• Title/Summary/Keyword: X-ray measurement

Search Result 1,305, Processing Time 0.037 seconds

Structural and photoelectrical properties of copper phthalocyanine(CuPc) thin film on Si substrate by thermal evaporation (Si 기판위에 열증착법으로 제조한 copper phthalocyanine(CuPc) 박막의 구조 및 광전특성)

  • Lee, Hea-Yeon;Jeong, Jung-Hyun;Lee, Jong-Kyu
    • Journal of Sensor Science and Technology
    • /
    • v.6 no.5
    • /
    • pp.407-413
    • /
    • 1997
  • The crystallized CuPc(copper phthalocyanine) film on a p-type <100> Si substrate is prepared at the substrate temperature of $300^{\circ}C$ by thermal evaporation. X -ray diffraction analysis showed the CuPc film to have a-axis oriented structure. For the measurement of photovoltaic characteristics of the CuPc/Si film and the Si substrate, a transverse current-voltage (I-V) curve is observed. In the dark, the Au/Si junction is shown to be ohmic contact. However, under illumination, a photovoltaic effect is not observed. The I-V curve in the dark indicates that the CuPc film on Si may form an ohmic contact. Since the CuPc film is a p-type semiconductor, the CuPc/p-Si junction has no barrier at the interface. Under illumination, the CuPc/Si junction shows a large photocurrent comparing with that of the wafer. The result indicates that the CuPc layer plays an important role in the photocarrier generation under red illumination (600 nm). The CuPc/Si film shows the photo voltaic characteristics with a short-circuit photocurrent ($J_{sc}$) of $4.29\;mA/cm^{2}$ and an open-circuit voltage ($V_{oc}$) of 12 mA.

  • PDF

A study on measurement of the pollution levels and disinfection of medical radiation shielding for lead apron (의료방사선 차폐용 납 가운의 오염도 측정 및 소독에 관한 연구)

  • Kim, Hyeon-Ju
    • Journal of the Korea Academia-Industrial cooperation Society
    • /
    • v.17 no.5
    • /
    • pp.490-497
    • /
    • 2016
  • This study compared and analyzed the pollution levels of radiation shielding aprons and ways to sterilize them using 30 lead aprons. After collecting samples from the center of the lead apron, where contact is most frequent, experiments were conducted employing Coagula and Latex methods. Using the culture medium where bacteria grew, measurements of the pathogen count and identification were performed. The greatest number of pathogens were $7.16{\pm}10$, which were detected on the lead apron from general X-ray room #2, but there was no significant difference according to the facilities (p > 0.05). Compared to how many pathogens remained between using the disinfectant ethanol and tissue, the pathogens decreased by $0.01{\pm}0.4$ (p < 0.05) after using disinfectant ethanol and by $0.87{\pm}1.7$(p < 0.05) after using disinfectant tissue. The Pearson correlation test revealed a significant correlation (-0.296, p < 0.05) between them. According to this research, there were pathogens on the lead aprons and the number of pathogens was determined by statistical analysis. It is expected that the rate of radiology technologists, patients, and medical equipment infected by pathogens will be reduced by the proper use of sterilization with a disinfectant ethanol.

Analysis of Image Factors of X-ray Films: Study for the Intelligent Replenishment System of Automatic Film Processor (자동현상기 지능화에 필요한 연산처리 기법의 개발을 위한 방사선 필름의 영상 지수의 분석)

