• 대한치과보철학회지
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• 제26권1호
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• pp.23-30
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• 1988

An in vitro study was performed to compare the retentive value of cast post cemented with three commonly used cements and one composite resin. Twenty cast posts were made from twenty extracted lower premolars. The samples were randomly divided into four groups. The first group was cemented with zinc phosphate cement, the second group with polycarboxylate cement, the third group with glass-ionomer cement, and the fourth group with composite resin. The tensile load test was performed on an Instron testing machine with crosshead speed of 2 mm/min and the results were compared statistically. The results were as follows ; 1. The mean value of tensile break force of cemented cast post was 23.36Kg in case of zinc phosphate cement, 16.28Kg in case of polycarboxylate cement, 22.09Kg in case of glass-ionomer cement , and 26.88Kg in case of composite resin. 2. Retention was not significantly different among zinc phosphate cement, glass-ionomer cement and composite resin. 3. Polycarboxylate cement was found to be less retentive than zinc phosphate cement, glass-ionomer cement , and composite resin.

• Restorative Dentistry and Endodontics
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• 제13권2호
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• pp.307-322
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• 1988

The purpose of this study is to evaluate the pulpal responses to the base materials such as zinc oxide eugenol cement, calcium hydroxide, zinc phosphate cement, polycarboxylate cement and glass ionomer cement. The 100 caries free dog teeth were devided into 2 groups by remaining dentin thickness (Group A: 0.4-0.6 mm, Group B: 0.8-1.0 mm) and each group were devided into 5 subgroups. The intervals of observation period are 3days, 1 week, 2 weeks, 4 weeks and 8 weeks respectively after experiment. The specimens were fixed with 10% formalin and decalcifed in 5% nitric acid. All specimens were stained with Hematoxylin-Eosin and examined histopathologically. The results were as follows. 1. In group A, atropy or hyperplasia in odontoblasts were seen in zinc oxide eugenol cement, calcium hydroxide and zinc phosphate cement. No changes in odontoblasts were seen in polycarboxylate cement and glass ionomer cement. 2. In group A, increase of predentin were seen in all experimental materials. 3. In group A, vascular congestion were seen in all experimental materials and inflammation were seen on 3 days in zinc oxide eugenol cement, 8 weeks in zinc phosphate cement and hemorrage were seen on 3 days in zinc phosphate cement. 4. In group B, changes of odontoblasts were not seen all experimental materials. 5. In group B, increase of predentin and vascular congestion were seen in all experimental materials but inflammation were not seen.

• Restorative Dentistry and Endodontics
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• 제18권2호
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• pp.507-513
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• 1993

본 연구의 목적은 3종의 일반적 glass ionomer cement과 1종의 광중합형 glass ionomer cement을 자료로 하여 연화후 3, 5, 7, 10분 경과시켜 methylene blue용액에 침적하여 그침투를 측정하여 물의 영향을 관찰하고 이상의 시간과 관련하여 수분과 접촉시 그 용해도를 zinc phosphate와 polycarboxylate cement와 비교관찰하였다. blue stained zone은 모든 glass ionomer cement에서 나타났고 inner opaque zone은 두종의 regular glass ionomer cement에서만 나타났다. 연화시작부터 물에 침적시키는 사이시간이 연장되매 따라 모든 cement에서 두 zone의 후경이 감소하였고 regular glass ionomer cement의 면으로 부터 물질의 손실량은 현저히 감소하였으며 물질의 손실량에 대해서는 light curing glass ionomer cement는 시간에 거의 영향을 받지 않았으며 zinc phosphate cement파 polycarboxylate cement도 이와 유사성을 보였다.

• 한국결정성장학회지
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• 제17권3호
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• pp.102-107
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• 2007

인산염계 유리를 사용하여 PDP 소자의 하판유전체 후막을 제작하였다. 유전체 후막의 제조는 soda-lime glass위에 silk screen printing 법을 사용하였다. 기판과 유전체후막의 열팽창계수를 맞추기 위하여 $TiO_2$와 $Al_2O_3$를 충진제로 사용하였다. 유전체의 결정화 거동은 DTA, XRD를 사용하였으며 광학적 열적 전기적인 특성을 알아보기 위하여 UV-spectrometer, Dilatometer, Impedance Analyser를 사용하였다. 실험결과 주 결정상은 메타인산아연과 피로인산아연으로 나타났다. $TiO_2$의 첨가로 인하여 반사율은 높아졌으나 상대적으로 유전상수는 높아졌다. 또한 $Al_2O_3$를 첨가한 경우 반사율은 크게 변화가 없었으나 유전상수 값은 낮아졌다. 또한 열팽창 계수는 약 $62{\times}10^{-7}/^{\circ}C$ 정도였다.

