• Title/Summary/Keyword: X-ray computed microtomography

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Nondestructive Evaluation of Microstructure of SiCf/SiC Composites by X-Ray Computed Microtomography

  • Kim, Weon-Ju;Kim, Daejong;Jung, Choong Hwan;Park, Ji Yeon;Snead, Lance L.
    • Journal of the Korean Ceramic Society
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    • v.50 no.6
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    • pp.378-383
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    • 2013
  • Continuous fiber-reinforced ceramic matrix composites (CFCCs) have a complex distribution of porosity, consisting of interfiber micro pores and interbundle/interply macro pores. Owing to the complex geometry of the pores and fiber architecture, it is difficult to obtain representative microstructural features throughout the specimen volume with conventional, destructive ceramographic approaches. In this study, we introduce X-ray computed microtomography (X-ray ${\mu}CT$) to nondestructively analyze the microstructures of disk shaped and tubular $SiC_f$/SiC composites fabricated by the chemical vapor infiltration (CVI) method. The disk specimen made by stacking plain-woven SiC fabrics exhibited periodic, large fluctuation of porosity in the stacking direction but much less variation of porosity perpendicular to the fabric planes. The X-ray ${\mu}CT$ evaluation of the microstructure was also effectively utilized to improve the fabrication process of the triple-layered tubular SiC composite.

Microscale Analysis of the Anisotropic Sintering of Metal Powder Compacts

  • Vagnon, Alexandre;Kapelski, Georges;Bouvard, Didier.
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2006.09a
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    • pp.260-261
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    • 2006
  • The behaviour of steel powder compacts during sintering has been investigated by dilatometry and X-ray computed microtomography. Dilatometry measurements showed that the anisotropic deformation results from various phenomena arising at different moments of the cycle including the delubrication stage. Microtomography provided 3D images of the microstructure induced by prior die pressing and its changes throughout sintering. Finally a schematic description of the main phenomena responsible for the deformation of metal powder compacts during sintering is proposed.

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Analysis of Failure Mechanisms during Powder Compaction

  • Wu, Chuan-Yu;Bentham, A.C.;Mills, A.
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2006.09a
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    • pp.26-27
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    • 2006
  • Capping mechanisms during the compaction of pharmaceutical powders were explored. Both experimental and numerical investigations were performed. For the experimental study, an X-ray Computed Microtomography system has also used to examine the internal failure patterns of the tablets produced using a compaction simulator. Finite element (FE) methods have also been used to analyse the powder compaction. The experimental and numerical studies have shown that the shear bands developed at the early stage of unloading appear to be responsible for the occurrence of capping. It has also been found that the capping patterns depend on the compact shape.

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Computational rock physics: Lattice-Boltzmann fluid flow simulation in porous media and its applications

  • Keehm, Young-Seuk;Mukerji, Tapan;Nur, Amos
    • 한국지구물리탐사학회:학술대회논문집
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    • 2003.11a
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    • pp.661-668
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    • 2003
  • This paper presents Lattice-Boltzmann simulation techniques for single-phase and two-phase fluid flow in porous media. Numerical experiments were performed in a digital rock sample from X-ray microtomography. Computed results showed very good agreement with laboratory measurements of permeability and relative permeability. Two applications using these simulation techniques show the potential of the Lattice-Boltzmann flow simulation to solve many difficult problems coupled with fluid flow in porous media.

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Image Calibration Techniques for Removing Cupping and Ring Artifacts in X-ray Micro-CT Images (X-ray micro-CT 이미지 내 패임 및 동심원상 화상결함 제거를 위한 이미지 보정 기법)

  • Jung, Yeon-Jong;Yun, Tae-Sup;Kim, Kwang-Yeom;Choo, Jin-Hyun
    • Journal of the Korean Geotechnical Society
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    • v.27 no.11
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    • pp.93-101
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    • 2011
  • High quality X-ray computed microtomography (micro-CT) imaging of internal microstructures and pore space in geomaterials is often hampered by some inherent noises embedded in the images. In this paper, we introduce image calibration techniques for removing the most common noises in X-ray micro-CT, cupping (brightness difference between the periphery and central regions) and ring artifacts (consecutive concentric circles emanating from the origin). The artifacts removal sequentially applies coordinate transformation, normalization, and low-pass filtering in 2D Fourier spectrum to raw CT-images. The applicability and performance of the techniques are showcased by describing extraction of 3D pore structures from micro-CT images of porous basalt using artifacts reductions, binarization, and volume stacking. Comparisions between calibrated and raw images indicate that the artifacts removal allows us to avoid the overestimation of porosity of imaged materials, and proper calibration of the artifacts plays a crucial role in using X-ray CT for geomaterials.