  • Park, Sung-Tae;Yoon, Chong-Hyun;Park, Kwang-Bo;Auh, Yong-Ho;Lee, Hyoung-Jin;In, Kyung-Hwan;Kim, Keon-Chung
    • Journal of radiological science and technology
    • /
    • v.21 no.1
    • /
    • pp.35-39
    • /
    • 1998
  • We analyzed image factors to determine the characteristic factors that need for intelligent replenishment system of the auto film processor. We processed the serial 300 sheets of radiographic films of chest phantom without replenishment of developing and fixation replenisher. We took the digital data by using film digitizer which scaned the films and automatically summed up the pixel values of the films. We analyzed characteristic curves, average gradients and relative speeds of individual film using densitometer and step densitometry. We also evaluated the pH of developer, fixer, and washer fluid with digital pH meter. Fixer residual rate and washing effect were measured by densitometer using the reagent methods. There was no significant reduction of the digital density numbers of the serial films without replenishment of developer and fixer. The average gradients were gradually decreased by 0.02 and relative speeds were also gradually decreased by 6.96% relative to initial standard step-densitometric measurement. The pHs of developer and fixer were reflected the inactivation of each fluid. The fixer residual rates and washing effects after processing each 25 sheets of films were in the normal range. We suggest that the digital data are not reliable due to limitation of the hardware and software of the film digitizer. We conclude that average gradient and relative speed which mean the film's contrast and sensitivity respectively are reliable factors for determining the need for the replenishment of the auto film processor. We need more study of simpler equations and programming for more intelligent replenishment system of the auto film processor.

  • PDF

Preparation of Bismuth Telluride Thin Films using RF magnetron sputtering and Study on Their Thermoelectric Properties (RF 마그네트론 스퍼터링을 이용한 Bismuth Telluride 박막의 제조와 그 열전 특성 연구)

  • Kim, Dong-Ho;Lee, Gun-Hwan
    • Journal of the Korean Vacuum Society
    • /
    • v.14 no.4
    • /
    • pp.215-221
    • /
    • 2005
  • Thermoelectric bismuth telluride thin films were prepared on $SiO_{2}$/Si substrate with co-sputtering of bismuth and tellurium targets. The effects of deposition temperature on surface morphology, crystallinity and electrical transport properties were investigated. Hexagonal crystallites were clearly visible at the surface of films deposited above $290 ^{\circ}C$. Change of dominant phase from rhombohedral $Bi_2Te_3$ to hexagonal BiTe was confirmed with X-ray diffraction analysis. The deviation from stoichiometric composition at high deposition temperature resulted in the change of structural and electrical characteristics. Seebeck coefficients of all samples have negative value, indicating the prepared $Bi_XTe_Y$ films are n-type thermoelectric. Optimum of Seebeck coefficient and power factor were obtained at the deposition temperature of $225 \^{circ}$C (about -55 $\mu$V/K and $3\times10^{-4}$ W/$k^{2}$m, respectively). Deterioration of thermoelectric properties at higher temperature.

Effect of Deposition Temperature on the Characteristics of Low Dielectric Fluorinated Amorphous Carbon Thin Films (증착온도가 저유전 a-C:F 박막의 특성에 미치는 영향)

  • Park, Jeong-Won;Yang, Sung-Hoon;Park, Jong-Wan
    • Korean Journal of Materials Research
    • /
    • v.9 no.12
    • /
    • pp.1211-1215
    • /
    • 1999
  • Fluorinated amorphous carbon (a-C:F) films were prepared by an electron cyclotron resonance chemical vapor deposition (ECRCVD) system using a gas mixture of $C_2F_6$ and $CH_4$ over a range of deposition temperature (room temperature ~ 300$^{\circ}C$). 500$^{\AA}C$ thick DLC films were pre-deposited on Si substrate to improve the strength between substrate and a-C:F film. The chemical bonding structure, chemical composition, surface roughness and dielectric constant of a-C:F films deposited by varying the deposition temperature were studied with a variety of techniques, such as Fourier transform infrared spectroscopy(FTIR), X-ray photoelectron spectroscopy(XPS), atomic force microscopy (AFM) and capacitance-voltage(C-V) measurement. Both deposition rate and fluorine content decreased linearly with increasing deposition temperature. As the deposition temperature increased from room temperature to 300$^{\circ}C$, the fluorine concentration decreased from 53.9at.% down to 41.0at.%. The dielectric constant increased from 2.45 to 2.71 with increasing the deposition temperature from room temperature to 300$^{\circ}C$. The film shrinkage was reduced with increasing deposition temperature. This results ascribed by the increased crosslinking in the films at the higher deposition temperature.

