• 제목/요약/키워드: accelerated heat-treatment

검색결과 82건 처리시간 0.026초

열처리 인공촉진열화가 배접지의 광학적 및 기계적 특성에 미치는 영향 (Optical & Mechanical Characteristics of Lining Papers by the Artificial Heat Ageing Treatment)

  • 정선화;최경화;박지희;강영석;윤경동
    • 보존과학연구
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    • 통권30호
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    • pp.93-102
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    • 2009
  • This study was carried out to investigate the effect of artificial accelerated ageing treatment on the permanence of lining papers produced from Korea and Japan. As time gone by, organic cultural properties are affected by chemical and physical deterioration because of various factors including the conditions of preservation environment and their material properties. In the public historical storage or owned as private collections, are vulnerable to sever amages caused by poor preservation environment as well as by other natural factors. In this study, the deterioration behaviors of lining paper in optical & mechanical properties were discussed. Overall, lining papers produced from Korea showed lower reduction in mechanical strength properties compared to the lining papers produced from Japan.

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Glass Remote Phosphor 구조를 갖는 백색 LED 패키지의 형광체 함량과 열처리 온도 최적화 (Optimization of Phosphor Contents and Heat-treatment Temperature in White LED Package with Glass Remote Phosphor Structure)

  • 정희석;홍석기;염정덕
    • 조명전기설비학회논문지
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    • 제30권3호
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    • pp.30-38
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    • 2016
  • In this research, a 6W white LED package with a Glass Remote Phosphor was developed to improve the life of an LED package. The Glass Remote Phosphor was fabricated by the Phosphor in Glass (PiG) method, wherein phosphor YAG:Ce was mixed with glass frit and then heat treated. A paste with 75wt.% of a phosphor substance and 25wt.% glass frit was coated on a glass substrate two times using the screen-printing technique and heat-treated at $800^{\circ}C$ ; this structure gave a luminous efficacy of 136.1lm/W, color rendering index of 74Ra, and color temperature of 5,342K, thus satisfying the requirements as a light source for lighting. Moreover, an IES LM-80 accelerated life test was conducted on the same LED package for 6,000h in order to estimate the L70 lifetime based on IES TM-21. The results showed guaranteed lifetimes of 213,000h at $55^{\circ}C$, 245,000h at $85^{\circ}C$, and 209,000h at $95^{\circ}C$.

발전설비 보일러 튜브용 X20강의 가속열처리에 의한 재질 열화 (Material Degradation of X20 Steel (12Cr-1MoVNi) for Boiler Tube of Power Plant)

  • 최병학;윤기봉;이남혁;김신;이길재;김광호;권동일
    • 대한금속재료학회지
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    • 제46권5호
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    • pp.276-282
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    • 2008
  • Material degradation of Cr steels in boiler tubes was accompanied by the microstructural changes including carbide behavior and crack formation. The microstructural change and the mechanical behavior of hardness and creep properties in accelerated heat-treatments were studied in order to identify the material degradation of the X20 Cr steel. The degradation behavior was occurred in the hardness increasing followed by decreasing due to carbide dissolution and precipitation.

Ti-6Al-4V 합금의 알칼리 및 열처리가 인산칼슘 침착에 미치는 영향 (Effect of Alkali and Heat Treatments of Ti-6Al-4V Alloy on the Precipitation of Calcium Phosphate)

