• Title/Summary/Keyword: Z.-M. 방법

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SURFACE ROUGHNESS OF EXPERIMENTAL COMPOSITE RESINS USING CONFOCAL LASER SCANNING MICROSCOPE (공초점 레이저 주사 현미경을 이용한 실험적 레진의 표면 조도에 대한 연구)

  • Bae, J.H.;Lee, M.A.;Cho, B.H.
    • Restorative Dentistry and Endodontics
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    • v.33 no.1
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    • pp.1-8
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    • 2008
  • The purpose of this study was to evaluate the effect of a new resin monomer, filler size and polishing technique on the surface roughness of composite resin restorations using confocal laser scanning microscopy. By adding new methoxylated Bis-GMA (Bis-M-GMA, 2,2-bis[4-(2-methoxy-3-methacryloyloxy propoxy) phenyl] propane) having low viscosity, the content of TEGDMA might be decreased. Three experimental composite resins were made: EX1 (Bis-M-GMA/TEGDMA = 95/5 wt%, 40 nm nanofillers); EX2 (Bis-M-GMA/TEGDMA = 95/5 wt%, 20 nm nanofillers); EX3 (Bis-GMA/TEGDMA = 70/30 wt%, 40 nm nanofillers). Filtek Z250 was used as a reference. Nine specimens (6 mm in diameter and 2 mm in thickness) for each experimental composite resin and Filtek Z250 were fabricated in a teflon mold and assigned to three groups. In Mylar strip group, specimens were left undisturbed. In Sof-lex group, specimens were ground with #1000 SiC paper and polished with Sof-lex discs. In DiaPolisher group, specimens were ground with #1000 SiC paper and polished with DiaPolisher polishing points. The Ra (Average roughness), Rq (Root mean square roughness), Rv (Valley roughness), Rp (Peak roughness), Rc (2D roughness) and Sc (3D roughness) values were determined using confocal laser scanning microscopy. The data were statistically analyzed by Two-way ANOVA and Tukey multiple comparisons test (p = 0.05). The type of composite resin and polishing technique significantly affected the surface roughness of the composite resin restorations (p < 0.001). EX3 showed the smoothest surface compared to the other composite resins (p < 0.05). Mylar strip resulted in smoother surface than other polishing techniques (p < 0.05). Bis-M-GMA. a new resin monomer having low viscosity, might reduce the amount of diluent, but showed adverse effect on the surface roughness of composite resin restorations.

Characterization of Kraft Lignin by 13C-Nuclear Magnetic Resonance Spectroscopy (13C-NMR에 의한 크라프트 리그닌의 특성)

  • Lee, Beom-Goo;Hwang, Byung-Ho
    • Journal of the Korean Wood Science and Technology
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    • v.17 no.4
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    • pp.44-56
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    • 1989
  • To recover much residual lignin from the black liquor of kraft pulp. the black liquor was extracted and purified with many organic solvents. Many kinds of lignins were isolated from each fraction obtained and the characteristics of these lignins investigated by $^{13}C$-NMR spectroscopy. If M$\ddot{o}$rck's method was compared with Kirk's method. M$\ddot{o}$rck's method was better than Kirk's method because the particular signals of each lignin occur more in the former than m the latter. Especially the $^{13}C$-NMR spectrum of the MCS fraction identifies with those of other researchers. The experiment that the kraft lignin from Pinus densiflora S. et Z. found in Korea was investigated by $^{13}C$-NMR spectroscopy was performed first in Korea.

