layerwise model is adopted to determine the fracture parameters in terms of energy release rates and stress intensity factors. The p-convergent approach is based on the concept of subparametric element. In assumed displacement field, strain-displacement relations and 3-D constitutive equations of a layer are obtained by combination of 2-D and 1-D higher-order shape functions. In the elements, Lobatto shape functions and Gauss-Lobatto technique are employed to interpolate displacement fields and to implement numerical quadrature. Using the models and techniques considered, effects of composite laminate configuration according to inclined angles and adhesive properties on the performance of bonded composite patch are investigated. In addition to these, the out-of-plane bending effect has been investigated across the thickness of patch repaired laminate plates due to the change of neutral axis. The present model provides accuracy and simplicity in terms of stress intensity factors, stress distribution, number of degrees of freedom, and energy release rates as compared with previous works in literatures.

Interfacial Evaluation and Microfailure Sensing of Nanocomposites by Electrical Resistance Measurements and Wettability (전기저항측정법 및 젖음성을 이용한 나노복합재료의 미세파손 감지능 및 계면물성 평가)

  • Park, Joung-Man;Kwon, Dong-Jun;Shin, Pyeong-Su;Kim, Jong-Hyun;Baek, Yeong-Min;Park, Ha-Seung
    • Composites Research
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    • v.30 no.2
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    • pp.138-144
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    • 2017
  • Damage sensing of polymer composite films consisting of poly(dicyclopentadiene) p-DCPD and carbon nanotube (CNT) was studied experimentally. Only up to 1st ring-opening polymerization occurred with the addition of CNT, which made the modified film electrically conductive, while interfering with polymerization. The interfacial adhesion of composite films with varying CNT concentration was evaluated by measuring the wettability using the static contact angle method. 0.5 wt% CNT/p-DCPD was determined to be the optimal condition via electrical dispersion method and tensile test. Dynamic fatigue test was conducted to evaluate the durability of the films by measuring the change in electrical resistance. For the initial three cycles, the change in electrical resistance pattern was similar to the tensile stress-strain curve. The CNT/p-DCPD film was attached to an epoxy matrix to demonstrate its utilization as a sensor for fracture behavior. At the onset of epoxy fracture, electrical resistance showed a drastic increase, which indicated adhesive fracture between sensor and matrix. It leads to prediction of crack and fracture of matrix.

Properties of ZnO:Ga Transparent Conducting Film Fabricated on O2 Plasma-Treated Polyethylene Naphthalate Substrate (산소플라즈마 전처리된 Polyethylene Naphthalate 기판 위에 증착된 ZnO:Ga 투명전도막의 특성)

  • Kim, Byeong-Guk;Kim, Jeong-Yeon;Oh, Byoung-Jin;Lim, Dong-Gun;Park, Jae-Hwan;Woo, Duck-Hyun;Kweon, Soon-Yong
    • Korean Journal of Materials Research
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    • v.20 no.4
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    • pp.175-180
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    • 2010
  • Transparent conducting oxide (TCO) films are widely used for optoelectronic applications. Among TCO materials, zinc oxide (ZnO) has been studied extensively for its high optical transmission and electrical conduction. In this study, the effects of $O_2$ plasma pretreatment on the properties of Ga-doped ZnO films (GZO) on polyethylene naphthalate (PEN) substrate were studied. The $O_2$ plasma pretreatment process was used instead of conventional oxide buffer layers. The $O_2$ plasma treatment process has several merits compared with the oxide buffer layer treatment, especially on a mass production scale. In this process, an additional sputtering system for oxide composition is not needed and the plasma treatment process is easily adopted as an in-line process. GZO films were fabricated by RF magnetron sputtering process. To improve surface energy and adhesion between the PEN substrate and the GZO film, the $O_2$ plasma pre-treatment process was used prior to GZO sputtering. As the RF power and the treatment time increased, the contact angle decreased and the RMS surface roughness increased significantly. It is believed that the surface energy and adhesive force of the polymer surfaces increased with the $O_2$ plasma treatment and that the crystallinity and grain size of the GZO films increased. When the RF power was 100W and the treatment time was 120 sec in the $O_2$ plasma pretreatment process, the resistivity of the GZO films on the PEN substrate was $1.05\;{\times}\;10^{-3}{\Omega}-cm$, which is an appropriate range for most optoelectronic applications.