  • 박재한;임기정;김상목;김병옥;한경윤
    • Journal of Periodontal and Implant Science
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    • 제30권1호
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    • pp.187-203
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    • 2000
  • The precipitation of calcium phosphate on implant surface has been known to accelerate osseointegration and to enhance osseous adaptation. The present study was performed to examine whether the precipitation of calcium phosphate on Ti-6Al-4V alloy could be affected by the immersion in NaOH solution and heat treatment. Ti-6Al-4V alloy plates of $15{\times}3.5{\times}1mm$ in dimension were polished sequentially from #240 to #2,000 emery paper and one surface of each specimen was additionally polished with $0.1{\mu}m$ alumina paste. Polished specimens were soaked in various concentrations of NaOH solution(0.1, 1.0, 3.0, 5.0, 7.0, 10.0 M) at $60^{\circ}C$ for 24 hours for alkali treatment, and 5.0 M NaOH treated specimens were heated for 1 hour at each temperature of 400, 500, 600, 700, $800^{\circ}C$. After the alkali and heat treatments, specimens were soaked in the Hank's solution with pH 7.4 at $36.5^{\circ}C$ for 30days.The surface ingredient change of Ti-6Al-4V alloy was evaluated by thin-film X-ray diffractometer(TF-XRD) and the surface microstructure was observed by scanning electron microscope(SEM), and the elements of surface were analyzed by X-ray photoelectron spectroscopy(XPS). The results were obtained as follows ; 1. The precipitation of calcium phosphate on Ti-6Al-4V alloy was accelerated by the immersion in NaOH solution and heat treatment. 2. In Alkali treatment for the precipitation of calcium phosphate on Ti-6Al-4V alloy, the optimal concentration of NaOH solution was 5.0 M. 3. In heat treatment after alkali treatment in 5.0 M NaOH solution, the crystal formation on alloy surface was enhanced by increasing temperature. In heat treated alloys at $600^{\circ}C$, latticed structure and prominences of calcium phosphate layer were most dense. On heat treated alloy surface at the higher temperature(${\geq}700^{\circ}C$), main crystal form was titanium oxide rather than apatite. The above results suggested that the precipitation of calcium phosphate on the surface of Ti-6Al-4V alloy could be induced by alkali treatment in 5.0 M-NaOH solution and by heat treatment at $600^{\circ}C$.

감육배관의 건전성평가 및 정비 관련 기술기준 고찰 (Review on the Integrity Evaluation and Maintenance of Wall-Thinned Pipe)

  • 이성호;이요섭;김홍덕;이경수;황경모
    • 한국압력기기공학회 논문집
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    • 제11권2호
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    • pp.51-60
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    • 2015
  • Local wall thinning and integrity degradation caused by several mechanisms, such as flow accelerated corrosion, cavitation, flashing and/or liquid droplet impingement, is a main concern in secondary steam cycle piping system of nuclear power plants in terms of safety and operability. Thinned pipe management program (TPMP) has being developed and optimized to reduce the possibility of unplanned shutdown and/or power reduction due to pipe failure caused by wall thinning. In this paper, newest technologies, standards and regulations related to the integrity assessment, repair and replacement of thinned pipe component are reviewed. And technical improvement items in TPMP to secure the reliability and effectiveness are also presented.

고탄소강의 흑연화에 미치는 Ni첨가의 영향 (Effects of Ni additions on Graphitization in High carbon steel)

  • 박영구;우기도;진영철;류재화;박종현
    • 열처리공학회지
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    • 제12권1호
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    • pp.55-65
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    • 1999
  • Graphitization of cementite in high carbon steels at subcritical temperature is reported. We have studied about the effects of Ni in these steels on graphitization. The chemical compositions of the specimens were Fe-(0.54, 0.7)%-C-1.0%Si-0.1%Mn-(0.2~1.0)%Ni. After annealing at $650^{\circ}C$, $680^{\circ}C$ and $700^{\circ}C$ during various time the microstructures and hardness change were observed. In order to recover the initial hardness of high carbon steel, dissolution treatment of graphite was performed at $870^{\circ}C$. In case of 0.7%C steel, graphitization was accelerated rather 1.0%Ni addition steel than 0.2% and 0.54%Ni addition steels but the graphite is coarser. In case of 0.54%C-0.2%Ni steel, graphite particles were distributed relatively homogeniously and finely. Nickel addition promotes graphitization of these steels but makes graphite blocky.

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조선왕조실록 밀랍본 복원기술연구(제2보) - 실록의 복원용지 탐색을 위한 전통한지의 열화특성 평가 - (The Study of Restoration Technique of Wax-Treated Volume for the Annals of the Joseon Dynasty(II) - Evaluation of aging characteristics of Korean traditional paper, Hanji as the restoration material of the annals -)

  • 정선화;정소영;서진호
    • 펄프종이기술
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    • 제40권2호
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    • pp.43-56
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    • 2008
  • The purpose of the experiment was to evaluate the material stability of the paper of the annals of Joseon Dynasty for the conservation purpose and the categories were as listed below : 1. Procuring traditional Hanji and semi-Hanji from different regional hanji paper mill. 2. Artificial accelerated aging treatment to examination its stability (UV irradiation, dry heat) 3. Analysis of optical, physical characteristic. The suitable Hanji for categories would be used as a reconstruction material for the waxel paper in the papers of the annals of Joseon Dynasty.

