• Journal of Environmental Health Sciences
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• v.35 no.2
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• pp.130-142
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• 2009

This study compared FTIR with XRD method for the analysis of quartz by % recovery, coefficient of variation (CV) and influence of the interference. the results were as the following. 1. In FTIR method, the coefficient of determination ($r^2$) was 0.9998 in a calibration curve of $695\;cm^{-1}$, and the limit of detection was $4.9{\mu}g/sample$. 2. The highest recovery was $799\;cm^{-1}$ (98.2%). 3. The CVpooled of the FTIR method was approximately 10% in three wave numbers. 4. The analysis of qualitative and quantitative for quartz is difficult with mixed cristobalite and iron oxide. 5. In XRD method with rotating sample holder and LynxEye detector, the coefficient of determination was 0.9996 in a calibration curve, and the limit of detection was $5.9{\mu}g/sample$. 6. The recovery and CV pooled were 104.3%, and 11 %, respectively. 7. In muffle furnace ashing, the quartz weight decreased to 34% when the maximum weight of the iron oxide was more than eight times. In conclusion, the accuracy (% recovery) and precision (CV) of FTIR and XRD method for analyzing $\alpha$-quartz were similar. FTIR method was a disadvantage for sample matrix because it indicates possibility of interference. However, XRD method distinguished specific crystalline forms of silica, and the majority of silicate minerals. In addition, XRD method recommend filter dissolution to pretreatment method.

• Transactions of the Korean Society of Mechanical Engineers B
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• v.29 no.6 s.237
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• pp.671-686
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• 2005

The transient nature and complex geometries of two-phase gas-liquid flows cause fundamental difficulties when measuring flow velocity using an electromagnetic flowmeter. Recently, a current-sensing flowmeter was introduced to obtain measurements with high temporal resolution (Ahn et al.). In this study, current-sensing flowmeter theory was applied to measure the fast velocity transients in slug flows. The velocity fields of axisymmetric gas-liquid slug flow in a vertical pipe were obtained using Volume-of-Fluid (VOF) method, and the virtual potential distributions for the electrodes of finite size were also computed using the finite volume method for simulating slug flow. The output signal prediction for slug flow was carried out from the velocity and virtual potential (or weight function) fields. The flowmeter was numerically calibrated to obtain the cross-sectional liquid mean velocity at an electrode plane from the predicted output signal. Two calibration parameters are proposed for this procedure: a flow pattern coefficient and a localization parameter. The flow pattern coefficient was defined by the ratio of the liquid resistance between the electrodes for two-phase flow with respect to that for single-phase flow, and the localization parameter was introduced to avoid errors in the flowmeter readings caused by liquid acceleration or deceleration around the electrodes. These parameters were also calculated from the computed velocity and virtual potential fields. The results can be used to obtain the liquid mean velocity from the slug flow signal measured by a current-sensing flowmeter.

• Journal of KIISE
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• v.44 no.6
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• pp.559-565
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• 2017

A UAV(unmanned aerial vehicle) requires higher reliability for external effects such as electromagnetic interference because a UAV is operated by pre-designed programs that are not under human control. The design of a small UAV with a complete resistance against the external effects, however, is difficult because of its weight and size limitation. In this circumstance, a conventional small UAV dropped to the ground when an external effect caused the rebooting of the flight-control computer(FCC); therefore, this paper presents a novel algorithm for the improvement of the flight safety of a small UAV. The proposed algorithm consists of three steps. The first step comprises the calibration of the navigation equipment and validation of the calibrated data. The second step is the storage of the calibration data from the UAV take-off. The third step is the restoration of the calibration data when the UAV is in flight and FCC has been rebooted. The experiment results show that the flight-control system can be safely operated upon the rebooting of the FCC.

• Journal of the Korean Vacuum Society
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• v.12 no.3
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• pp.157-161
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• 2003

Nowadays there are increasing demands for more accurate measurement of atmospheric pressure according to the development of environmental industries. One of the most important pressure gauges for satisfying these demands is a quartz resonance barometer. In order to calibrate such an accurate barometer, laser/ultrasonic mercury manometers have been used. However, complexity and cost of mercury manometers made it out of use gradually. As a substitute, a gas-operated pressure balance is used for calibration of precise barometers. In such a case, commercially available pressure balances cannot be entirely suitable because consequent exposure of the piston, cylinder and masses to the atmosphere causes the problem of contamination. In this paper a device for changing the masses in situ without breaking the vacuum is described. This device made it possible to add or remove weights in the absolute mode, thereby greatly reducing the time between observations. At the same time, we investigated the characteristics of a commercial precise barometer using this new apparatus.

• Journal of the Korean Institute of Illuminating and Electrical Installation Engineers
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• v.22 no.4
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• pp.61-67
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• 2008

In this papar, the flow meter system for pulverized coal is developed for the pulverizer-burner system of the boiler or the blast furnace. The sensor of the system a lied the capacitance with a pair of electrode on the outer wall of the electric insulator pipe. The circuit is designed for the measurement of the granule flow density combining as a measuring electrode and a reference. In order to measure granule-flow density, the calibration curve between the weight measured from loadcell and the voltage from the circuit is created. It is verified that the flow meter system has reliability and accuracy using on-line test.