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Consideration of Normal Variation of Perfusion Measurements in the Quantitative Analysis of Myocardial Perfusion SPECT: Usefulness in Assessment of Viable Myocardium (심근관류 SPECT의 정량적 분석에서 관류정량값 정상변이의 고려: 생존심근 평가에서의 유용성)

  • Paeng, Jin-Chul;Lim, Il-Han;Kim, Ki-Bong;Lee, Dong-Soo
    • Nuclear Medicine and Molecular Imaging
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    • v.42 no.4
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    • pp.285-291
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    • 2008
  • Purpose: Although automatic quantification software of myocardial perfusion SPECT provides highly objective and reproducible quantitative measurements, there is still some limitation in the direct use of quantitative measurements. In this study we derived parameters using normal variation of perfusion measurements, and tried to test the usefulness of these parameters. Materials and Methods: In order to calculate normal variation of perfusion measurements on myocardial perfusion SPECT, 55 patients (M:F = 28:27) of low-likelihood for coronary artery disease were enrolled and $^{201}TI$ rest/$^{99m}Tc$-MIBI stress SPECT studies were performed. Using 20-segment model, mean (m) and standard deviation (SD) of perfusion were calculated in each segment. As a myocardial viability assessment group, another 48 patients with known coronary artery disease, who underwent coronary artery bypass graft surgery (CABG) were enrolled. $^{201}TI$ rest/$^{99m}Tc$-MIBI stress / $^{201}TI$ 24-hr delayed SPECT was performed before CABG and SPECT was followed up 3 months after CABG. From the preoperative 24-hr delayed SPECT, $Q_{delay}$ (perfusion measurement), ${\Delta}_{delay}$ ($Q_{delay}$ - m) and $Z_{delay}$ (($Q_{delay}$ - m)/SD) were defined and diagnostic performances of them for myocardial viability were evaluated using area under curve (AUC) on receiver operating characteristic (ROC) curve analysis. Results: Segmental perfusion measurements showed considerable normal variations among segments. In men, the lowest segmental perfusion measurement was $51.8{\pm}6.5$ and the highest segmental perfusion was $87.0{\pm}5.9$, and they are $58.7{\pm}8.1$ and $87.3{\pm}6.0$, respectively in women. In the viability assessment $Q_{delay}$ showed AUC of 0.633, while those for ${\Delta}_{delay}$ and $Z_{delay}$ were 0.735 and 0.716, respectively. The AUCs of ${\Delta}_{delay}$ and $Z_{delay}$ were significantly higher than that of $Q_{delay}$ (p = 0.001 and 0.018, respectively). The diagnostic performance of ${\Delta}_{delay}$, which showed highest AUC, was 85% of sensitivity and 53% of specificity at the optimal cutoff of -24.7. Conclusion: On automatic quantification of myocardial perfusion SPECT, the normal variation of perfusion measurements were considerable among segments. In the viability assessment, the parameters considering normal variation showed better diagnostic performance than the direct perfusion measurement. This study suggests that consideration of normal variation is important in the analysis of measurements on quantitative myocardial perfusion SPECT.

A case study for the dispersion parameter modification of the Gaussian plume model using linear programming (Linear Programming을 이용한 가우시안 모형의 확산인자 수정에 관한 사례연구)

  • Jeong, Hyo-Joon;Kim, Eun-Han;Suh, Kyung-Suk;Hwang, Won-Tae;Han, Moon-Hee
    • Journal of Radiation Protection and Research
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    • v.28 no.4
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    • pp.311-319
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    • 2003
  • We developed a grid-based Gaussian plume model to evaluate tracer release data measured at Young Gwang nuclear site in 1996. Downwind distance was divided into every 10m from 0.1km to 20km, and crosswind distance was divided into every 10m centering released point from -5km to 5km. We determined dispersion factors, ${\sigma}_y\;and\;{\sigma}_z$ using Pasquill-Gifford method computed by atmospheric stability. Forecasting ability of the grid-based Gaussian plume model was better at the 3km away from the source than 8km. We confirmed that dispersion band must be modified if receptor is far away from the source, otherwise P-G method is not appropriate to compute diffusion distance and diffusion strength in case of growing distance. So, we developed an empirical equation using linear programming. An objective function was designed to minimize sum of the absolute value between observed and computed values. As a result of application of the modified dispersion equation, prediction ability was improved rather than P-G method.

