• Title/Summary/Keyword: Z. O. E.

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Phytochemical Studies on Lonicera Caulis (2) - Aliphatic and Phenolic Compounds (인동의 성분연구 (2) - 지방족 및 페놀성 화합물)

  • Kim, Ju-Sun;Yean, Min-Hye;Seo, Hyun-Kyu;Lee, Je-Hyun;Kang, Sam-Sik
    • Korean Journal of Pharmacognosy
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    • v.40 no.4
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    • pp.326-333
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    • 2009
  • Fourteen compounds were isolated from the 70% ethanol extract of Lonicera Caulis (Caprifoliaceae) and their structures were identified as seven aliphatic compounds [long-chain alcohols (1, 2), trilinolein (3), hexacosanol (4), fatty acids (6), 9,12,13-trihydroxyoctadeca-10(E),15(Z)-dienoic acid (10), and pinellic acid (11)] and seven phenolics [bis(2-ethylhexyl) phthalate (dioctylphthalate, DOP) (5), coniferaldehyde (7), caffeic acid docosanoyl ester (8), caffeic acid (9), coniferyl aldehyde 4-O-glucoside (12), linarin (13), and coniferin (14)]. The chemical structures of these compounds were identified on the basis of spectroscopic methods and comparison with literature values. All the compounds except for caffeic acid (9) were isolated from this plant parts for the first time.

A STUDY OF THE APICAL LEAKAGE OF VARIOUS RETROGRADE FILLING MATERIALS (Retrograde filling시 수종 충전재료에 따른 폐쇄효과에 대한 연구)

  • Do, Jeong-Wook;Kwon, Hyuk-Choon
    • Restorative Dentistry and Endodontics
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    • v.14 no.1
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    • pp.97-105
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    • 1989
  • This study was conducted to evaluate and compare the apical leakage among the retrograde filling materials; retrograde filling with non-zinc amalgam, cavity varnish and non-zinc amalgam, z.o.e cement, Glass Ionomer cement, scotch bond and silux. Sixty single rooted teeth were divided into six groups and each tooth was individually prepared for its particular group. The specimens were incubated at $37^{\circ}C$ for 24 hrs and then were infiltrated by 2% methylene blue for 7 days. Apical leakage was evaluated by measuring the degree of dye penetration between the filling material and the canal wall. The results were as follows: 1. The scotch bond and silux group showed the least amount of apical leakage and the control group showed the greatest amount of apical leakage. 2. The groups retrofilled with cavity varnish and amalgam, glass-Ionomer cement, scotch bond and silux showed significantly good apical seal than control group. 3. The groups retrofilled with glass Ionomer cement, scotchbond and silux showed significantly good apical seal than the groups retrofilled with Amalgam and Zinc oxide eugenol cement.

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Magnetic Properties of Ni-Cu-Zn Ferrite with varying Ni, Cu (Ni, Cu 변화에 따른 Ni-Cu-Zn Ferrite의 자기적 특성)

  • 백승철;정승우;김태원;김성수;최우성
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 1999.05a
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    • pp.259-262
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    • 1999
  • In this study, we investigated magnetic Properties of N $i_{0.2-x}$C $u_{x}$Z $n_{0.305}$F $e_{0.495}$ (x=0 ~0.2) ferrites. As the increased, the density and shrinkage increased until 5.3g/㎤, 20% respects, but the absorption decreased rate until 0.01%. As a results of the density, absorption rate, and shrinkage rate, the grain growth progressed rapidly in x=0.125 at 105$0^{\circ}C$, x=0.075 at 115$0^{\circ}C$, and x=0.025 at 115$0^{\circ}C$ for 3hours. As the CuO concentration increased, initial permeability increased at sintered 105$0^{\circ}C$ and 115$0^{\circ}C$ for 3 hours, but decreased at 125$0^{\circ}C$ for 3 hoers. The complex permeability as a function of frequency were high values at sintered 105$0^{\circ}C$ for 3 hours in x=0.005, 0.075.5.5.5.

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Enhancement of Electromagnetic Properties of (NiCuZn)-Ferrites by Using Ultra-fine Powders Synthesis (나노분말합성에 의한 (NiCuZn)-Ferrites의 전자기적 특성 향상)