• 대한치과교정학회지
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• 제11권2호
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• pp.151-160
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• 1981

The purpose of this study was to compare the retentive values of various dental cements used for cementing the orthodontic bands on the teeth. Sound freshly extracted human premolar teeth were selected for the study. Eleven commercial dental cements (Zinc phosphate, reinforced Zinc-oxide eugenol, Carboxylate and Glass ionomer cements) were handled under standardized conditions. All cemented speciments were then kept in a thermostatic humidor cabinet regulated at $23{\pm}2^{\circ}C$ and more than $95\%$ relative humidity and tested after 24 hours and 1 week each. The force required to remove the cemented orthodontic bands from the teeth was determined on an Instron Universal Testing Machine using a modified specimen holding device with a cross-head speed of 0.20mm/min. The results obtained were as follows: 1, The retentive values of the band cemented with zinc phosphate cements and carboxylate cements were considerably higher than those of the reinforced zinc oxide-eugenol and glass ionomer cements. 2. There was no significant difference between the retentive value of carboxylate cements as compared with zinc phosphate cements. 3. The retentive value of the reinforced zinc oxide eugenol cements was lowest all of the coements. The retentive values expressed for all cements up to at least one week were highly but no significant difference was found between the 24-hour and 7 day time intervals.

• 대한치과보철학회지
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• 제20권1호
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• pp.25-32
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• 1982

An in vitro study was conducted to compare the bond strength of cements between Verabond coping and various cores. Fifty-four idential cores simulating maxillary central incisor prepared for PFM crowns were made. Eighteen samples were made with 20K cast gold, eighteen with Verabond, and eighteen with Adaptic. Samples were randomly divided into three groups, each consisting of six 20K cast gold, six verabond, and six Adaptic samples. The first group was cemented with zinc phosphate cement, the second group with poly-carboxylate cement, and the third group with glass ionomer cement. Constant finger pressure was applied for cementation. The sample were then stored at $37^{\circ}C$ in distilled water bath for 24 hours. The tensile strength test was performed on an Instron Universal test machine with crosshead speed of 0.05cm/min and the results compared statistically. Results of the study showed that: 1. A significant difference of bond strength was observed with different types of dental cements and core materials. 2. With gold core, zinc phosphate cement was stronger than both the polycarboxylate cement and glass ionomer cement, which did not differ in bond strength. 3. With base-metal core, zinc phosphate cement showed the highest bond strength and was followed by polycarboxylate cement and glass ionomer cement. 4. With composite resin core, zinc phosphate cement showed the highest bond strength and was followed by glass ionomer cement and polycarboxylate cement. 5. The base-metal core (Verabond core) privided the highest retention of all core materials.

• The Journal of Advanced Prosthodontics
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• 제8권6호
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• pp.449-456
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• 2016

PURPOSE. This in vitro study evaluated the effects of four different cements on the color attributes of a zirconia ceramic. MATERIALS AND METHODS. 40 zirconia ceramic disk specimens (0.5 mm thickness, 10 mm diameter, 0.1 mm cement space) were fabricated by a computer-aided design and computer-aided manufacturing system. The specimens were divided into 4 groups of 10 specimens and cemented to composite substrates using four different cements including: Glass Ionomer, Panavia F2.0, Zinc Phosphate, and TempBond. The $L^*$, $a^*$, and $b^*$ color attributes of the specimens were measured before and after cementation by a spectrophotometer. Additionally, ${\Delta}E$ values were measured to determine color changes for the groups and then compared with the perceptional threshold of ${\Delta}E=3.3$. Repeated Measures ANOVA, Tukey Post Hoc, Bonferroni, One-way ANOVA, and One-sample t-test tests were used to analyze the data. All tests were carried out at the 0.05 level of significance. RESULTS. Statistically significant differences were detected in the ${\Delta}E$ values for Zinc Phosphate (P<.0001) and TempBond (P<.0001) groups. However, there were no statistically significant differences in this respect for Glass Ionomer (P=.99) and Panavia F2.0 (P=1) groups. The means and standard deviations of the ${\Delta}E$ values for Glass Ionomer, Panavia F2.0, Zinc Phosphate, and Tempbond groups were $2.11{\pm}0.66$, $0.94{\pm}0.39$, $5.77{\pm}0.83$, and $7.50{\pm}1.16$ Unit, respectively. CONCLUSION. Within the limitations of this study, it was concluded that Zinc Phosphate and Tempbond cements affected the color attributes of the tested zirconia ceramic beyond the perceptional threshold. However, Glass Ionomer and Panavia F2.0 cements created acceptable color changes.