Al-Zn-Mg-Cu-(Sc) 합금의 석출특성 (Precipitation Behavior of Al-Zn-Mg-Cu-(Sc) Alloy)

  • 최갑송;문호정;우기도
    • 열처리공학회지
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    • 제19권5호
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    • pp.257-261
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    • 2006
  • Scandium(Sc) in Al-Zn-Mg-Cu based Al alloy on precipitation phenomenon was compared to a 7001(Al-7.2%Zn-3.2%Mg-1.8%Cu) Al alloy. GP zone and ${\eta}^{\prime}$ phases were the main strengthening phases at low aging temperature under $100^{\circ}C$, but ${\eta}^{\prime}$ and $Al_3Sc$ phases were the main strengthening phases at high aging temperature above $1600^{\circ}C$ in Sc added 7000(Al-7.7%Zn-2.0%Mg-1.9%Cu-0.1%Zr) Al alloy. With the addition of 0.1%Sc in 7000 Al alloy, the activation energy for the GP zone, ${\eta}^{\prime}$ and ${\eta}$ phase decreased compared to the 7001 Al alloy. This result indicates that the Sc accelerated the precipitation for the GP zone, ${\eta}^{\prime}$ and ${\eta}$ phases in 7000 Al alloy. Al-7.7%Zn-2.0%Mg-1.9%Cu-0.1%Zr-0.1 Sc alloy has higher strength than 7001 Al alloy, which has high strength.

Coated Conductor의 특성 및 미세조직에 미치는 고온열처리 영향 (Effects of High Temperature Heat Treatment on the Microstructure and Superconducting Property of HTS Coated Conductor)

  • 도민호;홍계원;이희균
    • Progress in Superconductivity
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    • 제11권1호
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    • pp.1-7
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    • 2009
  • 고온초전도 CC를 다른 산소 분압에서 Ag과 YBCO의 녹는점 보다 낮은 온도에서 열처리시 CC의 특성에 미치는 영향을 실험하였다. 전류의 수송능력과 미세구조는 보호층인 Ag의 존재여부에 다양하게 영향을 미친다. Ag를 제거한 CC를 $850^{\circ}C$의 산소 분위기에서 2시간 동안 열처리 한 시편의 경우 CC의 임계전류의 특성에 영향을 미치지 않았다. 그러나 Ag를 제거하지 않은 CC를 $800^{\circ}C$의 산소 분위기에서 2시간 동안 열처리한 시편의 경우 임계전류가 140 A에서 8 A로 떨어지는 결과를 보였다. 또한, Ag을 제거하지 않은 CC를 1000 ppm 산소 분위기의 $800^{\circ}C$에서 2시간 동안 열처리한 시편의 경우 임계전류 값이 원래 $I_c$ 값의 $70{\sim}80%$의 임계전류 값이 나타났다. SEM 이미지와 XRD 회절 분석 결과 Ni과 Cr 원자들이 표면으로 확산되어 CC의 전류수송 특성에 영향을 미친다.

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저장 전 열처리가 생강의 이화학적 및 관능적 특성에 미치는 영향 (Effects of Heat Pretreatment on the Quality under Storage of Fresh Ginger Rhizomes)

  • 정헌식;이현정;성종환;문광덕
    • 한국식품저장유통학회지
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    • 제16권5호
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    • pp.623-628
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    • 2009
  • 생강의 근경을 열풍(40, 50, $60^{\circ}C$)으로 일정시간(10, 30, 60분) 처리한 후 LDPE 필름(0.04 mm)으로 밀봉 포장하고 $12{\pm}1^{\circ}C$에서 2개월간 저장하면서 포장 내 기체조성과 생강의 품질특성을 조사하였다. 포장 내 산소와 이산화탄소 농도는 열처리 온도가 높고 시간이 길수록 낮고 높은 경향이었다. 발아율은 $40^{\circ}C$ 처리구에서 보다 높았으며, 부패율은 고온 장시간 처리구 일수록 증가하는 경향을 보였다. 육질경도는 열처리 온도가 높아지고 시간이 길어질수록 낮은 수준을 나타내었다. 중량감소율과 가용성 고형분 함량은 열처리 조건의 영향을 받지 않았으며, pH는 고온 장시간 처리구 일수록 다소 높은 수준을 나타내었다. 관능적 외관, 냄새 및 전반적 기호도 등은 열처리 온도가 증가하고 시간이 길어질수록 낮게 평가되었다. 이러한 결과로써, 생강의 포장 전에 $40^{\circ}C$ 이상의 열풍으로 10분 이상 처리는 품질유지에 효과가 없으며, 고온일수록 품질손실을 촉진하는 것으로 판단되었다.