  • 허은광;강영조;김정식
    • Proceedings of the International Microelectronics And Packaging Society Conference
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    • 2002.11a
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    • pp.109-113
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    • 2002
  • 본 연구에서는 공침법에 의한 초미세분말을 이용하여 제조된 (NiCuZn)-ferrite와 건식법을 이용하여 제조된 (NiCuZn)-ferrite의 저온소결 특성 및 전자기적 특성을 상호 비교 분석하였다. 조성은 (N $i_{0.4-x}$C $u_{x}$Z $n_{0.6}$)$_{1+w}$(F $e_2$ $O_4$/)$_{1-w}$에서 x의 값을 0.2, w의 값은 0.03으로 고정하였고, 소결은 공침법으로 합성된 분말의 경우 초기열처리과정을 거쳐 최종적으로 90$0^{\circ}C$에서, 건식법의 경우 11$50^{\circ}C$의 온도에서 진행하였다. 그 결과, 공침법으로 제조된 (NiCuZn)-ferrite는 건식법으로 제조된 (NiCuZn)-ferrite보다 20$0^{\circ}C$이상 낮은 소결온도에서 높은 소결밀도 값을 가졌으며, 품질계수 등 칩 인덕터에서 중요한 요소인 전자기적 특성이 우수하게 나타났다. 또한, 공침법으로 합성된 페라이트는 분말의 초기열처리온도에 따라 최종소결 특성이 크게 변하였다. 그밖에 공침법과 건식법으로 합성한 (NiCuZn)-ferrite의 결정성, 미세구조들을 XRD, SEM, TEM을 이용하여 비교 고찰하였다.하였다.다.

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The Black Hole Mass - Stellar Velocity Dispersion Relation of Narrow-Line Seyfert 1 Galaxies

  • Yoon, Yosep;Woo, Jong-Hak
    • The Bulletin of The Korean Astronomical Society
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    • v.37 no.2
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    • pp.75.1-75.1
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    • 2012
  • Narrow-Line Seyfert 1 galaxies are arguably the most important AGN subclass in investigating the origin of the black hole mass-galaxy stellar velocity dispersion (MBH-${\sigma}$) relation because of their high accretion rates close to the Eddington limit. Currently, it is still under discussion whether NLS1s are off from the local MBH-${\sigma}$ relation. We select a sample of 325 NLS1 at relatively low redshift (z<0.1) from the SDSS DR7 by constraining FWHM of $H{\beta}$ in the range of 800-2,200 km/s. Among them, we measured stellar velocity dispersion of 40 objects which show strong stellar absorption lines, e.g. Mg b triplet(${\sim}5175{\AA}$), Fe($5270{\AA}$). In contrast, the other 285 objects show too weak stellar absorption lines to measure velocity dispersion. Using the sample of 40 objects with stellar velocity dispersion measurements, we investigate whether NLS1s follow the same MBH-${\sigma}$ relation as normal galaxies and broad line AGNs. We also test the reliability of the width of narrow lines as a surrogate of stellar velocity dispersion by comparing directly measured stellar velocity dispersion with ${\sigma}$ inferred from [O III], [N II], [S II] line widths, respectively. We will discuss the connection between AGN activity in NLS1s and galaxy evolution based on these results.

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Influence of Glabrousness on the Insect Resistance and Some Agronomic Characters in Rice Plant (수도 매끄러운엽 품종과 껄끄러운엽 품종에 있어서의 벼멸구 저항성, 수량성 및 제현비율의 비교)

  • M. H, Heu;S. Z, Park;E. W, Lee;S. Y, Choi
    • KOREAN JOURNAL OF CROP SCIENCE
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    • v.25 no.2
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    • pp.1-5
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    • 1980
  • Comparisons were made between pubescent and smooth leaved cultivars or lines for the brown planthopper feeding preference, adult emergence percent, nymphal period, grain yield and brown rice recovery percent, and found that there were no significant differences of the traits tested between smooth and pubescent.

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Evaluation of the Cytotoxicity of Root Canal Disinfectants and Root Canal Sealers on L Cells in Vitro (수종(數種) 근관소독제(根管消毒劑) 및 근관충전재(根管充塡材)의 세포독성(細胞毒性)에 관(關)한 실험적(實驗的) 연구(硏究))

  • Chung, Choong-Mo
    • Restorative Dentistry and Endodontics
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    • v.7 no.1
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    • pp.85-99
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    • 1981
  • This study was to evaluate the cytotoxic effect of three root canal disinfectants (formocresol, camphorated phenol and eugenol) and ten root canal sealers(Cavitec, Hypo-cal, Vitapex, AH26, Canals, Mynol, $N_2$, $N_2$-Medical, Z. O. E. and Calvital) in vitro. The experiments were performed in four differrent modes. In the first and second experiment, the "long-distance" cytotoxicity of three root canal disinfectants were tested on L cells. In the third exeriment, ten root canal sealers were tested for cytotoxicity by means of the tissue culture-agar overlay method immediately, 4 and 24 hours after the experiment. In the fourth experiment, the study with radioactively labeled L cells were employed to determine the relative cytotoxicity of ten root canal sealers. The results were as follows; 1. Every vapors from disinfectants showed more or less cytotoxicity. Of the three disinfectats, formocresol appeared to be the highest cytotoxic effect and camphorated phenol was the lowest. 2. Root canal sealers tested in tbis study showed cytotoxicity at every stage of time intervals. 3. The highest cytotoxic effect was freshly mixed $N_2$ meaical and $N_2$ also revealed the highest cytotoxic effect after 4 or 24 hours among these materials. Vitapex was found the lowest cytotoxic effect at all experimental stage. 4. Root canal sealers except N2 and Mynol showed cytotoxic effect were decreased cytotoxicity according to the time elapsed.

