• Journal of information and communication convergence engineering
• /
• v.1 no.2
• /
• pp.63-66
• /
• 2003

High $T_c$ superconducting lines will be applied as key materials in the areas of power transmission line; magnetic levitation of vehicle; magnetic separation; magnetic energy storage and marine propulsion. A combination method of electrophoresis deposition and zone-melting for preparation of YBaCuO tape is proposed. The submicron particle powder of YBaCuO made by sol-gel method is used in the electrophoresis process. A 40∼50 ${\mu}\textrm{m}$ thickness of YBaCuO film on Ag plate could be deposited in about three minutes. After deposition the film is rolled and heat treated in order to increase the density and the adhesion of the film to the Ag plate. Silver(Ag) and lead oxide(PbO) were added in the YBaCuO powder in order to reduce its melting point. The YBaCuO coating with controlled Ag and PbO contents was preliminarily zone-melted at about $945^{\circ}C$.

• Journal of Welding and Joining
• /
• v.33 no.3
• /
• pp.54-61
• /
• 2015

In this study, effect of laser power on hardness and microstructure of SKD61 Hot Die steel of which surface was melted and hardened with Yb:YAG disk laser was investigated. Beam speed was fixed at 70 mm/sec and distance between them was 0.8 mm about Laser surface melting. The only thing that was changed laser power. Laser powers were 2.0, 2.4 and 2.8 kW. No defect was found under all conditions. As the laser power increased, the penetration depth were deepened and the bead width was also widened. There was no hardness deviation of fusion zone at same laser power and it was higher than that of heat affected zone. In addition, the more laser power increased, the more hardness in fusion zone decreased. Fusion zone was macroscopically dendrite structure. However, core matric in dendrite was lath martensite of 100 nm size. There were $M_{23}C_6$ of 500 nm and the VC and $Mo_2C$ of a nano meters on boundary of dendrite.

• Journal of the Korean Institute of Telematics and Electronics A
• /
• v.30A no.6
• /
• pp.31-37
• /
• 1993

InSb thin films were fabricated by zone melting recrystallization of In/Sb multilayered thin films prepared by sequential evaporation. Unreacted metal phase or dispersed metal precipitates lowered the electron mobility and the electron mobility increased with development of (111) prefered orientation. Properties of the film could be controlled by changing mzximum temperature and scanning speed, and the electron mobility as high as 12, 000 cm $^2$/Vsec could be obtained under the optimized conditions.

• Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
• /
• 2002.11a
• /
• pp.91-94
• /
• 2002

The conditions of zone-melting method such as a sample travel speed in a furnace, content of Nd422, control of melting temperature, and heat-treatment with/without Ar gas for $NdBa_{2}Cu_{3}O_{7-\delta}$ superconductor was optimized, As a results, a $NdBa_{2}Cu_{3}O_{7-\delta}$ sample with a surface area of $25mm^{2}$ showed a good superconducting properties when its travel speed was 6 mm/h, The improvement of superconductivity added with 10~20 wt% of Nd422 phase increasing pinning effect was also shown. The critical current density, $J_{c}$ was remarkable affected by the condition of heat-treatment temperature of $NdBa_{2}Cu_{3}O_{7-\delta}$superconductor with/without Ar ambient gas.

• Journal of the Korean Institute of Electrical and Electronic Material Engineers
• /
• v.29 no.2
• /
• pp.110-113
• /
• 2016

(YNdSm)-Ba-Cu-O system high Tc composite superconductors were directionally grown by zone melting process, having large temperature gradient, in air atmosphere. Cylindrical green rods of $(YNdSm)_{1.8}Ba_{2.4}Cu_{3.4}O_x$ [(YNS)1.8]composite oxides by CIP (cold isostatic pressing) method using rubber mold were fabricated. The microstructure and superconducting properties were investigated by XRD, TEM and SQUID magnetometer. The size of nonsuperconducting $(YNdSm)_2BaCuO_5$ inclusions of the melt-textured (YNS)1.8 sample with $CeO_2$ additive were remarkably reduced and uniformly distributed within the superconducting (YNS)1.8 matrix. (YNS)1.8 samples, with / without $CeO_2$ additive, showed an onset $T_c{\geq}90K$ and sharp superconducting transition. The critical current density $J_c$ value of the (YNdSm)1.8 superconductor with $CeO_2$ additive were 840 A, $1.2{\times}104A/cm^2$ in 77 K, 0 Tesla by direct current transport method.

• Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
• /
• 2003.05b
• /
• pp.12-15
• /
• 2003

The YBaCuO thick film was deposited by the electrophoresis in the solution with different dimension particles. The morphology of the films deposited from different particles size was compared. The powder made by sol-gel method has the submicron particles, which deposit the most smooth film, and without microcracks after sintering. After sintering of the deposited film, the zone-melting process was carried out in low oxygen partial pressure (100 Pa) and Ag was used as substrate. And the zone-melted YBaCuO was studied by XRD.

