• Title/Summary/Keyword: acetate

Search Result 5,813, Processing Time 0.032 seconds

Studies on Pullorum Disease II. The Effect of Cortisone Acetate, Estrogenic Hormone and Tocopherol on the Diagnosis of Reactors of Pullorum Disease (닭의 추백리병에 관한 연구 II. 추백리병 진단에 있어서 Hormone 효과에 관한 연구)

  • Choi, J.Y.;Lee, S.Y.;Lee, C.K.
    • Korean Journal of Veterinary Research
    • /
    • v.10 no.2
    • /
    • pp.7-12
    • /
    • 1970
  • This study was conducted to abserve the effects of cortisone acetate, estrogenic hormone and tocopherol on the antibody tresponse to both pullorum suspects and negatives of The increase of antibody titer was shown in a few birds after the treatment of either cortisone acetate or estrogenic hormone. There wuas no change in antibody titer of chickens treated with tocopherol.

  • PDF

Emulsion Polymerization of Vinyl Acetate with Triton-X as Emulsifier (Triton X 系를 乳化劑로 하는 Vinyl Acetate 의 乳化重合)

  • Chung, Ki-Hyun;Han, Sang-Ku
    • Journal of the Korean Chemical Society
    • /
    • v.6 no.1
    • /
    • pp.19-24
    • /
    • 1962
  • In the emulsion polymerization of vinyl acetate with Triton-X(Alkyl-aryl-polyether alcohol) and polyvinyl alcohol as emulsifier, some relations between the conditions of polymerization and the polymerization rate, polymerization degree and stability of the emulsion are studied and discussed.

  • PDF

Anti-tumor Activity of Acanthospermum hispidum DC on Dalton Ascites Lymphoma in Mice

  • Rajendran, N.N.;Deepa, N.
    • Natural Product Sciences
    • /
    • v.13 no.3
    • /
    • pp.234-240
    • /
    • 2007
  • The present study investigated the anti-tumor activity of ethyl acetate extract of Acanthospermum hispidum DC against daltons ascites lymphoma in mice. The extract was prepared by cold maceration with ethyl acetate for 3 - 7 days and evaporated in vacuum to dry. (Yield : 14.2 g, 1.42% w/w). The extract was fractionated by column chromatography by using gradient elution technique and the diterpenes fraction isolated (0.649 g). Both extract and the fraction were administered as oral suspension with tween 20 in water to tumor bearing mice (DAL) and changes in dead cell count, histopathology of tumor cells, hematological parameters and median survival time (MST) were examined and compared with that of tumor control or 5-Fluorouracil (5-FU). The results indicate that both ethyl acetate extract and fraction possess anti-tumor activity. The study suggests that Acanthospermum hispidum DC seems promising as a source of diterpenes for potential anti-tumor activity.

Quality Evaluation of Alismatis Rhizoma by High Performance Liquid Chromatography

  • Lee Sang-Myung;Kang Jong-Seong;Hwang Gwi-Seo;Kim Young-Ho;Lee Cheal-Gyu;Yeo Woon-Hyung;Bae Ki-Hwan
    • Archives of Pharmacal Research
    • /
    • v.27 no.4
    • /
    • pp.460-464
    • /
    • 2004
  • The quality of Alismatis Rhizoma was evaluated by reversed-phase high performance liquid chromatographic method. Alisol B 23-acetate was used as a standard marker for evaluation. This component was fully separated from the other components in the plant extracts on a ODS column. Identifcation of alisol B 23-acetate was carried out by comparing the LC/MS spectrum of separated peak from the extract with that of standard. Alisol B 23-acetate contents in Alismatis Rhizoma obtained from several herbal markets were varied from $0. 15\%$ to $0.56\%$.

Organic Thin Film Transistors with Gate Dielectrics of Plasma Polymerized Styrene and Vinyl Acetate Thin Films

  • Lim, Jae-Sung;Shin, Paik-Kyun;Lee, Boong-Joo
    • Transactions on Electrical and Electronic Materials
    • /
    • v.16 no.2
    • /
    • pp.95-98
    • /
    • 2015
  • Organic polymer dielectric thin films of styrene and vinyl acetate were prepared by the plasma polymerization deposition technique and applied for the fabrication of an organic thin film transistor device. The structural properties of the plasma polymerized thin films were characterized by Fourier-transform infrared spectroscopy, X-ray diffraction, atomic force microscopy, and contact angle measurement. Investigation of the electrical properties of the plasma polymerized thin films was carried out by capacitance-voltage and current-voltage measurements. The organic thin film transistor device with gate dielectric of the plasma polymerized thin film revealed a low operation voltage of −10V and a low threshold voltage of −3V. It was confirmed that plasma polymerized thin films of styrene and vinyl acetate could be applied to functional organic thin film transistor devices as the gate dielectric.

