• Proceedings of the Korean Society of Tribologists and Lubrication Engineers Conference
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• 1999.11a
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• pp.233-239
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• 1999

The feasibility of an ultrasonic technique using a pulse-echo method of normal-incident compressional waves was evaluated for its sensitivity to the worn surface and near surface damage due to wear. Worn surfaces were generated at various oscillation frequency under a given load and amplitude and these surface were in situ monitored using a ultrasonic wave detection system. Analysis of the ultrasonic waves received from the worn surface revealed a close relationship between the surface and near-surface damage and the maximum echo-amplitude of the compressional waves. The ultrasonic technique was successful in assessing the level of severity of the worn surface in real time during the wear process. It is also shown that the wear depth can be easily measured by the calculation of change of the specimen thickness based on the wave speed measured for the specimen medium.

• Tribology and Lubricants
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• v.16 no.5
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• pp.351-356
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• 2000

The feasibility of an ultrasonic technique using a pulse-echo method of normal-incident compressional waves was evaluated for its sensitivity to the worn surface and near surface damage due to wear. Worn surfaces were generated at various oscillation frequency under a given load and amplitude and these surface were in situ monitored using a ultrasonic wave detection system. Analysis of the ultrasonic waves received from the worn surface revealed a close relationship between the surface and near-surface damage and the maximum echo-amplitude of the compressional waves. The ultrasonic technique was successful in assessing the level of severity of the worn surface in real time during the wear process. It is also shown that the wear depth can be easily measured by the calculation of change of the specimen thickness based on the wave speed measured for the specimen medium.

• Tribology and Lubricants
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• v.20 no.1
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• pp.7-13
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• 2004

High strength steels are widely used as tribo-materials in the field. Previous study revealed that for mild steel, the states of strain on the worn surface measured by X-ray diffraction has a good relationship with the state of wear. The objective of this study is to identify the relationship between the state of strain on the worn surface and the state of wear in high strength steels. Sliding wear tests were carried out using several hardened steels. X-ray diffraction tests were conducted to analyze the state of strain on the worn surface during wear. The experimental results indicated that the state of strain on worn surface in the hardened steel shows the same tendency as in the mild steel. It is clear that change of half value width on the worn surface as a function of sliding speeds is broadly similar in shape to wear characteristics curve and its magnitude has a good relationship with the wear rate at two different wear modes in the hardened steel.

• KSTLE International Journal
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• v.1 no.2
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• pp.69-75
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• 2000

The paper compares topography, phase contrast and force spectroscopy in atomic force microscopy data for evaluating the microheterogeneity of surface layer. The worn surface of ion-plated TiN coating was measured using both a laboratory-built and a commercial AFM. The results of analysis revealed structural and micromechanical heterogeneity of the worn surfaces. We demonstrated that the phase image allows relatively qualitative estimation of elastic modulus of the sample surface. The tribolayer formed in the worn surface possessed much lower stiffness than the original coating. It is shown that the most stable phase imaging is provided with a stiff cantilever. In this case, phase contrast is well conditioned, first of all, by microheterogeneity of elastic properties of the investigated surfaces. In this study an attempt was also made to correlate the results of phase imaging with that of the farce spectroscopy. The joint analysis of information on the surface properties obtained by the phase imaging and quantitative data measured with the force spectroscopy methods allows a better understanding of the nature of the surface micromechanical heterogeneity.

• Journal of the Korean Ceramic Society
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• v.30 no.12
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• pp.1059-1065
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• 1993

The sliding wear behavior of the plasma sprayed zirconia containing 8wt% yttria was investigated over a range of room temperature to 800℃. Both of the friction coefficient and the wear loss increased reaching its maximum at about to 499℃. and then decreased again with increasing temperature up to 800℃. The worn surface at elevated temperature were observed and analyzed by scanning electron microscopy and X-ray diffractometer to study the mechanisms of high temperature wear behavior. Surface morphology of the worn samples changes with temperature. Monoclinic (m)/tetragonal (t) x-ray peak intensity ratio of wear debris and worn surface decreased with increasing temperature. Non-transformable tetragonal (t') to metastable tetragonal (t) phase transformation of worn surface increased with increasing temperature. The results indicate that dehumidification and above phase changes are contributing to the high temperature wear behavior of the plasma sprayed ZrO2-Y2O3 coatings.

