• Title/Summary/Keyword: Z.-M. 방법

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Effect of Various Surface Treatment Methods on Shear Bond Strength of Orthodontic Brackets to Aged Composite Resin (시효된 복합레진 표면에 다양한 표면 처리 후 부착한 교정용 브라켓의 전단응력)

  • Park, Jongcheol;Park, Howon;Lee, Juhyun;Seo, Hyunwoo
    • Journal of the korean academy of Pediatric Dentistry
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    • v.41 no.2
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    • pp.125-133
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    • 2014
  • The purpose of this study was to investigate the effect of various surface treatment methods on the shear bond strength of orthodontic brackets in vitro. Ninety six specimens, 6 mm in diameter and 5 mm in height, were made with composite resin ($Filtek^{TM}$ Z350 XT, 3M ESPE, USA) and treated with an aging procedure. After aging, the specimens were randomly separated in six groups: (1) control with no surface treatment, (2) 37% phosphoric acid gel, (3) 4% hydrofluoric acid gel, (4) sodium bicarbonate particle abrasion, (5) diamond bur, and (6) 1 W carbon dioxide laser for 5s. The metal brackets were bonded to composite surfaces by means of an orthodontic adhesive (Transbond XT, 3M Unitek, USA). Shear bond strength values were evaluated with a universal testing machine (R&B Inc., Korea). Analysis of variance showed a significant difference between the groups. Group 5 had the highest mean shear bond strength (11.9 MPa), followed by group 6 (11.1 MPa). Among the experimental groups, group 2 resulted in the weakest mean shear bond strength (5.22 MPa). The results of this study suggest that the repair shear bond strength of the aged composite resin was acceptable by surface treatment with a carbon dioxide laser.

Eine methodologische Untersuchung der koreanisch-deutschen ILI-Verbindung zur Anwendung der auf dem EuroNet basierten lexikalisch-semantischen Datenbasis (유로워드넷 기반의 어휘 데이터베이스 활용을 위한 한국어-독일어 ILI 대응 방법론 연구)

  • Oh Jang-Geun
    • Koreanishche Zeitschrift fur Deutsche Sprachwissenschaft
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    • v.6
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    • pp.323-344
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    • 2002
  • EuroNet ist eine multilinguale Datenbasis mit WordNets $f\"{u}r\;einige\;europ\"{a}ische$ Sprachen ($holl\"{a}ndisch$, italienisch, spanisch, deutsch, $franz\"{o}sisch$, tschechisch und estnisch). Die WordNets werden genauso wie das amerikanische WordNet $f\"{u}r$ Englisch (Princeton WordNet, Miller et al. 1990) in Synsets (Zusammensetzen der synonymen $W\"{o}rter$) mit grundlegenden lexikalisch-semantischen Relationen zwischen ihnen $ausgedr\"{u}ckt$ strukturiert. Jedes WordNet stellt also ein einzigartiges innersprachliches System $f\"{u}r$ die lexikalischen und konzeptuellen Relationen dar. $Zus\"{a}tzlich$ werden diese auf dem Princeton WordNet basierten WordNets (z.B. GermaNet) mit einem Inter-Linguale-Index (kurz, ILI) verbunden. $\"{U}ber$ diesem Index werden die Sprachen zusammengeschaltet, damit zu gehen ist $m\"{o}glich$, von den $W\"{o}rtern$ in einer Sprache zu den $\"{a}hnlichen\;W\"{o}rtern$ in jeder $m\"{o}glicher$ anderen Sprache. Der Index gibt auch Zugang zu einer geteilten Top-Ontologie von 63 semantischen Unterscheidungen. Diese Top-Ontologie stellt einen allgemeinen semantischen Rahmen $f\"{u}r$ aile Sprachen zur $Verf\"{u}gung,\;w\"{a}hrend$ sprachspezifische Eigenschaften in den einzelnen WordNets beibehalten werden. Die Datenbasis kann, unter anderen, $f\"{u}r$ einsprachige und multilinguale Informationsretrieval benutzt werden. In der vorliegenden Arbeit handelt sich also um eine methodologische Untersuchung der koreanisch-deutschen ILI-Verbindung zur Anwendung der auf dem EuroNet basierten lexikalischen, semantischen Datenbasis. Dabei werden einzelnen Lexeme in koreanischen, deutschen WordNets $zun\"{a}chst$ mit Hilfe der Sense-Analyse semantisch differenziert, und dann durch lexikalische und konzeptuelle Relationen(ILI) miteinander verbunden. Die Equivalezverbindungen dienen, sprachspezifische Konzepte zum ILI abzubilden. Sie werden von einem anderen Synset der moglichen Relationen aus der Euronet-Spezifikation genommen. Wenn es keinen ILI-Rekord gibt, der ein direktes Equivalenz zu einem gegebenen Konzept darstellt, kann das Konzept in der Frage $\"{u}ber$ EQ-Near-Synonymie, EQ-Hyperonymie oder EQ-Hyponymie Relationen verbunden werden.

