• 한국지반공학회:학술대회논문집
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• 한국지반공학회 1999년도 가을 학술발표회 논문집
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• pp.75-80
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• 1999

In this study, clay sampled from Yangsan$.$Mulkum site were used to analyze mineral properties. Mineral and chemical properties of clay were investigated through X-ray fluorescence spectrometer(XRF), X-Ray Diffraction(XRD), and Scanning Electron Microscope(SEM) analysis. The result of this test represents that Yangsan$.$Mulkum clay are composed of quartz, albite, anorthite, orthocalse and illite.

• 비파괴검사학회지
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• 제16권1호
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• pp.10-18
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• 1996

본 연구에서는 SS41 불림재와 M.E.F. 복합 조직강에 대해서 파괴 역학 파라미터와 X-선 파라미터 사이의 관계를 규명하였다. 피로 균열 진전 실험이 수행되었고, X-선 회절 방법이 피로 파단면에 적용되었다. 피로 파단면을 순차적으로 전해 연마하면서 깊이에 따른 X-선 파라미터(잔류응력, 반가폭)의 변화를 관찰하였다. 최대 소성역 깊이 $w_y$는 SS41 불림재에서는 반가폭의 분포로, M.E.F. 복합 조직강에 대해서는 잔류 응력의 분포로 결정할 수 있었다. 피로 파단면의 깊이 방향에 따른 X-선 파라미터의 분포로부터 $K_{max}$과 $w_y$의 관계식이 실험 데이타로부터 얻어지고, 이 식들으로부터 $K_{max}$은 $w_y$의 측정에 의하여 추정되어질 수 있다.

• 한국해양공학회지
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• 제22권6호
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• pp.27-34
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• 2008

The temperature distribution in the weldment is not uniform because a weldment is locally heated. Thermal plastic deformation results from the local expansion and shrinkage by the heating and cooling of metal. Therefore, residual stresses and distortion occur in the weldment. In this study, we had conducted on the weld thermal cycle simulation that is supposed as the HAZ on SS400 steel and STS304 steel. The residual stresses that were obtained from the drawing and the weld thermal cycle simulation were estimated by X-ray diffraction. We also carried out ultrasonic test for the weld thermal cycle simulated specimens, and then conducted on nondestructive evaluation by the ultrasonic parameters obtained ultrasonic test. From the results, residual stresses of weld thermal cycle simulated specimens after the residual stress removal heat treatment are lower than that of the drawing.

• 한국진공학회:학술대회논문집
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• 한국진공학회 2016년도 제50회 동계 정기학술대회 초록집
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• pp.360.2-360.2
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• 2016

CuSn thin films were fabricated by rf magnetron co-sputtering method on the Si(100) substrate for evaluation of the antibacterial effect. The co-sputtering process was performed with different rf powers and sputtering times to regulate the thickness of the films and relative atomic ratio of Cu to Sn. The physicochemical properties of the CuSn thin films were characterized by X-ray diffraction (XRD), X-ray photoelectron spectroscopy (XPS), X-ray induced Auger electron spectroscopy (XAES), Optical microscope (OM), 4-point probe, and antibacterial test. An antibacterial test was conducted with Escherichia coli (E. coli) and Staphylococcus aureus (S. aureus) as changing contact times between CuSn fillms and bacteria suspension. We compared to the crystalline structures of films before sterilization and after sterilization by XRD measurement. The changes of oxidation states of Cu and Sn and the chemical environment of films before and after antibacterial test were investigated with high resolution XPS spectra in the regions of Cu 2p, Cu LMM, and Sn 3d. After antibacterial test, the morphology of the films was checked with an OM images. The electrical properties of the CuSn films such as surface resistance and conductivity were measured by using 4-point probe.

• Tribology and Lubricants
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• 제18권4호
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• pp.260-266
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• 2002

In this study, the effects of oxide layer farmed on the wear tracks of TiN coated silicon wafer on friction and wear characteristics were investigated. Silicon wafer was used for the substrate of coated disk specimens, which were prepared by depositing TiN coating with 1 ${\mu}{\textrm}{m}$ in coating thickness. AISI 52100 steel ball was used fur the counterpart. The tests were performed both in air for forming oxide layer on the wear track and in nitrogen to avoid oxidation. This paper reports characterization of the oxide layer effects on friction and wear characteristics using X-ray diffraction(XRD), Auger electron spectroscopy(AES), scanning electron microscopy (SEM) and multi-mode atomic force microscope(AFM).

