• Title/Summary/Keyword: X-Ray fluorescence spectrometer analysis

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Characteristics of Clay Minerals in Sihwa Area (시화지구 연약점토의 광물학적 특성)

  • 김낙경;박종식;김유신
    • Proceedings of the Korean Geotechical Society Conference
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    • 2003.03a
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    • pp.773-780
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    • 2003
  • The characteristics of soft clays is very important for the land development plan. This study is to investigate correlations between the engineering properties and the characteristics of clay minerals of the disturbed clay samples obtained from Sihwa area. This study included X-Ray Diffraction Analysis, X-Ray Fluorescence Spectrometer Analysis, Scanning Electron Microscopy Analysis and Energy Dispersive X-Ray Spectrometer Analysis. The correlations between the clay mineral properties and the laboratory and field testing results were investigated.

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The Correlations between Mineralogy and Engineering Characteristics of Soft Clay in Sihwa Area (시화지구 연약점토의 광물학적 특성과 공학적 특성의 상관관계)

  • Kim Nak-Kyung;Park Jong-Sik;Joo Yong-Sun
    • Journal of the Korean Geotechnical Society
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    • v.20 no.9
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    • pp.155-166
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    • 2004
  • The characteristics of soft clays are very important for the land development plan. This study is to investigate correlations between the engineering properties and the characteristics of clay minerals of the undisturbed clay samples obtained from Sihwa area. This study included X-Ray diffraction analysis, X-Ray fluorescence spectrometer analysis, scanning electron microscopy analysis and energy dispersive X-Ray spectrometer analysis. The correlations between the clay mineral properties and the laboratory and field testing results were investigated. The characteristics of soft clay in Sihwa area were compared with those in Yangsan and Kunsan area.

The analytical application for cement using X-Ray diffraction and X-Ray fluorescence spectrometer (X-Ray Diffraction과 X-Ray Fluorescence를 이용한 시멘트 비교 분석)

  • Jung, Ji Eun;Jang, Yu Rim;Kim, Ki-Wook;Heo, Sangcheol;Min, Ji-Sook
    • Analytical Science and Technology
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    • v.26 no.5
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    • pp.340-351
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    • 2013
  • The chemical element and structural characterization of different types of cements and its brick stones are been investigated under forensic aspects using X-ray florescence (XRF) and X-ray diffraction (XRD) spectrometer. The XRF provides rapid compositional data for controlling almost all stages of raw materials, clinker and cement. The decisive advantage of XRD methods is based on the unique character of the diffraction patterns of crystalline substances, the ability to distinguish between elements and their oxides, and the possibility to identify chemical compounds, polymeric forms, and mixed crystals by non-destructive examination. Therefore, combination of these examinations is useful and able to apply for the forensic analysis in comparison of cements and brick stones. There are more study remained to determine the viability of method for forensic analysis of brick stones and the limits of the discrimination that can be achieved.

X-ray Fluorescence Analysis of Chemical Ingredients for Portland Cement (X-선 형광분석법에 의한 포틀란드 시멘트의 정량분석)

  • 임헌진;백연봉;김도생;윤준수;이경원
    • Journal of the Korean Ceramic Society
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    • v.33 no.8
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    • pp.928-934
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    • 1996
  • Quantitative analysis each portland cement components was conducted by standard calibration method using X-ray fluorescence spectrometer. Standard sample and the unknown sample were prepared by fused cast bead method. In checking the errors of standard cement 227A372 the relative errors of constituents such as CaO, SiO2, Al2O3, Fe2O3, MgO and SrO were less than 1% and the relative errors of constituents such as So3, K2O, TiO2, Na2O P2O5, and Mn2O3 were less than 5% Sample preparation was mainly contributed to the errors. Compared with general wet chemical method the results of X-ray fluorescence analyses were more precise and accurate. Moreover it is possible to analyze precisely a little amount of the constituents such as SrO, Mn2O3 and P2O5 the analyses of which were very difficult using the wet chemical method.

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Mineral Properties of Yangsan.Mulkum Clay (양산물금 점토의 광물학적 특성)

  • 정하익;이용수;진규남;진현식
    • Proceedings of the Korean Geotechical Society Conference
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    • 1999.10a
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    • pp.75-80
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    • 1999
  • In this study, clay sampled from Yangsan$.$Mulkum site were used to analyze mineral properties. Mineral and chemical properties of clay were investigated through X-ray fluorescence spectrometer(XRF), X-Ray Diffraction(XRD), and Scanning Electron Microscope(SEM) analysis. The result of this test represents that Yangsan$.$Mulkum clay are composed of quartz, albite, anorthite, orthocalse and illite.

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A Study of Neolithic era Plain Coarse Pottery of Cheju Island by Mossbauer Spectroscopy (제주도 신석기 토기에 대한 Mossbauer 연구)

  • 윤태건;최원준;고정대;홍성락
    • Journal of the Korean Magnetics Society
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    • v.10 no.4
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    • pp.183-190
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    • 2000
  • This study aims at making a research into the physical and chemical properties of the neolithic era potterys, which are unearthed from Gosanli, Sagaeli, Bukchonli, Samyangdong and Gonaili districts in Cheju Island, by using X-ray diffraction, X-ray fluorescence spectrometer and Mossbauer spectroscopy. This results are as follows. The principal component of five plain coarse pottery sherds by X-ray fluorescence spectrometer and X-ray diffraction spectrum at the room temperature is silicate mineral which is equal to SiO$_2$, and they also have a little magetite, hematite and goethite. The most existent Fe is Fe$\^$+3/ through Mossbauer spectroscopy analysis of plain coarse pottery sherds and it is presumed that the magnetic hyperfine splitting caused this result. The ratio of Fe$\^$2+//(Fe$\^$2+/+Fe$\^$3+/) is mostly zero by Mossbauer spectrum at the room temperature of plain coarse pottery sherds and it is thought because they were fired in the atmosphere.

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