Fluorine Labeling in Biosynthetic Studies (I) : Synthesis of Fluorfarnesols

  • Park, O-Sook
    • Archives of Pharmacal Research
    • /
    • v.9 no.4
    • /
    • pp.237-242
    • /
    • 1986
  • The Synthesis of E, E, E-12-fluorofarnesol and E, Z-6-fluorofarnesol which are key intermediates for the study of biosynthesis of some sesquiterpenes, is described. E, E-Farnesyl acetate is treated with selenium dioxide to give E, E, E-12-hydroxy farnesyl acetate, whih is transformed by DAST into E, E, E-12-hydroxy farnesyl acetate, which is transformed by DAST into E, E, E,-12-fluorofarnesylacetate. The latter compound is hydrolyzed to E, E, E,-12-fluorofarnesol. The reformatsky reaction of 6-methyl-5-hepten-2-one with ethyl bromofluoroacetate affords ethyl 2-fluoro-3-hydroxy-3, 7 dimethyl-6-octanoate. This ester is acetylated and eliminated to give ethyl (Z)-2-fluoro-3, 7-dimethylocta-2, 6-dienoate, which is transformed to allyl bromide via allylic alcohol. The allyl bromide is treated with dianion of methyl acetate to give-keto ester. The $\beta$-keto ester is converted to diethyl phosphoryloxy compound. The conjugate addition of lithium dimethylcuprate to the latter compound gives fluoro ester, which is treated with DIBAL to afford E, Z-6-fluorofarnesol.

  • PDF

Photosensitive Effects of Poly(vinyl cinnamoyl acetate) by New Squarylium Dyes(II) (신규 Squarylium Dyes에 의한 Poly(vinyl cinnamoyl acetate)의 고감도화(II))

  • 손세모;곽선엽
    • Journal of the Korean Graphic Arts Communication Society
    • /
    • v.18 no.1
    • /
    • pp.113-120
    • /
    • 2000
  • A previous paper was reported in being sensetized photopolymer, poly(vinyl cinnamoyl acetate) (PVCiA)1) with some squarylium dyes such as 1,3-bis(4 or 6-trifluouomethy1-1,3,3-trimethylindo) squarylium dyes(TFSQ). Here, we synthesized new 1,3-bis(4 or 6-nitro-1,3,3-trimethylindo) squarylium dyes(NISQ) to sensetize photopolymer, such as poly(vinyl cinnamoyl acetate). Absorption's coefficient of (NISQ8) is 8.5x105, the sensitivity of PVCiA added with NISQ8(3%) was highly sensitized 8 times than not added, and 2 times than TFSQ8(3%). Maybe, high absorption'scoefficient and red shift of NISQs with strongly withdrawing group to TFSQs afford to the high sensitivity of PVCiA.

  • PDF

Vapor Permeation of Aqueous Ester Solutions Through Surface-modified Alumina Membrane (표면 개질한 알루미나막을 통한 ester 수용액의 증기 투과)

  • 오한기;송근호;이광래
    • Membrane Journal
    • /
    • v.10 no.4
    • /
    • pp.186-191
    • /
    • 2000
  • The recovery of three ethyl esters (aroma model compounds; ethyl acetate, ethyl propionate. ethyl butyrate) from aqueous solutions was studied for vapor permeation with surface-modified hydrophobic alumina membrane, Although the driving force of ethyl butyrate is the highest, the ethyl butyrate concentration in permeate is lower than those of propionate and acetate. Since the solubility of aroma compounds for water is very low, phase separation occurred in permeate, and we could obtain pure ethyl esters. The experimental results showed that the porous hydrophobic alumina membrane had high selectivity and permeation flux on the ester-model compounds.

  • PDF

Three Dimensionally Ordered Microstructure of Polycrystalline Zirconia Ceramics with Micro-Porosity

  • Chang, Myung Chul
    • Journal of the Korean Ceramic Society
    • /
    • v.53 no.1
    • /
    • pp.50-55
    • /
    • 2016
  • In order to make a highly ordered three-dimensionally macro-porous structure of zirconia ceramics, porogen precursors PMMA beads were prepared by emulsion polymerization using acrylic monomer. The monodisperse PMMA latex beads were closely packed by centrifugation as a porogen template for the infiltration of zirconium acetate solution. The mixed compound of PMMA and zirconium acetate was dried. According to the firing schedule, dry compacts of PMMA and zirconium acetate were calcined at $475^{\circ}C$ to obtain micro-, macro-, and meso- structures of polycrystalline zirconia with monodispersed porosity. Inorganic frameworks composed of $ZrO_2$ were formed and showed a three Dimensionally Ordered Microstructure [3DOM] of $ZrO_2$ ceramics. The obtained $ZrO_2$ skeleton was calcined at $710^{\circ}C$. The 3DOM $ZrO_2$ skeleton showed color tuning in solutions such as deionized [DI] $H_2O$ and/or methanol. The monodispersed crystalline micro-structure with micro/meso porosity was observed by FE-SEM.