• Survey Research
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• v.5 no.2
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• pp.49-70
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• 2004

This paper is a broad review about general regression estimators, which are very useful when auxiliary variables are available in survey sampling. We investigate the process of development of general regression estimators from birth to suggestion of variance estimation method and examine some properties of general regression estimators by comparing with calibration and QR estimators. We also present some forms of general regression estimators available under complex sampling designs such as stratified sampling and cluster sampling. Finally, we comment some advantages as well as disadvantages of general regression estimators and theoretical and practical development in the future.

• Journal of the Korean Society of Manufacturing Process Engineers
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• v.11 no.1
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• pp.46-49
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• 2012

Gears are reliable and efficient power transmission elements. They have been widely used in all kinds of machinery. Nowadays, resource conservation energy conservation environmental improvements from the request of the compact, light weight, high efficiency, low cost Higher efficiency is required. Tooth root and bottom profiles of cylindrical gears affect bending fatigue life, but they are hard to measure with conventional gear measuring machine(GMM), because GMM is normally customized to measure only gear working flanks. The authors try to develop a new type of GMM by installing an extra 3D scanning probe and control software to measure tooth root and bottom profiles. First, in order to measure in various directions, a 3D scanning probe has been attached to the GMM developed. Next, calibration algorithm has been developed. Deviations of the calibration results are measured and it is found that systematic error must be caused by heat from driving motors. A new alternative GMM with driving motors generating less heat was designed and two GMMs are compared. Finally, 3 Dimension measurement of tooth root and bottom profiles of cylindrical gears is described.

• Bulletin of the Korean Chemical Society
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• v.23 no.3
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• pp.488-496
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• 2002

SPME techniques have proven to be very useful tools in the analysis of wide VOCs in the air. In this study, we estimated VOCs in ambient and workplace air using a Tedlar ba /SPME/GC/MS system. The calibration curve was set to be linear over the range of 1-30 ppbv. The detection limits ranged from 10 pptv to 0.93 ppbv for all VOCs. Reproducibility of TO-14 target gas mixtures by SPME/GC/MS averaged at 8.8 R.S.D (%). Air toxic VOCs (hazardous air pollutants, HAPs) containing a total of forty halohydrocarbons, aromatics, and haloaro-matic carbons could be analyzed with significant accuracy, detection limit and linearity at low ppbv level. Only reactive VOCs with low molecular weight, such as chloromethane, vinylchloride, ethylchloride and 1,2-dichloro-ethane, yielded relatively poor results using this technique. In ambient air samples, ten VOCs were identified and quantified after external calibration. VOC concentration in ambient and workplace air ranged from 0.04 to 1.85 ppbv. The overall process was successfully applied to identify and quantify VOCs in ambient/workplace air.

• Steel and Composite Structures
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• v.34 no.4
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• pp.561-580
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• 2020

Buckling restrained braces (BRBs) were developed as an enhanced alternative to conventional braces by restraining their global buckling, thus allowing development of a stable quasi-symmetric hysteretic response. A wider adoption of buckling restrained braced frames is precluded due to proprietary character of most BRBs and the code requirement for experimental qualification. To overcome these problems, BRBs with capacities corresponding to typical steel multi-storey buildings in Romania were developed and experimentally tested in view of prequalification. In the second part of this paper, a complex nonlinear numerical model for the tested BRBs was developed in the finite element environment Abaqus. The calibration of the numerical model was performed at both component (material models: steel, concrete, unbonding material) and member levels (loading, geometrical imperfections). Geometrically and materially nonlinear analyses including imperfections were performed on buckling restrained braces models under cyclic loading. The calibrated models were further used to perform a parametric study aiming at assessing the influence of the strength of the buckling restraining mechanism, concrete class of the infill material, mechanical properties of steel used for the core, self-weight loading, and frame effect on the cyclic response of buckling restrained braces.

• Journal of Biosystems Engineering
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• v.22 no.2
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• pp.256-265
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• 1997

The objectives of this study were to examine the ability to predict soluble solid and firmness in intact apples based on the visible/near-infrared spectroscopic technique. Two cultivars of apples, Delicious and Gala, were handled, tested and analyzed separately. Reflectance spectra, Magness-Tayor (MT) firmness, and soluble solids in apples were measured sequentially. Maximum and minimum diameters, height, and weight of apples were recorded before the MT firmness tests. A spectrophotometer was used to collect reflectance spectra of intact apples over a wavelength range of 400 to 2, 498 nm. The W firmness tests were conducted using a standard 11.1mm (7/16 in.) MT probe mounted in an Instron universal testing machine. A digital refractormeter was used to measure soluble solid contents in the apples. Apple samples were divided into a calibration set and a prediction set. The calibration set was used during model development, and the prediction set was used to predict soluble solids and firmness from unknown spectra. The method of partial least square (PLS) analysis was used. An unique set of PLS loading vectors (factors) was developed for soluble solid content and firmness. The PLS model showed good correlations between predicted and measured soluble solids of intact apples in 860～1078 nm of the wavelengths. However, the PLS analysis was not good enough to predict the apple firmness.