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Analysis of Amineptine and its Metabolites in Human Urine by Gas Chromatography/Mass Spectrometry (Gas Chromatography/Mass Spectrometry를 이용한 뇨중 Amineptine과 그 대사체 분석방법에 관한 연구)

  • Lee, Jeong Ae;Kim, Younglim;Lho, Dong-Seok
    • Analytical Science and Technology
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    • v.13 no.3
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    • pp.385-393
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    • 2000
  • A gas chromatography-mass spectrometric (GC/MS) procedure for the determination of amineptine (dihydro-10, 11-dibenzo[a, d] cycloheptenyl-5-amino-7-heptanoic acid) and its main metabolites in human urine was described. Amineptine has been known to be extensively metabolized by the ${\beta}$-oxidation of the heptanoic side chain with formation of pentanoic side chain metabolite ($C_5$-metabolite), and lactamizarion by internal dehydration of (${\beta}$-oxidized metabolite (${\delta}$-lactam). The detection of these compounds was based on acid hydrolysis, liquid-liquid extraction and trimethylsilylated derivatization of the carboxylic acid group. For the determination of amineptine and its metabolites in biological fluids, selected ions at the m/ 192, molecular ion and one of the characteristic ions were monitored by GC/MS. On the excretion study of amineptine in human urine, 70-90% of amineptine, ${\delta}$-lactam, and $C_5$-metabolite were found to be excreted within 4 hours and their excretion completed within 20 hours.

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Antarctic DEMs Generation Using KOMPSAT-3A Stereo Images and Comparison by DEM Matching (KOMPSAT-3A 입체영상을 이용한 남극 DEM 제작과 DEM 매칭에 의한 두 시기의 DEM 비교)

  • Lee, Hyoseong;Hwang, Hobin;Seo, Doochun;Ahn, Kiweon
    • Journal of the Korean Society of Surveying, Geodesy, Photogrammetry and Cartography
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    • v.35 no.3
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    • pp.167-174
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    • 2017
  • Antarctica, where ice sheet has been declined rapidly, should be monitored periodically. However, there are difficult to access for local survey or aircraft observation due to the vast and extreme environments of the polar regions. In order to overcome this problem, there have been a lot of studies by acquiring radar or laser data by satellite. It is also difficult to accurately measure the changes of the surface where is composed of snow or ice layer, and it is also difficult to product a high-resolution DEM. This study therefore aims to product DEMs of two periods using high-resolution KOMPSAT-3A stereo images, and DEM matching is implemented by the LZD(Least-squares Z-Differences) method to detect DEM changes in both periods. As a result, the proposed method could be suggested as comparing height differences of the two DEMs within 1m precision.