  • PDF

Age Estimation by Dental Radiographs in Korean Adults (한국 성인에서 치과용 방사선사진에 의한 연령감정)

  • Jeon, Hee-Sun;Tea, Il-Ho;Ko, Myung-Yun;Ahn, Yong-Woo
    • Journal of Oral Medicine and Pain
    • /
    • v.34 no.2
    • /
    • pp.179-188
    • /
    • 2009
  • Aim of this study is to examine correlation between size of the coronal pulp cavity and chronological age in adult. Total 716 teeth (218 mandibular canines, 230 first premolars, 268 second premolars) free from pathologies and dental restorations were selected from 276 patients (111 males, 165 females), ranging from 20-69 years. Using periapical X-ray, the height (mm) of the crown (CH=coronal height) and the height (mm) of the coronal pulp cavity (CPCH=coronal pulp cavity height) of the teeth were measured. The tooth-coronal index (TCI) after Ikeda et al (Jpn. J. For. Med. 1985;39:244-250) was computed for each tooth and regressed on real age. With increasing age, the TCI was relatively decreased, indicating the reduction of length of the pulp chamber. Even reduction of the TCI with aging was found in combined group rather than in each sex and type of tooth separately. The most definite reduction was in canine of combined group. The correlation coefficient was strongest when measurement from canines of females (r2=0.247).

The comparisons of layers and the effect of additional firings on flexural strength and translucency of 5Y-ZP (Translucent zirconia의 layer 간 비교 및 추가적인 소성이 굽힘강도, 투과도에 미치는 영향)

  • Kim, Hyung-Joon;Shin, Soo-Yeon
    • Journal of Dental Rehabilitation and Applied Science
    • /
    • v.37 no.3
    • /
    • pp.111-122
    • /
    • 2021
  • Purpose: The purpose of this in vitro study was to investigate the flexural strength and translucency of three layers in 5Y-ZP and to assess the effect of additional firings on these properties. Materials and Methods: Sintered zirconia blocks were sectioned according to three layers : incisal, transition, and body. Disc-shaped specimens were fabricated from each layer. The diameter of specimens was 15.0 mm and each thickness of specimens for biaxial flexural strength test and translucency was 1.2 mm and 1.0 mm. The specimens were classified into subgroups according to the number of firing (0, 1, and 3 times; n = 10/subgroup) and the additional firings were performed under 900℃ using a furnace. Biaxial flexural strength and translucency was measured using universal testing machine and uv-vis spectrophotometer. X-ray diffraction (XRD) analysis was used for measurement of the phase identification. One-way ANOVA, Tukey HSD test were performed (α = 0.05). Results: There was no significant difference in flexural strength between the three layers (P > 0.05), while there was significant difference in translucency between different layers (P < 0.05). The flexural strength of incisal and transition layer was decreased by the single additional firing, and the three additional firings significantly decreased the flexural strength of three layers. The translucency of layer was decreased by additional firings except the body layer. The XRD patterns of all groups were similar. Conclusion: Three layers of 5Y-ZP were different only in translucency. Additional firings affected the flexural strength and translucency differently depending on the layers but crystalline phases were not changed.

Highly-permeable Mixed Matrix Membranes Based on SBS-g-POEM Copolymer, ZIF-8 and Ionic Liquid (SBS-g-POEM 공중합체, ZIF-8, 이온성 액체에 기반한 고투과성 혼합 매질 분리막)

  • Kang, Dong A;Kim, Kihoon;Kim, Jong Hak
    • Membrane Journal
    • /
    • v.29 no.1
    • /
    • pp.44-50
    • /
    • 2019
  • In this paper, we developed mixed matrix membranes (MMMs) consisting of SBS-g-POEM block-graft copolymer, ionic liquid (EMIMTFSI) and ZIF-8 nanoparticles to separate a $CO_2/N_2$ gas pair. The SBS-g-POEM is a rubbery block-graft copolymer synthesized through low-cost free-radical polymerization. The EMIMTFSI was dissolved into the SBS-g-POEM matrix and solution synthesized ZIF-8 nanoparticles were also dispersed into the copolymer matrix. The physico-chemical properties of manufactured membranes were characterized by Fourier transform infrared spectroscopy (FT-IR), differential scanning calorimetry (DSC), scanning electron microscopy (SEM), X-ray diffraction (XRD), which showed that the components were compatible with each other. The gas separation performance was confirmed by time-lag measurements showing $CO_2$ permeability of 537.0 barrer and $CO_2/N_2$ selectivity of 15.2. The result represents the EMIMTFSI and ZIF-8 nanoparticles improves the gas permeability more than two-times, without significantly sacrificing the $CO_2/N_2$ selectivity.