• 대한치과의사협회지
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• 제10권8호
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• pp.531-534
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• 1972

The author measured exothermic temperature of the 5 kinds of zinc phosphate cement and 3 kinds of copper phosphate cement during setting process. Cements were mixed on the glass slab with flexible steel spatula at room temperature (25.8℃) for one minute (spatulating speed was 100 strokes per minute) and placed in the incubator of which temperature was held at 37℃ and thermometer was inserted into the cement mass. The powder liquid ration was 3.0gm:1ml and 1.5gm:1ml. The results were as follows. 1) The heat generated after mixing these cements was under 47.22℃. 2) The range of thermal change of the zinc phosphate cements during setting process was wider than copper phosphate cements. 3) The exothermic temperature from the thin mix was higher than thick mix. 4) The exothermic temperature of the zinc phosphate cements was higher than copper phosphate cements.

• 한국세라믹학회지
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• 제37권9호
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• pp.900-908
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• 2000

일반적인 유리용융과 열처리법을 이용하여 많은 양의 금속구리 미립자가 분산된 Zinc Phosphate 유리를 제조하였다. 금속산화물로는 Cu$_2$O를, 환원제로는 SnO를 사용하였다. XRD와 전자회절로부터 열처리에 의해 금속구리의 결정상이 석출됨을 알 수 있었고, TEM에 의해 석출상의 크기는 수~20nm 정도임을 알 수 있었다. 또한 570nm에서의 광흡수 피크로부터도 금속구리의 석출을 확인할 수 있었다. 석출입자의 크기와 흡광은 석출을 위한 열처리 온도와 시간이 증가함에 따라 증가하였다. XPS 스펙트럼으로는 구리의 산화상태 중 Cu$^{2+}$ 이온의 상태만을 분명히 할 수 있었다. 매질유리의 BO/NBO의 비는 열처리 전후 크게 변화가 없었으며, 열처리 후 Cu$^{2+}$ 이온이 다소 감소되는 경향을 보였다.

• 대한치과보철학회지
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• 제38권5호
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• pp.618-630
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• 2000

As Fiber-reinforced composite restorations cannot be made without leaving a marginal gap, luting cements play a pivotal role in sealing the margins as a prevention against margnal leakage. A recently introduced adhesive resin cement system is claimed to adhere chemically, as well as mechanically, to tooth substances, dental alloys and porcelain. But when considering the clinical variation conventional cementation using Zinc Phosphate and Glass-Ionomer can be requested. A vitro study was undertaken to compare microleakage and marginal fitness of Fiber-reinforced composite crowns(Targis/Vectris) depending upon luting cements. Fifty non-carious human premolar teeth were randomly divided into five experimental groups of 10 teeth each and luted with five luting cements. ($Bistite\;II^(R),\;Super-bond^(R),\;Variolink\;II^(R)$), Zinc phosphate and Glass-Ionomer cement) After 24 hours of being luted, all specimens were thermocycled 300 times through water bath of $5^{\circ}C\;and\;55^{\circ}C$ in each bath, then the quality of the marginal fitness was measured by the Digital Microscope and marginal leakage was characterized using Dye Penetration technique and the Digital Microscope The results were as follows : 1. The mean values of marginal fit were Bistite II($46.78{\mu}m$), Variolink II($56.25{\mu}m$), Super-Bond($56.78{\mu}m$), Glass-Ionomer($99.21{\mu}m$), Zinc Phosphate($109.49{\mu}m$) indicated a statistically significant difference at p<0.001. 2. The mean microleakage values of tooth-cement interface, restoration-cement interface were increased in the order of Variolink II, Bistite II, Super-Bond, Glass-Ionomer, Zinc Phosphate 3. Crowns luted with resin cement (Bistite II, Super-Bond, Variolink II, etc) exhibited less marginal gap and marginal leakage than those luted with conventional Glass-Ionomer and Zinc Phosphate cement. 4. The results indicated that all five luting systems yielded comparable and acceptable marginal fit.