• Title/Summary/Keyword: Wet mixing

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A Study on the Development and Performance Test of the Non-gravity Fluidized Dryer (무중력 유동층 건조기 개발과 성능평가)

  • Han, J.W.;Kum, S.M.;Lee, C.E.
    • Proceedings of the KSME Conference
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    • 2001.06d
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    • pp.665-670
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    • 2001
  • The purpose of this study is to develop a new type dryer, which is to proceed mixing and drying of wet-materials at the same time and drying process is carried out in a closed system. In this drying system, thermal contact occurs, when a fluidized zone is created by paddle mechanism. Accordingly, wet-materials is dried in a short time without any damage. Also wet-materials could be dried uniformly to low moisture contents. It is suitable to dry a small quantity of multi-kind materials. And drying process is carried out in a closed system, so as for environmental pollution dust not to be emitted into the atmosphere. Accordingly, it could be used to dry not only food and chemical materials, but also environmental pollution materials.

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Chemical Preparation of $PbTiO_3$ Powder from Aqueous Solution (습식반응에 의한 $PbTiO_3$ 분말제조에 관한 연구)

  • 이경희;이병하;고영래
    • Journal of the Korean Ceramic Society
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    • v.22 no.2
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    • pp.39-43
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    • 1985
  • This study presents the results of an overall effort to detemine the applicability of the chemical wet process informing lead titanate electronic ceramics. Although pure lead titanate has not proven to be an important technological materials when prepared via conventional processing procedures this work is interesting as a study of chemical wet processing and a way of preparing pbTiO3 for study. The result obtained from this experiment were as follows ; Optimum synthesis condition which synthesize PbTiO3 by chemical wet process was obtained by firing at 50$0^{\circ}C$ after mixing $Pb(OH)_2$- gel and $Ti(OH)_4$ -gel at 7$0^{\circ}C$ for 4 hours.

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Design of Smart Controller using Intelligent Algorithm for Wet Station (지능형 알고리즘을 이용한 Wet Station용 스마트 제어기 설계)

  • 홍광진;김종원;조현찬;김광선;김두용;조중근
    • Proceedings of the Korean Institute of Intelligent Systems Conference
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    • 2004.10a
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    • pp.67-70
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    • 2004
  • Semiconductor Wet Station has a very important place in semiconductor process. It is important that to discharge chemical with fit concentration and temperature using chemical supply system for clean process. The chemical supply system which is used currently is not only difficult to make a fit mixing rate of chemical which is need in clean' process, but also difficult to make fit concentration and temperature. Moreover, it has high stability but it is inefficient spatially because its volume is great. We propose In-line System to improve system with implement analysis of fluid and thermal transfer on chemical supply system and understand problem of system.

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Effects of UF Resin and Taro Adhesive Mixture on Plywood Bonding Strength (요소수지(尿素樹脂)와 토란접착제(土卵接着劑) 혼용(混用)이 합판(合板)의 접착력(接着力)에 미치는 영향(影響))

  • Lee, Phil-Woo;Park, Heon
    • Journal of the Korean Wood Science and Technology
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    • v.12 no.1
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    • pp.3-10
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    • 1984
  • Taro-UF mixed type resin system was developed for gluing plywoods. The taro adhesive that was activated with sodium hydroxide was mixed with the definite ratios of UF resin adhesive. At the sametime, wheat-UF mixed type resin was also applied with the same method as taro-UF mixed type resin The mixing ratios of taro or wheat adhesive: UF resin were 0:100, 10:90, 20:80, 30:70, 40:60, 50:50, 60:40, 80:20, and 100:0 by weight. In addition, the UF resins extended with wheat powder at the extending ratios of wheat powder UF resin, 10:90, 20:80, 30:70, 40:60, and 50:50 by weight, were also used. The dry and wet shear strengths of the plywoods of 30:70 (taro adhesive : UF resin) mixing ratio were highest. The dry shear strengths of the plywoods manufactured with the UF resin-mixing taro adhesive were higher than those of the plywoods with the UF resin-mixing wheat adhesive at 10:90, 20:80, 30:70, 40:60, 50:50, and 60:40 (taro or wheat adhesive: UF resin) mixing ratios. At all mixing ratios, the wet shear strengths of the plywoods manufactured with the UF resin-mixing taro adhesive were higher than those of the plywoods with the UF resin-mixing wheat adhesive. The dry and wet shear strengths of the plywoods manufactured with the UF resin-mixing wheat adhesive were higher than those of the plywoods with the wheat powder-extending UF resin at the mixmg ratios, 10:90, 20:80, 30:70, and 40:60 (wheat adhesive or wheat powder: UF resin). So, it was found that the plywoods manufactured with the UF resin-mixing taro adhesive and the UF resin mixing wheat adhesive had better shear strength than the plywoods with the wheat powder-extending UF resin. It was because the taro adhesive and wheat adhesive themselves took the bonding properties after being activated with alkali.