A Search for Red Phosphors Using Genetic Algorithm and Combinatorial Chemistry (유전알고리즘과 조합화학을 이용한 형광체 개발)

  • 이재문;유정곤;박덕현;손기선
    • Journal of the Korean Ceramic Society
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    • v.40 no.12
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    • pp.1170-1176
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    • 2003
  • We developed an evolutionary optimization process involving a genetic algorithm and combinatorial chemistry (combi-chem), which was tailored exclusively for tile development of LED phosphors with a high luminescent efficiency, when excited by soft ultra violet irradiation. The ultimate goal of our study was to develop oxide red phosphors, which are suitable for three-band white Light Emitting Diodes (LED). To accomplish this, a computational evolutionary optimization process was adopted to screen a Eu$^{3+}$-doped alkali earth borosilicate system. The genetic algorithm is a well-known, very efficient heuristic optimization method and combi-chem is also a powerful tool for use in an actual experimental optimization process. Therefore the combination of a genetic algorithm and combi-chem would enhance the searching efficiency when applied to phosphor screening. Vertical simulations and an actual synthesis were carried out and promising red phosphors for three-band white LED applications, such as Eu$_{0.14}$Mg$_{0.18}$Ca$_{0.07}$Ba$_{0.12}$B$_{0.17}$Si$_{0.32}$O$_{\delta}$, were obtained.

Validation of urinary N-methylacetamide reference material for proficiency test (숙련도시험을 위한 소변 중 N-메틸아세트아미드 표준시료 검증)

  • Lee, Mi-Young
    • Analytical Science and Technology
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    • v.27 no.6
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    • pp.339-346
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    • 2014
  • The author assessed the availability of urine reference material for proficiency test provided for laboratories in occupational health. N-methylacetamide is the biomarker of exposure to N,N-dimethyl acetamide, which was used as the substitute for hepatotoxic N,N-dimethylformamide (DMF). N-methylacetamide (NMAC) urine samples of 3 different levels covering the 0.2~2 times of the exposure limit were tested. Stability test up to 180 days (0, 7, 30, 60, 180 days) at 4 different temperatures (-60, -20, 5, $25^{\circ}C$) and homogeneity test were performed for these samples. New analytical condition by GC/MSD using SIM mode (m/z 58, 59) and DB-624 column was investigated for better selectivity, sensitivity and resolution. Urinary NMAC samples showed good homogeneity for 3 levels. These samples also showed good stability up to 180 days. The data of stability and homogeneity of urinary DMAC confirmed the basis of including this item into Korean proficiency test for occupational health laboratories since 2008.

Investigation of Current Fluctuation at a River (하천에서의 흐름변동 조사)

  • Lee, Hyun-Seok;Kwon, Hyung-Joong;Kim, Young-Sung;Lee, Geun-Sang
    • Proceedings of the Korea Water Resources Association Conference
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    • 2007.05a
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    • pp.522-526
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    • 2007
  • 항공사진을 이용하여 하천의 경년변화를 조사하다 보면, 사주 변동에 따라 하천의 주 흐름이 다양하게 변화되고 있음을 알 수 있다. 이처럼 특정 하천의 지정된 구간에서의 흐름변동은 많은 시간에 걸쳐 이루어진다. 바꾸어 말하면, 짧은 시간 동안 자연하천에서의 주 흐름 변화를 관찰 하기는 일반적으로 매우 어렵다. 본 연구에서는 이틀이라는 짧은 시간 동안에, 하천에서의 주 흐름 변동에 따른 특성변화를 조사하였다. 이러한 조사는 "조정지 댐에서의 수문 조작"이라는 인위적인 방법을 동원함으로서 가능하였다. 모든 조정지 댐에서는 하천 유지를 위한 일정양의 물을 수문을 통하여 방류한다. 대청댐 하류에 있는 조정지 댐에는 폭이 약 10m에 이르는 10개의 수문이 있다. 평상시에는 우안으로부터 5번째에 있는 중앙의 수문을 개방하여 초당 약 18톤의 물을 방류한다. 그러므로 본 연구에서는 방류하고자 하는 지점의 수문높이를 조정하여 일정량을 유지한 채, 수문의 위치를 중앙에서 좌안 그리고 우안의 순으로 변경 하였다. 방류 수문 위치를 변경함에 따라 하천에서의 수리특성을 조사하기 위하여, 흐름이 안정 될 때까지 충분히 기다린 후, 각각의 경우에서의 하류지역을 대상으로 현지관측 및 수치실험을 실시하였다. 조사는, 첫째 지형측량, 유량측정 및 수위변동 등을 포함한 정밀현장조사, 둘째 일반적인 모델에 정밀조사 결과를 적용시킴으로서 얻을 수 있는 가시화 기법 개발 등의 순으로 진행하였다. 수치실험에 사용한 모델은 하천에서의 흐름거동을 2차원적으로 해석하는데 많이 사용되고 있는 상용프로그램인 SMS (Surface-Water Modeling System)의 RMA2 모형이다. 이모형은 RMA (Resource Management Associates, Inc.)에 의해 처음 개발된 2차원 유한요소 모델이며 지배방정식은 z방향을 수심 적분한 2차원 천수방정식으로, x와 y방향에 대한 Navier-Stokes 방정식과 연속 방정식으로 구성된다. 본 연구에서는 현장 조사 시 지배인자 파악의 중요성 및 수치계산을 위한 검증자료의 필요성을 강조하기 위하여, 일반적인 방법으로 수행한 계산 결과 및 다양한 현장 특성을 고려한 계산 결과를 비교 하였다. 그 결과 본 연구는 (1)최신 장비들의 도입 및 검증과 기존 장비의 활용 범위 확대, (2)기존의 상용 프로그램을 이용한 하천 흐름특성의 가시화 실현 등에 의의가 있다고 사료된다.