• Proceedings of the Korean Society of Tribologists and Lubrication Engineers Conference
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• 2002.10b
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• pp.223-224
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• 2002

The mechanisms of formation of transfer film under the condition of wear of Steel AISI1020 by natural rubber were investigated. The transfer film was observed and the formation mechanisms were clarified. The formation process of transfer film on the worn surface of the steel could be divided into two stages. Firstly, the adhesive layer emerged on the worn surface of the steel by adhesion of natural rubber. in which the macromolecular chains of natural rubber joined to the surface of the steel by Van der Waals' force. And then, the iron atom and metal oxide reacted with the macromolecular of natural rubber in the adhesive layer and produced Fe-polymer compound. As a result, the transfer film was formed on the worn surface of the steel. The transfer film was joined to the worn surface of the steel by the chemical bonds and electrostatic force.

• Proceedings of the Korean Society of Tribologists and Lubrication Engineers Conference
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• 2001.06a
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• pp.299-304
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• 2001

Tribofilms formed on worn surface protect the DLC coating surface and decrease the friction coefficient. However it is very difficult to evaluate their micromechanical properties due to their small thickness, inhomogeneity and discontinuity. The phase contrast images in tapping mode atomic force microscopy allow an estimation of inhomogeneity in micromechanical properties of the sample surface. The purpose of this investigation is to demonstrate how the phase contrast images contribute to the characterization of thin tribofilms.

• Carbon letters
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• v.10 no.2
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• pp.97-100
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• 2009

In this work, effects of carbon matrix on sliding friction and wear behavior of four kinds of C/C have been investigated against 40 Cr steel ring mate. Composite A with rough lamination carbon matrix (RL) shows the highest volume loss and coefficient of friction, while composite D with smooth lamination/resin carbon matrix (SL/RC) shows the lowest volume loss. The worn surface of composite A appears smooth, whereas that of composite C with smooth lamination carbon (SL) appears rough. The worn surface of composite D appears smooth under low load but rough under high load. Atomic force microscope images show that the size of wear particles on the worn surface is also dependent on the carbon matrix.

• Proceedings of the Korean Society of Tribologists and Lubrication Engineers Conference
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• 1999.11a
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• pp.19-24
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• 1999

Understanding of wear mode and prediction of wear rate of parts in sliding contact are very important in field of meterial design relating with wear resistant. This paper has been undertaken to analyze the possibility of elucidation of wear mode and prediction of wear rate for annealed steel in sliding contact using the X-ray diffraction. The sliding wear test with various velocities using pin-on-disc machine and the X-ray diffraction test on the worn surface have been carried out. The results have been shown that the magnitude of residual stress and half-value breadth on the worn surface have a good correlation with wear mode. The difference between before and after test of half-value breadth on worn surface has been shown to be exponential relation with wear rate in the same wear mode.

• Journal of Powder Materials
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• v.11 no.5
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• pp.376-382
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• 2004

Nanoscale Cu-Ni alloy nanopowders have been produced by a pulsed wire evaporation method in an inert gas. The effect of Cu-Ni alloy nanopowders as additives to motor oil on the tribological properties was studied at room temperature. The worn surfaces were characterized by Scanning Electron Microscopy (SEM) and Energy-Dispersive X-ray Spectroscopy (EDS). Cu-Ni alloy nanopowders as additives lowered coefficient of friction and wear rate. It was found that a copper containing layer on the worn surface was formed, and deposited layers of the metal cladding acted as lubricant on the worn surface, reducing the friction coefficient. It was clearly demonstrated that Cu-Ni alloy nanopowders as additives are able to restore the worn surface and to preserve the friction surfaces from wear.