• 대한기계학회:학술대회논문집
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• 대한기계학회 2004년도 춘계학술대회
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• pp.42-47
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• 2004

Metallic glasses are amorphous meta-stable solids and are now being processed in bulk form suitable for structural applications including impact. Bulk metallic glasses have many unique mechanical properties such as high yield strength and fracture toughness, good corrosion and wear resistance that distinguish them from crystalline metals and alloys. However, only a few studies could be found mentioning the dynamic response and damage of metallic glasses under impact or shock loading. In this study, we employed a small explosive detonator for the dynamic indentation on a Zr-based bulk amorphous metal in order to evaluate the damage behavior of bulk amorphous metal under impact loading. These results were compared with those of spherical indentation under quasi-static and impact loading. The interface bonded specimens were adopted to observe the appearances of subsurface damage induced during indentation under different loading conditions.

• 대한기계학회:학술대회논문집
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• 대한기계학회 2003년도 추계학술대회
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• pp.1246-1251
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• 2003

The fracture behaviors of Zr-based bulk amorphous metals(BAMs) having compositions of $Zr_{55}Al_{10}Ni_{5}Cu_{30}$, were investigated under impact loading and quasi-static conditions. For experiments, a newly devised instrumented impact testing apparatus and the subsize Charpy specimens were used. The influences of loading rate and the notch shape on the fracture behavior of the Zr-based BAM were examined. The Zr-based BAMs showed an elastic deformation behavior without any plastic deformation on it before fracture. Most fracture energies were absorbed in the process of the crack initiation. The maximum load and fracture absorbed energy under quasi-static condition were larger than those under impact condition. However, there existed relatively insignificant notch shape effect. Fracture surfaces under impact loading were smoother than those under quasi-static loading. The absorbed fracture energy appeared differently depending on the extent of the vein-like pattern region due to the shear bands developed at the notch tip. It can be found that the fracture energy of the Zr-Al-Ni-Cu alloy is closely related with the development of shear bands during fracture.

• 대한기계학회논문집A
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• 제27권10호
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• pp.1630-1635
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• 2003

The deformation and fracture behaviors of a bulk amorphous metal, Zr-based one (Zr$\_$41.2/Ti$\_$13.8/Cu$\_$12.5/Ni$\_$10/Be$\_$22.5/: Vitreloy), were investigated over a strain rate range (7x10$\^$-4/～4 s$\^$-1/). The uniaxial compression test and the indentation test using 3mm-diameter WC balls were carried out under quasi-static loading conditions. As a result, at the uniaxial compressive state, the fracture stress of the material was very high (～1,700MPa) and the elastic strain limit was about 2%. The fracture strength showed a strain rate independent behavior up to 4 s$\^$-1/. Using indentation tests, the plastic deformation behavior of the Zr-based BAM up to a large strain value of 15% could be achieved, even though it was the deformation under locally constrained condition. The Meyer hardness of the Zr-based BAM measured by static indentation tests was about 5 GPa and it revealed negligible strain hardening behavior. At indented sites, the plastic indentation occurred forming a crater and well-developed multiple shear bands were generated around it along the direction of 45 degree when the indentation load exceeded 7kN. With increasing indentation load, shear bands became dense. The fracture surface of the specimen after uniaxial compressive tests showed vein-like pattern, typical morphology of many BAMs.

• 대한기계학회:학술대회논문집
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• 대한기계학회 2003년도 춘계학술대회
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• pp.101-106
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• 2003

In order to investigate the mechanical behavior of newly developed materials, the evaluation of mechanical properties using small-size specimen is essential. For those purposes, an instrumented impact testing apparatus, which provides the load-displacement curve under impact loading without oscillations, was devised. To develop the test procedure with the setup, the impact behaviors of various kinds of structural materials such as S45C, SCM4, Ti alloys (Ti-6V-4Al) and Zr-based bulk amorphous metal, were investigated through the instrumented Charpy V-notch impact tests. The calibrations of the dynamic load and displacement that was calculated based on the Newton' second law were carried out through the quasi-static load test and the comparison of a directly measured value using a laser displacement meter. Satisfactory results could be obtained. The crack initiation and propagation processes during impact fracture could be well divided on the curve, depending on the intrinsic characteristic of specimen tested; ductile or brittle. The absorbed impact energy in Zr-basd BAM was largely used for crack initiation not for crack propagation process. The fracture surfaces under impact loading showed different feature when compared with the static cases.

• 한국소성가공학회:학술대회논문집
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• 한국소성가공학회 2008년도 춘계학술대회 논문집
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• pp.258-262
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• 2008

Micro forming is a suited technology to manufacture very small metallic parts(several $mm{\sim}{\mu}m$). In this study, the micro forming property was studied, using Al5083 superplastic alloy with micro grain, suitable for the micro forming process and Zr-BMG amorphous with pseudo-superplastic phenomena in the supercooled liquid state. Micro forming experiments under stastic load status showed that distortion by slip and spin of the grain system and slip inside the grain was observed in the Al5083 superplastic alloy. In case of Zr-BMG, because there is no grain, the distribution of the forming property was similar to the load distribution between punch and metal.

• 한국분말재료학회지
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• 제13권5호
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• pp.351-359
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• 2006

Ni based($Ni_{57}Zr_{20}Ti_{18}Si_2Sn_3$) bulk metallic glass(BMG) powders were produced by a gas atomization process, and ductile Cu powders were mixed using a spray drying process. The Ni-based amorphous powder and Cu mixed Ni composite powders were compacted by a spark plasma sintering (SPS) processes into cylindrical shape. The relative density varied with the used SPS mold materials such as graphite, hardened steel and WC-Co hard metal. The relative density increased from 87% to 98% when the sintering temperature increased up to $460^{\circ}C$ in the WC-Co hard metal mold.