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A Study on Forest Vegetation in Mt. Cheongok, Kyungsangpuk-do - by the Method of Phytosociological Studies - (청옥산(靑玉山) 삼림식생(森林植生)에 관(關)한 연구(硏究) - 식물사회학적(植物社會學的) 분석방법(分析方法)으로 -)

  • Oh, Seung Hwan;Yun, Chung Weon;Bae, Kwan Ho;Hong, Sung Cheon
    • Journal of Korean Society of Forest Science
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    • v.87 no.1
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    • pp.27-39
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    • 1998
  • The Mt. Cheongok is located at the northern part of Kyungsangpookdo from $37^{\circ}$ 00' 00" to $37^{\circ}$ 05' 00" latitude and from $128^{\circ}$ 55' 00" to $129^{\circ}$ 00' 00" longitude. The altitude of the summit is 1,276.5m. This study was carried out to classify forest communities by the methods of Z${\ddot{u}}$rich-Montepellier schools. And, it also might be useful for selection of plant species, forest conservation, and prompting vegetation succession. The forest vegetation in Mt. Cheongok was classified into 12 communities, 4 groups, and 4 subgroups. Rhododendron micranthum subgroup of Pinus densiflora for. erecta community and Fraxinus mandshurica community were not found in cool temperate forest, southern zone yet. According to the coincidence method, Pines densiflora for. erecta community was mainly distributed from altitude 450m to 1,100m and from upper slope to ridge, and Quercus mongolica community was dominanced in the range of over altitude 700m. Pinus densiflora for. erecta community, distributed in upper slope and ridge, is judged to be maintained in the future. But Pinus densiflora for. erecta community, distributed in below middle slope, is judged to be changed into deciduous hardwood forest.

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INFLUENCE OF CAVITY SIZE AND RESTORATION METHODS ON THE CUSP DEFLECTION IN COMPOSITE RESTORATION (복합레진 수복시 와동의 크기 및 수복 방법이 교두 굴곡에 미치는 영향)