A study on the derivatization technique for tamoxifen metabolites in human urine by gas chromatography/mass spectrometry (기체크로마토그래피/질량분석기를 이용한 인체 내 뇨시료에서의 Tamoxifen 대사체 검출을 위한 유도체화 연구)

  • Kim, Yunje;Lee, Yoonjung
    • Analytical Science and Technology
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    • v.17 no.4
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    • pp.322-336
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    • 2004
  • The improved derivatization technique of tamoxifen metabolite in human urine is described for the acylation method that they are substituted by derivatization reagent like acyl anhydride for use of gas chromatography/mass spectrometry. The hydroxyl group of tamoxifen metabolite was derivatized by trifluoroacetic anhydride (TFAA), pentafluoroacetic anhydride (PFPA) and heptaflorobutylic anhydride (HFBA). It was investigated to the gas chromatography/mass spectrometry (GC/MS) technique use negative ion chemical ionization (NCI), positive ion chemical ionization (PCI) and electron impact (EI). In acylation of the metabolites of tamoxifen, the effective reaction temperature and time were shown to be at $50^{\circ}C$ for 30 min. The 4-hydroxytamoxifen, which is known to major metabolite of tamoxifen, was not detected in human urine, whileas the hydroxymethoxytamoxifen was detected. We thought that this result was from the single dose of tamoxifen.

A New Class of Self-Shrinking Generators (새로운 자기 수축 발생기)

  • 최세아;양경철
    • Proceedings of the Korea Institutes of Information Security and Cryptology Conference
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    • 2002.11a
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    • pp.88-91
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    • 2002
  • 자기 수축 발생기(self-shrinking generator)는 Meier와 Staffelbach에 의해 제안되었으며[4], 구조가 간단하고 키수열을 생성하는 속도가 빠르기 때문에 스트림 암호시스템으로 각광받고 있다 [5]. 본 논문에서는 자기 수축 발생기의 새로운 구성방법을 제안한다. 제안된 자기 수축 발생기는 하나의 선형귀환회로와 주어진 짝수 m에 의하여 정의되며 일반적으로 선형귀환회로의 귀환다항식으로 원시다항식을 사용한다. 이 경우 키수열은 균형성을 만족하며, 선형귀환회로의 귀환다항식의 차수를 $d_{Y}$ 라고 하면 주기는 $d_{Y-2}$ 이다. m을 $2^{η}$ζ로 표현하면 선형복잡도 Lz는 $d_{Y}$ +η-3/$\leq$ $L_{Z}$ $\leq$m/2($d_{Y}$ -1 - ($d_{Y}$ -2))이다. 따라서 제안된 자기 수축 발생기는 기존의 자기 수축 발생기에 비하여 암호학적으로 우수한 성질을 갖는다.다.

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Accuracy Analysis of Cadastral Control Point and Parcel Boundary Point by Flight Altitude Using UAV (UAV를 활용한 비행고도별 지적기준점 및 필지경계점 정확도 분석)

  • Kim, Jung Hoon;Kim, Jun Hyun
    • Journal of the Korean Society of Surveying, Geodesy, Photogrammetry and Cartography
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    • v.36 no.4
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    • pp.223-233
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    • 2018
  • In this study was classified the cadastral control points and parcel boundary points into 40m, 100m by flight altitude of UAV (Unmanned Aerial Vehicle) which compared the coordinates extracted from the orthophoto with the parcel boundary point coordinates by GNSS (Global Navigation Satellite System) ground survey. As a results of this study, first, in the spatial resolution analysis that the average error of the orthoimage by flight altitude were 0.024m at 40m, and 0.034m at 100m which were higher 40m than 100m for spatial resolution of orthophotos and position accuracy. Second, in order to analyze the accuracy of image recognition by airmark of flight altitude that was divided into three cases of nothing, green, and red of RMSE (Root Mean Square Error) were X=0.039m, Y=0.019m and Z=0.055m, the highest accuracy. Third, the result of the comparison between orthophotos and field survey results that showed the total RMSE error of the cadastral control points were X=0.029m, Y=0.028m, H=0.051m, and the parcel boundary points were X=0.041m, Y=0.030m. In conclusion, based on the results of this study, it is expected that if the average error of flight altitude is limited to less than 0.05m in the legal regulations related to orthophotos for cadastral surveying, it will be an economical and efficient method for cadastral survey as well as spatial information acquisition.