Development of Reinforcement Grout Materials Using Blast Furnace Slag Powder and Aramid Fiber (고로슬래그 미분말과 아라미드 섬유를 이용한 보강그라우트재 개발)

  • Seo, Hyeok;Park, Kyung-Ho;Kim, Chan-Jung;Kim, Ho-Chul;Kim, Daehyeon
    • Journal of the Korean Geosynthetics Society
    • /
    • v.18 no.1
    • /
    • pp.67-77
    • /
    • 2019
  • The grouting method is utilized to reinforce and waterproof poor grounds, enhance the bearing capacity of structures damaged resulting from settlement due to elevation and vibration or differential settlement, and for cutoff. The purpose of this research is to enhance the compressive strength of grout materials by using aramid fiber and develop a high-strength ground improvement method by using blast furnace slag powder. In this regard, this study has conducted a uniaxial compression test after checking the high charge (higher than 50%) of the ratio of blast furnace slag powder and cement at 100:0, 70:30 and 40:60%, adding the aramid mixture based on 0, 0.5 and 1.0% of the cement and furnace slag powder weight and creating sand gels based on surface oiling rate of 0.7 and 1.2%. For the environmental review evaluation, a heavy metal exudation test and a pH test measurement have been conducted. The experiment results showed that 1% increase of aramid fiber led to 1.3 times greater uniaxial compression intensity. As for the hexavalent chrome, a 30% increase in blast furnace slag powder led to approximately 50% decrease in heavy metal exudation. However, the pH test revealed that a 30% increase in blast furnace slag powder resulted in approximately 0.5 increase in pH. Further research on the pH part is needed in the future.

Effect of boron milling on phase formation and critical current density of MgB2 bulk superconductors

  • Kang, M.O.;Joo, J.;Jun, B.H.;Park, S.D.;Kim, C.S.;Kim, C.J.
    • Progress in Superconductivity and Cryogenics
    • /
    • v.21 no.1
    • /
    • pp.18-24
    • /
    • 2019
  • This study was carried out to investigate the effect of milling of boron (B), which is one of raw materials of $MgB_2$, on the critical current density ($J_c$) of $MgB_2$. B powder used in this study is semi-amorphous B (Pavezyum, Turkey, 97% purity, 1 micron). The size of B powder was reduced by planetary milling using $ZrO_2$ balls (a diameter of 2 mm). The B powder and balls with a ratio of 1:20 were charged in a ceramic jar and then the jar was filled with toluene. The milling time was varied from 0 to 8 h. The milled B powders were mixed with Mg powder in the composition of (Mg+2B), and the powder mixtures were uniaxially pressed at 3 tons. The powder compacts were heat-treated at $700^{\circ}C$ for 1 h in flowing argon gas. Powder X-ray diffraction and FWHM (Full width at half maximum) were used to analyze the phase formation and crystallinity of $MgB_2$. The superconducting transition temperature ($T_c$) and $J_c$ of $MgB_2$ were measured using a magnetic property measurement system (MPMS). It was found that $B_2O_3$ was formed by B milling and the subsequent drying process, and the volume fraction of $B_2O_3$ increased as milling time increased. The $T_c$ of $MgB_2$ decreased with increasing milling time, which was explained in terms of the decreased volume fraction of $MgB_2$, the line broadening of $MgB_2$ peaks and the formation of $B_2O_3$. The $J_c$ at 5 K increased with increasing milling time. The $J_c$ increase is more remarkable at the magnetic field higher than 3 T. The $J_c$ at 5 K and 4 T was the highest as $4.37{\times}10^4A/cm^2$ when milling time was 2 h. The $J_c$ at 20 K also increased with increasing milling time. However, The $J_c$ of the samples with the prolonged milling for 6 and 8 h were lower than that of the non-milled sample.