  • Lee Mi-Ra;Lee In-Bog;Seok Chang-In;Lee Sang-Tag;Um Chung-Moon
    • Restorative Dentistry and Endodontics
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    • v.29 no.6
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    • pp.532-540
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    • 2004
  • The aim of this study was to measure the cusp deflection during composite restoration for MOD cavity in premolar and to examine the influence of cavity dimension, C-factor and restoration method on the cusp deflection. Thirty extracted maxillary premolar were prepared to four different sizes of MOD cavity and divided into six groups. The width and depth of the cavity were as follows. Group 1; $1.5{\;}{\times}{\;}1{\;}mm$, Group 2; $1.5{\;}{\times}{\;}2{\;}mm$, Group 3; $3{\;}{\times}{\;}1{\;}mm$, and Group 4-6; $3{\;}{\times}{\;}2{\;}mm$ respectively. Group 1-4 were restored using bulk filling method with Z-250 composite. However, Group 5 was restored incrementally, and Group 6 was restored with an indirect resin inlay. The cusp deflection was recorded at the buccal and lingual cusp tips using LVDT probe for 10,000 seconds. The measured cusp deflections were compared between groups, and the relationship between the cube of the length of cavity wall/the cube of the thickness of cavity wall ($L^3/T^3$). C-factor and cusp deflection or % flexure ($100{\;}{\times}$ cuspal deflection / cavity width) was analyzed. The cusp deflection of Group 1-4 were $12.1{\;}\mu\textrm{m},{\;}17.2{\;}\mu\textrm{m},{\;}16.2{\;}\mu\textrm{m}{\;}and{\;}26.4{\;}\mu\textrm{m}$ respectively. The C-factor was related to the % flexure rather than the cusp deflection. There was a strong positive correlationship between the $L^3/T^3$ and the cusp deflection. The cusp deflection of Group 5 and 6 were $17.4{\;}\mu\textrm{m}{\;}and{\;}17.9{\;}\mu\textrm{m}$ respectively, which are much lower value than that of Group 4.

Radiosynthesis of $[^{11}C]6-OH-BTA-1$ in Different Media and Confirmation of Reaction By-products. ($[^{11}C]6-OH-BTA-1$ 조제 시 생성되는 부산물 규명과 반응용매에 따른 표지 효율 비교)

  • Lee, Hak-Jeong;Jeong, Jae-Min;Lee, Yun-Sang;Kim, Hyung-Woo;Lee, Eun-Kyoung;Lee, Dong-Soo;Chung, June-Key;Lee, Myung-Chul
    • Nuclear Medicine and Molecular Imaging
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    • v.41 no.3
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    • pp.241-246
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    • 2007
  • Purpose: $[^{11}C]6-OH-BTA-1$ ([N-methyl-$^{11}C$]2-(4'-methylaminophenyl)-6-hydroxybenzothiazole, 1), a -amyloid imaging agent for the diagnosis of Alzheimer's disease in PET, can be labeled with higher yield by a simple loop method. During the synthesis of $[^{11}C]1$, we found the formation of by-products in various solvents, e.g., methylethylketone (MEK), cyclohexanone (CHO), diethylketone (DEK), and dimethylformamide (DMF). Materials and Methods: In Automated radiosynthesis module, 1 mg of 4-aminophenyl-6-hydroxybenzothiazole (4) in 100 l of each solvent was reacted with $[^{11}C]methyl$ triflate in HPLC loop at room temperature (RT). The reaction mixture was separated by semi-preparative HPLC. Aliquots eluted at 14.4, 16.3 and 17.6 min were collected and analyzed by analytical HPLC and LC/MS spectrometer. Results: The labeling efficiencies of $[^{11}C]1$ were $86.0{\pm}5.5%$, $59.7{\pm}2.4%$, $29.9{\pm}1.8%$, and $7.6{\pm}0.5%$ in MEK, CHO, DEK and DMF, respectively. The LC/MS spectra of three products eluted at 14.4, 16.3 and 17.6 mins showed m/z peaks at 257.3 (M+1), 257.3 (M+1) and 271.3 (M+1), respectively, indicating their structures as 1, 2-(4'-aminophenyl)-6-methoxybenzothiazole (2) and by-product (3), respectively. Ratios of labeling efficiencies for the three products $([^{11}C]1:[^{11}C]2:[^{11}C]3)$ were $86.0{\pm}5.5%:5.0{\pm}3.4%:1.5{\pm}1.3%$ in MEK, $59.7{\pm}2.4%:4.7{\pm}3.2%:1.3{\pm}0.5%$ in CHO, $9.9{\pm}1.8%:2.0{\pm}0.7%:0.3{\pm}0.1%$ in DEK and $7.6{\pm}0.5%:0.0%:0.0%$ in DMF, respectively. Conclusion: The labeling efficiency of $[^{11}C]1$ was the highest when MEK was used as a reaction solvent. As results of mass spectrometry, 1 and 2 were conformed. 3 was presumed.