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Effects of Mixing Ratio of Urea and Mlelamine on Formaldehyde Emission and Bonding Properties of Plywoods Manufactured with Urea-Melamine Formaldehyde Adhesives (요소-멜라민 공축합 수지의 요소와 멜라민 혼합비율이 합판의 포름알데히드 방출과 접착성에 미치는 영향)

  • Park, Heon;Kang, Eun-Chang;Min, Kyeong-Heui
    • Journal of the Korea Furniture Society
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    • v.11 no.1
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    • pp.53-59
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    • 2000
  • This study was to measure formaldehyde emission and bonding strength of plywoods manufactured with urea-melamine formaldehyde adhesives, which were made from three different mixing ratios of urea and melamine, and with four different formaldehyde/urea-melamine molar ratios of 1.0,1.1,1.2 and 1.4. The results were as follows 1. Amount of formaldehyde emission was the lowest at the first method of molar ratio(F/(M+U)) 1.0. Amounts of formaldehyde emission of experimental manufactured adhesives were lower than that of commercial adhesive. 2. Bonding strength of dry specimen was the highest at the first method of molar ratio(F/(M+U)) 1.4. Dry bonding strength of molar ratio(F/(M+U)) 1.4 was similar to commercial adhesive. 3. Bonding strength of wet specimen was the highest at the second method of molar ratio(F/(M+U)) 1.4. Bonding strength of wet specimen used by the third method of molar ratio(F/(M+U)) 1.4 was almost equal to commercial adhesive.

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Understanding Wet-End Polymer Performance through Visualization of Macromolecular Events by Transmission Electron Microscopy

  • Nanko, Hiroki;Mcneal, Michelyn;Pan, Shaobo
    • Proceedings of the Korea Technical Association of the Pulp and Paper Industry Conference
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    • 2006.06a
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    • pp.1-18
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    • 2006
  • A novel transmission electron microscopy technique for the visualization of polymers adsorbed on secondary fines has been developed. This technique has been utilized in observing the adsorption behavior of various wet-end additives. The technique is sensitive enough not only to allow differentiation between linear and branched polymers, but also to observe differences in the adsorption behavior and conformational characteristics of particular polymeric derivatives. Conformational changes of a cationic polyacrylamide (CPAM) were examined in response to variations in wet-end conditions, such as mixing time and system conductivity. The molecular conformations of cationic starch and cationic guar gum were also examined by this technique. The technique has been employed to observe the effects of silica microparticles on the conformational characteristics of CPAM (drainage/retention aid) pre-adsorbed on secondary fines. The transmission electron microscopy method is a viable tool for investigating the macromolecular events that make up a large part of wet end chemistry in papermaking.

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A Study on Design of Intelligent Wet Station for Semiconductor (지능형 반도체 세정장비 설계에 관한 연구)

  • Kim Jong Won;Hong Kwagn Jin;Cho Hyun Chan;Kim Kwang Sun;Kim Doo Yong;Cho Jung Keun
    • Journal of the Semiconductor & Display Technology
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    • v.4 no.3 s.12
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    • pp.29-33
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    • 2005
  • As the integrated devices become more and more sophistcated, the diameter of wafers increased up to 300 mm and strict level of cleaning is necessary to remove the particulates on the surface of wafer. Therefore we need a new type of wet-station which can reduce DI water and chemical in the cleaning process. Moreover, it is important to control the temperature and the concentration of chemical in the wet-station. In the conventional chemical supply system, it is difficult not only to fit the mixing rate of chemicals in cleaning process, but also to fit the quantity and temperature. Thus, we propose a new chemicals supply system, which overcomes above problems by the analysis of fluid and thermal transfer on chemical supply system.