• Tribology and Lubricants
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• 제16권1호
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• pp.9-14
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• 2000

It has been cleared in previous author's paper that the fatigue life before the pitting on the rolling contact surface with lubricant are influenced by the wear amount. In this study, the wear type has been clarified when wear amount is extremely large such as the case without lubricant. The test of rolling contact fatigue has been conducted under two different of herzian pressures and three different of slide ratios without lubricant. In addition, residual stress and half-value breadth using X-ray diffraction on worn surface have been measured as well as the wear amount. The results show that the pitting type wear by rolling contact fatigue has not been occurred when the wear amount is considerably large. Thus this type of wear has been deduced by the fatigue wear depending on delamination theory.

• 한국윤활학회:학술대회논문집
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• 한국윤활학회 2002년도 제35회 춘계학술대회
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• pp.310-316
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• 2002

In this study, the effects of oxide layer formed on the wear tracks of TiN coated silicon wafer on friction and wear characteristics were investigated. Silicon wafer was used for the substrate of coated disk specimens, which were prepared by depositing TiN coating with $1{\mu}m$ in coating thickness. AISI 52100 steel ball was used for the counterpart. The tests were performed both in air for forming oxide layer on the wear track and in nitrogen to avoid oxidation. This paper reports characterization of the oxide layer effects on friction and wear characteristics using X-ray diffraction (XRD). Auger electron spectroscopy (AES), scanning electron microscopy (SEM) and sliding tests.

• 한국자기학회:학술대회 개요집
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• 한국자기학회 2011년도 임시총회 및 하계학술연구발표회
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• pp.19-19
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• 2011

We studied the effect of Dy content on the magnetic properties of cobalt ferrite single crystal. The $CoFe_{1.9}Dy_{0.1}O_4$ single crystals were grown by the flux method by using $Na_2B_4O_{7.}10H_2O$ (Borax) as a solvent (flux). The black and shiny single crystals were obtained as a product. The X-ray diffraction test at room temperature confirmed the spinel cubic symmetry with lattice constant a = $8.42{\AA}$ of the single crystals. The presences of constitute elements (Co, Fe and Dy) was endorsedby EDAX analysis. The saturation magnetization (Ms) of $CoFe_{1.9}Dy_{0.1}O_4$ single crystals was measured and is found to be 72emu/g or equivalently $3.2{\mu}B$/f.u. at 300 K. The observed Ms and coercivity (Hc) is found to be lower than that of pure $CoFe_2O_4$.

• 한국콘크리트학회:학술대회논문집
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• 한국콘크리트학회 2009년도 춘계 학술대회 제21권1호
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• pp.319-320
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• 2009

알칼리 활성 반응에 의한 고로 슬래그와 플라이 애시의 반응생성물에 대하여 강도실험 및 방사광 X선 회절 연구가 실시되었다. 본 연구는 지금까지 제올라이트 계열로 추정되어 왔던 지오폴리머의 실제 결정 구조가 무경절질형태의 ABC-6 family 제올라이트에 속해 있음을 제안한다.

• 한국소성가공학회:학술대회논문집
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• 한국소성가공학회 2005년도 추계학술대회 논문집
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• pp.418-422
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• 2005

In this study, the die design and die series on the surface residual stress of cold drawn eutectoid steel wire has been investigated. Test pieces were fabricated using die series with different mean and final reduction ratio. Surface residual stresses in the axial direction were measured by X-ray diffraction, Broker's 2-dimensional GADDS system. Results were compared with stress profiles which were calculated by 3D and 2D finite element simulation, Hibbitt's ABAQUS 6.4 program in Finite Element Analysis. By means of FEA method, optimal die shape considering delta-parameter were induced and applied in order to determine die sequence designs. Balance of the drawing stresses was also introduced to optimize die sequence.