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SYNTHESIS OF METASTABLE ALLOYS BY ION MIXING IN THE BINARY METAL SYSTEMS AND THEORETICAL MODELLING

  • Liu, B.X.;Zhang, Z.J.;Jin, O.;Pan, F.
    • Journal of the Korean Vacuum Society
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    • v.4 no.S2
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    • pp.148-155
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    • 1995
  • (1) The metastable crystalline(MX) phases formed by ion mixing are classified into 5 types, i.e. the super-saturated solid solutions and the enlarged HCP-I phases reported earlier, and the newly observed FCC-I phases in hcp-based alloys, The FCC-ll and HCP-ll phases in bcc-based alloys. The growth kinetics of the MX phases is discussed. (2) The interfacial free energy in the multilayered films was found to play an important role in ion beam mixing(IM) induced amorphization. By adding sufficient interfaces, amorphous alloys were obtained even in the systems with rather positive heat of formation. (3) Gibbs free energy diagrams of some representative systems were constructed, by calculating the free energy curves of all the competing phases. Steady-state thermal annealing was conducted and the results confirmed the relevance of the constructed diagrams, which were inturn employed to interpret the MX phase formation as well as the glass forming ability upon IM in the binary metal systems.

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ENHANCED ADHESION STRENGTH OF Cu/polyimide AND Cu/Al/polyimide BY ION BEAM MIXING

  • Chang, G.S.;Kim, T.G.;Chae, K.H.;Whang, C.N.;Zatsepin, D.S.;Kurmaev, E.Z.;Choe, H.S.;Lee, Y.P.
    • Journal of the Korean Vacuum Society
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    • v.6 no.S1
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    • pp.122-126
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    • 1997
  • the Cu/polyimide system is known to be the best candidate for a multilevel interconnection system due to the low resistance of Cu and to the low dielectric constant of polyimide respectively. Ion beam mixing of Cu(40nm)/polyimide was carried out at room temperature with 80 keV Ar+ and N2+ form $1.5\times$1015 to 15$\times$1015 ions/cm2. The quantitative adhesion strength was measured by a standard scratch test. X-ray photoelectron spectroscopy and x-ray emission spectrocopy are employed to investigate the chemical bonds and the interlayer compound formation of the films Cu/Al/polyimide showed more adhesion strength than Cu/polyimide after ion beam mixing and N2+ ions are more effective in the adhesion enhancement than Ar+ with the same sample geometry. The XES results shows the formation of interlayer compound of CuAl2O4 which can reflect more adhesive Cu/Al/polyimide which has not been reported previously. The latter results is understood by the fact that N2+ ions produce more pyridinelike moiety, amide group and tertiary amine moiety whcih are known as adhesion promotors.

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Piezoelectric and Electro-induced Strain Properties of $(Pb_{1-2x/3}Bi_x)[(Ni_{1/3}Nb_{2/3})_{0.4}(Ti_{0.6}Zr_{0.4})_{0.6}]O_3$Ceramics with the Substitution of $Bi_2O_3$ ($Bi_2O_3$치환에 따른 $(Pb_{1-2x/3}Bi_x)[(Ni_{1/3}Nb_{2/3})_{0.4}(Ti_{0.6}Zr_{0.4})_{0.6}]O_3$ 세라믹스의 압전 및 전계유기 왜형 특성)

  • 윤현상;정회승;임인호;윤광희;김준한;박창엽
    • Electrical & Electronic Materials
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    • v.10 no.5
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    • pp.434-439
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    • 1997
  • It this paper, the piezoelectric and electro-induced strain properties of (P $b_{1-}$2x/3/B $i_{x}$ )[N $i_{1}$3/N $b_{2}$3/)$_{0.4}$( $Ti_{0.6}$Z $r_{0.4}$)$_{0.6}$] $O_3$ceramics (x=0, 0.005, 0.02) were investigated with the substitution of B $i^{3+}$, and the feasibility of the application for bimorph actuator was evaluated by measuring the dynamic properties of the piezoelectric bimorph fabricated with above ceramics. Dielectric constant was enhanced with the increase of B $i^{3+}$ substitution, and appeared the maximum value of 5032 at x=0.01 composition. Increasing the substitution of B $i^{3+}$, the electromechanical coefficient( $k_{p}$ , $k_{31}$ ) was increased up to the substitution of 0.5 mol% B $i^{3+}$, showed the value of 0.656, 0.439, respectively. The piezoelectric constant( $d_{33}$ $d_{31}$ ) had the highest value of 344, 825 with the substitution of 0.5 mol% B $i^{3+}$. The strain, generated by 60 Hz AC electric field, had the largest value of 1200($\times$10$^{-6}$ $\Delta$1/1) in the composition with the substitution of 0.5 mol% B $i^{3+}$. The dynamic properties of the bimorph actuator, fabricated with the composition substitution of 0.5 mol% B $i^{3+}$, showed the largest value of 325 $\mu$m at $\pm$150 V square pulse. square pulse.are pulse..

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