• Journal of Welding and Joining
• /
• v.14 no.3
• /
• pp.93-104
• /
• 1996

This study evaluated relative hot cracking susceptibility of commercial aluminum alloy welds, and then suggested possible mechanisms operated in the weld fusion zone and in the heat affected zone based on the observed cracking morphologies, fractography and microstructural features. The fusion zone solidification cracking was found to be mainly due to a microsegregation of Cu, Si, and Mg in grain boundaries, while liquation cracking in the HAZ was by the incipient melting of the segregated grain boundaries and the consitutional liquation of large aging precipitates and intermetallic compounds in the partially melted zone adjacent to the fusion line which experienced a rapid thermal excursion during welding.

• Journal of Welding and Joining
• /
• v.31 no.1
• /
• pp.58-64
• /
• 2013

The following results were obtained, microstructures and tensile properties in arc brazed joints of DP(dual phase) steel using Cu-5.3wt%Sn insert metal was investigated as function of brazing current. 1) The Fusion Zone was composed of ${\alpha}Fe+{\gamma}Cu$ and Cu23Sn2. The reason for the formation of these solid solutions. Despite, Fe & Cu were impossible to solid solution at room temperature. It's melting & reaction to something of insert metal & Base Metal (DP Steel) by Arc. Brazing Process has faster cooling rate then Cast Process, Supersaturated solid solution at room temperature. 2) The increase Hardness of Fusion Zone was directly proportional to the rise of welding current. Because, ${\alpha}Fe+{\gamma}Cu$ phase (higher hardness than the Cu23Sn2.(104.1Hv < 271.9Hv)) Volume fraction was Growth, due to increasing the amount of base metal melting by High current. 3) The results of tensile shear test by Brazing, All specimens happen to fracture in Fusion Zone. On the other hand, when Brazing Current increasing tend to rise tensile load. but it was very small, about 26-30% of the base metal. 4) The result of fracture analysis, The crack initiate at Triple Point for meet to Upper B.M/Under B.M/Fusion Zone. This Crack propagated to Fusion zone. So ruptured by tensile strength. The Reason to in the fusion zone fracture, Fusion zone by Brazing of hardness (strength) was very lower then the base metal (DP steel). In addition the Fusion Zone's thickness in triple point was thin than the base metal's thickness in triple point.

• Economic and Environmental Geology
• /
• v.17 no.2
• /
• pp.109-114
• /
• 1984

The geophysical implications of the observed heat flow in the Korean Peninsula are examined. The Peninsula can be devided into two typical regions of high (Zone 1) and normal heat flows (Zone 2), and anomalous sharp change of heat flow between two zones is noteworthy. Zone 1 (southeastern coast of the Peninsula) to be connected to the East Sea (=Japan Sea) of high heat flow region corresponds with the region of late-Mesozoic to Tertiary igneous activity. With the radioactive elements concentrated in the crust, the observed heat flow in Zone 2 can be almostly explained. While, only a half of the heat flow in Zone 1 is explained. As a possible explanation of high heat flow in Zone 1, partial melting in the lower crust is examined. The temperature of $800-900^{\circ}C$ calculated at the bottom of the crust excludes the possibility of partial melting or magma generation in the crust. Alternatively, a remaining thermal effect of late-Mesozoic to Tertiary igneous activity is considered. However, it appears that the thermal effect already disappeared and that the vertical temperature distribution reached at steady state 30 MY ago (= 10 MY after the igneous activities came to an end). After all, the existence of some other effective heat transfer in Zone 1 is strongly suggested. The high heat flow to be same kind of anomalous one of the East Sea can be recognized as a result of the trench-back-arc thermal flux. The plate subduction in the Japan Trench will generate an induced flow above the slab of the East Sea, a typical back-arc basin, and hence the induced flow will heat the surrounding lithosphere.

• Journal of the Korean Crystal Growth and Crystal Technology
• /
• v.7 no.1
• /
• pp.151-162
• /
• 1997

The suitability of pivalic acid was confirmed as a secondary temperature standard material. Triple-point cells of pivalic acid were obtained by using combined process of vacuum distillation with zone refining. A detailed description of the purification process was given. The melting curves were used as criteria for determination of purities of pivalic acid. Triple points of these cells with purity of 99.9997% were measured to be $35.956\pm 0.003^{\circ}C$ by using the melting plateau curves. Thus the triple point cells of pivalic acid appear to be able to use for the calibration of thermistor thermometers with moderate precision.