Three-dimensional microstructure of human alveolar trabecular bone: a micro-computed tomography study

  • Lee, Ji-Hyun;Kim, Hee-Jin;Yun, Jeong-Ho
    • Journal of Periodontal and Implant Science
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    • v.47 no.1
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    • pp.20-29
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    • 2017
  • Purpose: The microstructural characteristics of trabecular bone were identified using micro-computed tomography (micro-CT), in order to develop a potential strategy for implant surface improvement to facilitate osseointegration. Methods: Alveolar bone specimens from the cadavers of 30 humans were scanned by high-resolution micro-CT and reconstructed. Volumes of interest chosen within the jaw were classified according to Hounsfield units into 4 bone quality categories. Several structural parameters were measured and statistically analyzed. Results: Alveolar bone specimens with D1 bone quality had significantly higher values for all structural parameters than the other bone quality categories, except for trabecular thickness (Tb.Th). The percentage of bone volume, trabecular separation (Tb.Sp), and trabecular number (Tb.N) varied significantly among bone quality categories. Tb.Sp varied markedly across the bone quality categories (D1: $0.59{\pm}0.22mm$, D4: $1.20{\pm}0.48mm$), whereas Tb.Th had similar values (D1: $0.30{\pm}0.08mm$, D4: $0.22{\pm}0.05mm$). Conclusions: Bone quality depended on Tb.Sp and number-that is, endosteal space architecture-rather than bone surface and Tb.Th. Regardless of bone quality, Tb.Th showed little variation. These factors should be taken into account when developing individualized implant surface topographies.

Comparison of limited- and large-volume cone-beam computed tomography using a small voxel size for detecting isthmuses in mandibular molars

  • de Souza Tolentino, Elen;Andres Amoroso-Silva, Pablo;Alcalde, Murilo Priori;Yamashita, Fernanda Chiguti;Iwaki, Lilian Cristina Vessoni;Rubira-Bullen, Izabel Regina Fischer;Duarte, Marco Antonio Hungaro
    • Imaging Science in Dentistry
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    • v.51 no.1
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    • pp.27-34
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    • 2021
  • Purpose: This study was performed to compare the ability of limited- and large-volume cone-beam computed tomography (CBCT) to display isthmuses in the apical root canals of mandibular molars. Materials and Methods: Forty human mandibular first molars with isthmuses in the apical 3 mm of mesial roots were scanned by micro-computed tomography (micro-CT), and their thickness, area, and length were recorded. The samples were examined using 2 CBCT systems, using the smallest voxels and field of view available for each device. The Mann-Whitney, Friedman, and Dunn multiple comparison tests were performed (α=0.05). Results: The 3D Accuitomo 170 and i-Cat devices detected 77.5% and 75.0% of isthmuses, respectively (P>0.05). For length measurements, there were significant differences between micro-CT and both 3D Accuitomo 170 and i-Cat(P<0.05). Conclusion: Both CBCT systems performed similarly and did not detect isthmuses in the apical third in some cases. CBCT still does not equal the performance of micro-CT in isthmus detection, but it is nonetheless a valuable tool in endodontic practice.