Photochromic Lens development to use Nano particle (1) - Photochromic Lens' estimation method and application - (Nano 입자를 이용한 Photochromic Lens 개발(1) - Photochromic Lens의 평가방법 및 적용 -)

  • Kim, Yong Geun;Seong, Jeong Sub
    • Journal of Korean Ophthalmic Optics Society
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    • v.7 no.2
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    • pp.169-174
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    • 2002
  • Make Photochromic lens Photochromism estimation method, and gouge photochromic lens and investigated UV light source to apply. UV light source irradiation ago and after wavelength dependence of photo-transmittance (T%) of darkening and fading state by do optical equipment which is consisted of spectrophotometer, light source, power meter and detecter. Use relative ratio value of maximum $T%{\times}{\lambda}$ area and saturated state area in light off. Dependences estimation introduced darkening efficiency $(K_d)=(1-C_1/A_1)/t_{on}$ relationship value course fading efficiency$(K_f)=(C_2/A_2)/t_{on}$ value during Photochromism's irradiation time in Photochromic lens. Wavelength dependence of transmittance (T%) has form of $T_m+T_1{\exp}[-(x_0-t)/a]$ in Darkening course fading state. Can receive each estimation parameter value as result that apply Photochromism's estimation parameter Z, $K_d$, $K_f$ in Photochromic lens.

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The Viticetea rotundifoliae in South Korea and Japan (한국과 일본의 순비기나무군강)

  • Jung, Yong-Kyoo
    • The Korean Journal of Ecology
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    • v.23 no.5
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    • pp.383-389
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    • 2000
  • A comparative analysis on the Viticetea rotundifoliae (coastal dune shrub vegetation) in South Korea and Japan was carried out. 569 releves from the most typical and homogeneous stands of the coastal dunes in South Korea and Japan were used. This study was accomplished by using the syntaxa and hierarchical system of the Viticetea rotundifoliae in South Korea and Japan according to the Zurich-Montpellier School's method, and syntaxonomy, synecology, syndynamics and syngeography between two countries were also compared with. Coastal dune shrub vegetation in South Korea and Japan were defined to the Viticetea rotundifoliae representing southern type coastal shrub in Northeast Asia. Coastal dune shrub communities of the Viticetea rotundifoliae in South Korea and Japan are considerably corresponded between the two, and contain their own characteristic syntaxa. Coastal dune shrub communities of the Viticetea rotundifoliae in Japan showed much diversification in syntaxa and species composition than those in South Korea.

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Habitat and Phytosociological Characters of Ceratopteris thalictroides, Endangered Plant Species on Paddy Field, in Nakdong River (논 잡초 멸종위기식물인 물고사리의 낙동강유역 자생지 최초보고 및 군락분류)

  • Choi, Byoung-Ki;Lee, Chang-Woo;Huh, Man-Kyu
    • Weed & Turfgrass Science
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    • v.3 no.1
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    • pp.50-55
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    • 2014
  • This study is aimed at classifying the syntaxa of Ceratopteris thalictroides dominant community on the Nakdong River, and to collect basic data for research of habitat. The communities were carried out by using the Z.-M. School's method and numerical classification technique. The result of syntaxa was classified three communities such as Persicaria japonica-Ceratopteris thalictroides community, Lindernia procumbens-Ceratropteris thalictroides community, and Limnophila indica-Ceratopteris thalictroides community. The ordination analysis displayed the vegetation types with respect to complex environmental gradients. After ordination and clustering analysis, the effective humidity, soil stability, trampling effects, anthropogenic effects and flooding frequency were identified as the important factors deciding the vegetation pattern. It was pointed out to establish a long-term ecological site for protecting such vulnerable vegetation against overexploitation and global climate change.