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Preparation of Silica-Filled SBR Compounds with Low Rolling Resistance by Wet Masterbatch

  • Yang, Jae-Kyoung;Park, Wonhyeong;Ryu, Changseok;Kim, Sun Jung;Kim, Doil;Seo, Gon
    • Elastomers and Composites
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    • v.55 no.1
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    • pp.26-39
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    • 2020
  • The physical properties of silica-filled SBR compounds (WSBR) prepared using silica-SBR wet masterbatches (WMB) were systematically investigated to understand the effect of the surface treatment of silica on the reinforcement performance of SBR. Treatment of silica with bis(triethoxysilylpropyl)tetrasulfide (TESPT) in the liquid phase, followed by mixing with an SBR solution and recovery by water stripping, easily produced silica-SBR WMB. However, insufficient surface treatment in terms of the amount and stability of the incorporated TESPT led to considerable silica loss and inevitable TESPT elution. Pretreatment of silica in the gas phase with TESPT and another organic material that enabled the formation of organic networks among the silica particles on the surface provided hydrophobated silica, which could be used to produce silica-SBR WMB, in high yields of above 99%. The amount and type of organic material incorporated into silica greatly influenced the cure characteristics, processability, and tensile and dynamic properties of the WSBR compounds. The TESPT and organic material stably incorporated into silica increased their viscosity, while the organic networks dispersed on the silica surface were highly beneficial for reducing their rolling resistance. Excessive dosing of TESTP induced low viscosity and a high modulus. The presence of connection bonds formed by the reaction of glycidyloxy groups with amine groups on the silica surface resulted in physical entanglement of the rubber chains with the bonds in the WSBR compounds, leading to low rolling resistance without sacrificing the mechanical properties. Mixing of the hydrophobated silica with a rubber solution in the liquid phase improved the silica dispersion of WSBR compounds, as confirmed by their low Payne effect, and preservation of the low modulus enhanced the degree of entanglement.

Influence of Silane Coupling Agent Treatments on Physical Properties of Rubbery Materials (실란 커플링제 처리방법이 고무 물성에 미치는 영향)

  • Woon, Jin-Bok
    • Elastomers and Composites
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    • v.36 no.4
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    • pp.237-245
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    • 2001
  • A study was made on the chemical treatment of silica and silane coupling agents, bistriethox ysilylpropyltetrasulfide(Si 69) and ${\gamma}$-mercaptopropyltrimethoxy silane (MPS) for reinforcement of silica formulation. The effects of chemical treatment method and the most popular two coupling agents were examined. The results clearly indicate that the wet method, coupling agent is combined chemically with the silica prior to mixing, has more dispersion, wetting ability, dynamic properties and stability than the dry method, coupling agent is premixed directly with the silica. The mixing was done using a bench-type kneader having two mixing cam and a two-roll mill, under approximately similar conditions. The physical properties of SBR vulcanizates give rise to marked improvements by addition of Si 69 and MPS in comparison with without silane coupling agents. The optimum amount of Si 69 and MPS was 2 w/w% by experiments in the dry method but was 4 w/w% by EA and TGA analysis in the wet method.

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Enhancement of Au·Ag Leaching by Mechanochemical Activation and Thiourea-Thiocyanate Mixing Solution (기계적-화학적 활성화와 티오요소-티오시안산염 혼합용액에 의한 Au·Ag 용출 향상)

  • You, Don-Sang;Park, Cheon-Young
    • Journal of the Korean earth science society
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    • v.35 no.6
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    • pp.401-411
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    • 2014
  • In order to enhance the Au Ag leach rate, a mechanochemical activation process and a mixed thiourea-thiocyanate solution has been applied to Au concentrate. To achieve mechanochemical activation, the Au concentrate was mechanically ground using a dry and a wet process. The results of a particle size distribution analysis and an XRD analysis, average particle size and crystallite size were much smaller in the dry-sample than in the concentrate sample. As well the size was smaller in the wet-sample than in the dry-sample. In SEM and XRD analysis, the amorphization effect was observed in the wet-sample due to mechanochemical activation. Au Ag leaching experiments were carried out with a thiourea solution, a thiocyanate solution and a mixed thiourea-thiocyanate solution. The Au Ag leach rate was much greater in the dry-ground-sample than in the concentrate sample, and the leach rate was greater in the wet-ground-sample than in the dry-sample. The Au Ag leach rate was much greater in the thiocyanate solution than in the thiourea solution, and the leaching rate was much greater in the mixed thiourea-thiocyanate solution than in the thiocyanate solution. Up to a 99% leach rate for Au Ag were only achieved in the wet-sample using the mixed thiourea-thiocyanate leaching solution.