Micro-computed tomography for assessing the internal and external voids of bulk-fill composite restorations: A technical report

  • Tosco, Vincenzo;Monterubbianesi, Riccardo;Furlani, Michele;Giuliani, Alessandra;Putignano, Angelo;Orsini, Giovanna
    • Imaging Science in Dentistry
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    • v.52 no.3
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    • pp.303-308
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    • 2022
  • Purpose: This technical report aims to describe and detail the use of micro-computed tomography for a reliable evaluation of the bulk-fill composite/tooth interface. Materials and Methods: Bulk-fill composite restorations in tooth cavities were scanned using micro-computed tomography to obtain qualitatively and quantitatively valuable information. Two-dimensional information was processed using specific algorithms, and ultimately a 3-dimensional (3D) specimen reconstruction was generated. The 3D rendering allowed the visualization of voids inside bulk-fill composite materials and provided quantitative measurements. The 3D analysis software VG Studio MAX was used to perform image analysis and assess gap formation within the tooth-restoration interface. In particular, to evaluate internal adaptation, the Defect Analysis addon module of VG Studio Max was used. Results: The data, obtained with the processing software, highlighted the presence and the shape of gaps in different colours, representing the volume of porosity within a chromatic scale in which each colour quantitatively represents a well-defined volume. Conclusion: Micro-computed tomography makes it possible to obtain several quantitative parameters, providing fundamental information on defect shape and complexity. However, this technique has the limit of not discriminating materials without radiopacity and with low or no filler content, such as dental adhesives, and hence, they are difficult to visualise through software reconstruction.

Comparison of micro-computerized tomography and cone-beam computerized tomography in the detection of accessory canals in primary molars

  • Acar, Buket;Kamburoglu, Kivanc;Tatar, Ilkan;Arikan, Volkan;Celik, Hakan Hamdi;Yuksel, Selcen;Ozen, Tuncer
    • Imaging Science in Dentistry
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    • v.45 no.4
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    • pp.205-211
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    • 2015
  • Purpose: This study was performed to compare the accuracy of micro-computed tomography (CT) and cone-beam computed tomography (CBCT) in detecting accessory canals in primary molars. Materials and Methods: Forty-one extracted human primary first and second molars were embedded in wax blocks and scanned using micro-CT and CBCT. After the images were taken, the samples were processed using a clearing technique and examined under a stereomicroscope in order to establish the gold standard for this study. The specimens were classified into three groups: maxillary molars, mandibular molars with three canals, and mandibular molars with four canals. Differences between the gold standard and the observations made using the imaging methods were calculated using Spearman's rho correlation coefficient test. Results: The presence of accessory canals in micro-CT images of maxillary and mandibular root canals showed a statistically significant correlation with the stereomicroscopic images used as a gold standard. No statistically significant correlation was found between the CBCT findings and the stereomicroscopic images. Conclusion: Although micro-CT is not suitable for clinical use, it provides more detailed information about minor anatomical structures. However, CBCT is convenient for clinical use but may not be capable of adequately analyzing the internal anatomy of primary teeth.

Influence of reconstruction parameters of micro-computed tomography on the analysis of bone mineral density

  • Gaeta-Araujo, Hugo;Nascimento, Eduarda Helena Leandro;Brasil, Danieli Moura;Madlum, Daniela Verardi;Haiter-Neto, Francisco;Oliveira-Santos, Christiano
    • Imaging Science in Dentistry
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    • v.50 no.2
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    • pp.153-159
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    • 2020
  • Purpose: This study was conducted evaluate the influence of reconstruction parameters of micro-computed tomography (micro-CT) images on bone mineral density (BMD) analyses. Materials and Methods: The sample consisted of micro-CT images of the maxillae of 5 Wistar rats, acquired using a SkyScan 1174 unit (Bruker, Kontich, Belgium). Each acquisition was reconstructed following the manufacturer's recommendations(standard protocol; SP) for the application of artifact correction tools(beam hardening correction [BHC], 45%; smoothing filter, degree 2; and ring artifact correction [RAC], level 5). Additionally, images were reconstructed with 36 protocols combining different settings of artifact correction tools (P0 to P35). BMD analysis was performed for each reconstructed image. The BMD values obtained for each protocol were compared to those obtained using the SP through repeated-measures analysis of variance with the Dunnett post hoc test(α=0.05). Results: The BMD values obtained from all protocols that used a BHC of 45% did not significantly differ from those obtained using the SP (P>0.05). The other protocols all yielded significantly different BMD values from the SP(P<0.05). The smoothing and RAC tools did not affect BMD values. Conclusion: BMD values measured on micro-CT images were influenced by the BHC level. Higher levels of BHC induced higher values of BMD.